公开(公告)号：US20140227162A1

公开(公告)日：2014-08-14

申请号：US13871285

申请日：2013-04-26

Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY

Inventor： Han-IK JOH ,  Su Young SON ,  Sung Ho LEE ,  Tae-Wook KIM

IPC: C01B31/04

CPC classification number: C01B31/0446 ,  B01J23/40 ,  B01J23/70 ,  B01J35/0013 ,  B01J35/06 ,  B01J35/065 ,  B01J37/0215 ,  B01J37/0232 ,  B32B18/00 ,  C01B32/184 ,  C01B2204/04 ,  C01B2204/32 ,  C04B35/524 ,  C04B35/62222 ,  C04B38/0032 ,  C04B2111/00844 ,  C04B2237/363 ,  C04B35/52

Abstract: The present disclosure relates to a polymer-based large-area carbon nanomesh and a method for preparing same. More particularly, the present disclosure provides a method for preparing a carbon nanomesh, including: preparing a polymer nanofilm by coating a solution of a block copolymer or a polymer mixture thereof on a substrate; stabilizing the polymer nanofilm by annealing such that the polymer nanofilm is phase-separated, a pore-forming polymer is removed and, at the same time, a nanomesh-forming polymer forms a stabilized porous polymer nanomesh; and carbonizing the stabilized porous polymer nanomesh by annealing at high temperature to prepare a carbon nanomesh. Using phase separation and cyclization of a polymer, a large-area carbon nanomesh with superior activity can be prepared simply with high reproducibility in large scale.

Abstract translation: 本公开内容涉及基于聚合物的大面积碳纳米体及其制备方法。 更具体地说，本公开内容提供了制备碳纳米管的方法，包括：通过将嵌段共聚物或其聚合物混合物的溶液涂布在基材上来制备聚合物纳米薄膜; 通过退火来稳定聚合物纳米薄膜，使得聚合物纳米薄膜相分离，除去成孔聚合物，同时形成纳米成型聚合物形成稳定的多孔聚合物纳米薄膜; 并通过在高温下退火来碳化稳定化的多孔聚合物纳米颗粒以制备碳纳米薄膜。 使用聚合物的相分离和环化，可以简单地以大规模的高再现性制备具有优异活性的大面积碳纳米体。