公开(公告)号：US20130129611A1

公开(公告)日：2013-05-23

申请号：US13673661

申请日：2012-11-09

Applicant: BASF SE

Inventor： Stefan Maurer ,  Hanpeng Jin ,  Jeff Yang ,  Ulrich Müller

IPC: C01B39/02

CPC classification number: C01B39/02 ,  B01J29/7015 ,  C01B39/026 ,  C01B39/46

Abstract: The present invention relates to an organotemplate-free synthetic process for the production of a zeolitic material having a CHA-type framework structure comprising YO2, X2O3, and optionally comprising Z2O5, wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO2, one or more sources for X2O3, and seed crystals having a CHA framework structure, wherein the CHA framework structure of the seed crystals comprises YO2, X2O3, and optionally comprises Z2O5; and (2) crystallizing the mixture obtained in step (1); wherein Y is a tetravalent element, X is a trivalent element, and Z is a pentavalent element, wherein optionally one or more sources for Z2O5 are further provided in step (1), and wherein if the CHA framework of the seed crystals does not contain Z2O5, the seed crystals then have a YO2:X2O3 molar ratio of 5 or greater than 5.

Abstract translation: 本发明涉及一种用于生产具有包含YO 2，X 2 O 3和任选地包含Z 2 O 5的CHA型骨架结构的沸石材料的有机模板合成方法，其中所述方法包括以下步骤：（1）提供包含 YO2的一种或多种来源，X 2 O 3的一种或多种来源和具有CHA骨架结构的晶种，其中晶种的CHA骨架结构包含YO 2，X 2 O 3，并且任选包含Z 2 O 5; 和（2）使步骤（1）中获得的混合物结晶; 其中Y是四价元素，X是三价元素，Z是五价元素，其中在步骤（1）中还可以任选地提供一种或多种Z2O5源，并且其中如果晶种的CHA骨架不包含 Z2O5，然后晶种的YO 2：X 2 O 3摩尔比为5或大于5。

公开(公告)号：US09527751B2

公开(公告)日：2016-12-27

申请号：US13673661

申请日：2012-11-09

Applicant: BASF SE

Inventor： Stefan Maurer ,  Hanpeng Jin ,  Jeff Yang ,  Ulrich Müller

IPC: C01B39/02 ,  B01J29/70 ,  C01B39/46

CPC classification number: C01B39/02 ,  B01J29/7015 ,  C01B39/026 ,  C01B39/46

Abstract: The present invention relates to an organotemplate-free synthetic process for the production of a zeolitic material having a CHA-type framework structure comprising YO2, X2O3, and optionally comprising Z2O5, wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO2, one or more sources for X2O3, and seed crystals having a CHA framework structure, wherein the CHA framework structure of the seed crystals comprises YO2, X2O3, and optionally comprises Z2O5; and (2) crystallizing the mixture obtained in step (1); wherein Y is a tetravalent element, X is a trivalent element, and Z is a pentavalent element, wherein optionally one or more sources for Z2O5 are further provided in step (1), and wherein if the CHA framework of the seed crystals does not contain Z2O5, the seed crystals then have a YO2:X2O3 molar ratio of 5 or greater than 5.

Abstract translation: 本发明涉及一种用于生产具有包含YO 2，X 2 O 3和任选地包含Z 2 O 5的CHA型骨架结构的沸石材料的有机模板合成方法，其中所述方法包括以下步骤：（1）提供包含 YO2的一种或多种来源，X 2 O 3的一种或多种来源和具有CHA骨架结构的晶种，其中晶种的CHA骨架结构包含YO 2，X 2 O 3，并且任选包含Z 2 O 5; 和（2）使步骤（1）中获得的混合物结晶; 其中Y是四价元素，X是三价元素，Z是五价元素，其中在步骤（1）中还可以任选地提供一种或多种Z2O5源，并且其中如果晶种的CHA骨架不包含 Z2O5，然后晶种的YO 2：X 2 O 3摩尔比为5或大于5。