Abstract:
An apparatus for synthesis and assaying of materials is provided that significantly improves throughput efficiency by allowing for material synthesis and assaying in the same assembly while possessing the ability to reach higher pressures and higher temperatures than existing designs capable of synthesis and assaying in the same assembly. In addition, the apparatus provides for gas flow over the material sample, allowing for a number of materials to be synthesized within the apparatus by gas synthesis.
Abstract:
An apparatus for synthesis and assaying of materials is provided that significantly improves throughput efficiency by allowing for material synthesis and assaying in the same assembly while possessing the ability to reach higher pressures and higher temperatures than existing designs capable of synthesis and assaying in the same assembly. In addition, the apparatus provides for gas flow over the material sample, allowing for a number of materials to be synthesized within the apparatus by gas synthesis.
Abstract:
A device for infusing liquid into material samples includes a container assembly configured to contain multiple material samples submerged in liquid. The material samples have pores containing air or gas. A pressure source and a vacuum source are both operatively connectable to the container assembly and alternately communicable with the container assembly to force the liquid to at least substantially fill the pores. The samples are thus ready for further processing, testing or use. A method of filling pores in material samples with liquid includes supporting multiple material samples within liquid in an airtight container assembly. The method further includes alternately applying a vacuum source and a pressure source to the container assembly, thereby replacing air with liquid in the pores of the material samples.
Abstract:
An apparatus for material synthesis and assaying includes a well assembly having a well containing material. The well assembly is configured such that the material may be synthesized within the well. A measurement device, including a gas delivery and control system is operatively connected to the well assembly and is configured to provide gas to the well for measuring at least one property of the material in the well. An enclosure assembly is provided that includes an enclosure substantially enclosing the gas delivery and control system and is configured to maintain the gas at a predetermined temperature.