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    PRODUCTION OF ALKANESULFONIC ACID
    7.
    发明专利
    PRODUCTION OF ALKANESULFONIC ACID 失效

    公开(公告)号：JPS61267544A

    公开(公告)日：1986-11-27

    申请号：JP27608585

    申请日：1985-12-10

    申请人： NIPPON MINING CO

    发明人： SATO YASUKAZU ,  MATSUDA KENICHI ,  SUZUKA TERUO ,  OZAKI HIROMI

    IPC分类号： B01J19/12 ,  C07C67/00 ,  C07C301/00 ,  C07C303/14 ,  C07C309/02

    摘要： PURPOSE:To obtain the titled compound useful as a raw material for surfactants, etc., by bringing a reaction solution partially into contact with sodium sulfite and returning the resultant reaction solution to the reaction system in reacting a saturated hydrocarbon with sulfur dioxide and oxygen in the absence of water in the reaction system by irradiation with light. CONSTITUTION:A saturated hydrocarbon is reacted with sulfur dioxide and oxygen in substantially the absence of water in a reaction system by irradiation with light at

    Production of alkanesulfonic acid
    9.
    发明专利
    Production of alkanesulfonic acid 失效
    生产碱性磷酸

    公开(公告)号：JPS60193961A

    公开(公告)日：1985-10-02

    申请号：JP4711784

    申请日：1984-03-14

    申请人： Nippon Mining Co Ltd

    发明人： SATOU YASUKAZU ,  YAMANE MAMORU ,  OZAKI HIROMI

    IPC分类号： C07C309/02 ,  C07C67/00 ,  C07C301/00 ,  C07C303/14 ,  C07C309/03

    摘要： PURPOSE: To produce the titled compound continuously, in high yield, preventing the deposition of colored material to the wall of the light source side, without lowering the rate of reaction, by dispersing sodium sulfite in a saturated hydrocarbon, and carrying out the photo-sulfoxylation reaction in the absence of water.
    CONSTITUTION: The objective compound can be produced by adding sodium sulfite to a saturated hydrocarbon (e.g. 8W24C n-paraffin), and reacting sulfur dioxide with oxygen under the radiation of light having a wavelength of ≤500nm using a high-pressure mercury lamp or low-pressure mercury lamp, etc. essentially in the absence of water, at -20W+200°C and 0W50atm. The amount of sodium sulfite is 0.1W10wt% based on the saturated hydrocarbon.
    USE: Useful as a raw material of an alkanesulfonic acid salt which is a surfactant for synthetic detergent, etc.
    COPYRIGHT: (C)1985,JPO&Japio

    摘要翻译： 目的：为了以高产率连续地制备标题化合物，通过将亚硫酸钠分散在饱和烃中，防止着色材料沉积到光源侧壁而不降低反应速率， 在没有水的情况下进行磺化反应。 构成：目标化合物可以通过将亚硫酸钠加入到饱和烃（例如8-24℃正构链烷烃）中，并在波长<= 500nm的光的辐射下使用高压汞使二氧化硫与氧反应来制备 灯或低压汞灯等，基本上在没有水的情况下，在-20〜+ 200℃和0-50℃。 亚硫酸钠的量基于饱和烃为0.1-10wt％。 用途：作为合成洗涤剂等的表面活性剂的烷烃磺酸盐的原料，有用