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公开(公告)号:US06352635B1
公开(公告)日:2002-03-05
申请号:US09760325
申请日:2001-01-12
申请人: Karl Leopold Krumel , Craig Joseph Bott , Michael Frederick Gullo , Carey Lee Scortichini , John Wesley Hull, Jr.
发明人: Karl Leopold Krumel , Craig Joseph Bott , Michael Frederick Gullo , Carey Lee Scortichini , John Wesley Hull, Jr.
IPC分类号: C25B300
摘要: Halogen substituents in the 5-position of 4-aminopicolinic acids are selectively reduced in the presence of halogen substituents in the 3- and 6-positions by electrolysis.
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2.
公开(公告)号:US07488828B2
公开(公告)日:2009-02-10
申请号:US11166485
申请日:2005-06-24
申请人: Christopher Thomas Hamilton , Michael Frederick Gullo , Michael Allen Gonzalez , Gary Alan Roth , David Bruce Gorman , Joachim Gebhardt , Norbert Götz , Hagen Jaedicke , Guido Mayer , Michael Rack
发明人: Christopher Thomas Hamilton , Michael Frederick Gullo , Michael Allen Gonzalez , Gary Alan Roth , David Bruce Gorman , Joachim Gebhardt , Norbert Götz , Hagen Jaedicke , Guido Mayer , Michael Rack
IPC分类号: C07D211/72
CPC分类号: C07D213/64
摘要: 4-Trifluoromethyl-2(1H)-pyridinone is prepared by reaction of 4-alkoxy-1,1,1-trifluorobut-3-en-2-one or 4,4-dialkoxy-1,1,1-trifluorobutan-2-one with a trialkyl phosphonoacetate followed by cyclization.
摘要翻译: 4-三氟甲基-2(1H) - 吡啶酮通过4-烷氧基-1,1,1-三氟丁-3-烯-2-酮或4,4-二烷氧基-1,1,1-三氟丁烷-2 - 与三烷基膦酰基乙酸酯接触,然后环化。
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