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公开(公告)号：US12103857B1
公开(公告)日：2024-10-01
申请号：US18303062
申请日：2023-04-19
Applicant: KUNMING UNIVERSITY OF SCIENCE AND TECHNOLOGY
Inventor： Feng Liang , Junxi Li , Da Zhang , Zhipeng Xie , Wenhui Ma , Bin Yang
IPC: C01B35/04
CPC classification number: C01B35/04
Abstract: A rapid preparation method of transition metal borides includes steps of: using a tungsten rod as the cathode, and a block mixture of boron powder and metal oxide as the anode, the block mixture and the tungsten rod are placed in an plasma device; the plasma device is evacuated, and then filled with a buffer gas and an electric arc is started to obtain a transition metal boride. The present disclosure adopts the direct current arc plasma method with the advantages of simple operation, low cost, environmental friendliness and controllable reaction atmosphere to prepare the transition metal boride, the preparation process is simple, the preparation process is fast, and the environment will not be affected.
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公开(公告)号：US11801552B2
公开(公告)日：2023-10-31
申请号：US17928471
申请日：2022-03-24
Applicant: Kunming University of Science and Technology
Inventor： Baoqiang Xu , Tengteng Shi , Bin Yang , Wenlong Jiang , Yang Tian , Lingxin Kong , Jinyang Zhao , Fei Wang
IPC: B22D43/00
CPC classification number: B22D43/007
Abstract: Disclosed is a device for continuous treatment of materials containing volatile components, which belongs to the field of pyrometallurgical equipment. The device includes a feeding unit, a heating unit, a slag raking unit and a slag collecting unit. The feeding unit is configured to feed the materials with a push rod or in a spiral mode. The heating unit is provided with a square furnace body, and a first slag raking port is provided in the lower part of the furnace body. The slag collecting unit is provided with a slag discharging port at the lower portion thereof, is provided with a slag smashing port at the sidewall thereof, and is provided with a viewing port at the top thereof. The slag collecting unit and the heating unit are connected through a pipeline, thus achieving the pressure balance of the whole device during operation.
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3.发明公开公开(公告)号：US20240328022A1
公开(公告)日：2024-10-03
申请号：US18743648
申请日：2024-06-14
Applicant: Kunming University of Science and Technology
Inventor： Jia Yang , Kanwen Hou , baohong Wei , Jiancheng Qian , Baoqiang Xu , Bin Yang , Dachun Liu , Wenlong Jiang , Yong Deng , Yifu Li , Yang Tian , Heng Xiong , Fei Wang , Qingchun Yu , Hongwei Yang
CPC classification number: C25C7/02 , C25C1/02 , C25C1/10 , C25C1/12 , C25C1/14 , C25C1/16 , C25C1/18 , C25C1/22
Abstract: This invention presents an electrochemical metallurgical technique for extracting metals and sulfur from metal sulfides, offering an adjustable composition and mechanical properties during electrode preparation. The metal sulfide anode, submerged in an electrolyte with a cathode made of materials like titanium, copper, stainless steel, lead, zinc, aluminum or graphite, undergoes electrolysis. This process oxidizes sulfur in the metal sulfide to the anode and releases metal ions into the electrolyte, where they're reduced at the cathode. The method yields metal at the cathode and sulfur at the anode, with minimal environmental impact, low investment, and straightforward process.
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公开(公告)号：US12051776B2
公开(公告)日：2024-07-30
申请号：US18537953
申请日：2023-12-13
Applicant: KUNMING UNIVERSITY OF SCIENCE AND TECHNOLOGY , JIANGSU FENGCHI CARBON BASED NEW MATERIAL RESEARCH INSTITUTE CO., LTD
Inventor： Feng Liang , Minjie Hou , Da Zhang , Tao Zhang , Sunzu Xiang , Wenlong Jiang , Baoqiang Xu , Bin Yang
IPC: H01M10/0562
CPC classification number: H01M10/0562 , H01M2300/0068
Abstract: A method for preparing a sodium super ionic conductor solid electrolyte by low-dimensional crystallization belongs to a field of energy materials. The method is based on the theory of negative ion coordination polyhedron growth unit, and uses low-temperature plasma as a protective gas of a spray drying equipment. While evaporating the solvent in a sodium super ionic conductor solid electrolyte precursor slurry, plasma active groups modify the particle surface of the sodium super ionic conductor solid electrolyte precursor particles in-situ. A free space dimension of crystal growth in the crystallization process is reduced, and directional growth of crystals in the solid phase sintering process is induced. Secondly, the dispersion stability of the sodium super ionic conductor solid electrolyte precursor particles is improved. Compared with the traditional high-temperature solid-state sintering process, the method has the advantages of fast crystallization speed, high crystal purity and integrity, good compactness, and uniform particles.
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公开(公告)号：US11817552B2
公开(公告)日：2023-11-14
申请号：US17993893
申请日：2022-11-24
Applicant: KUNMING UNIVERSITY OF SCIENCE AND TECHNOLOGY , JIANGSU FENGCHI CARBON-BASED NEW MATERIALS RESEARCH INSTITUTE CO., LTD.
Inventor： Feng Liang , Minjie Hou , Da Zhang , Tao Zhang , Sunzu Xiang , Wenlong Jiang , Baoqiang Xu , Bin Yang
IPC: H01M10/0565
CPC classification number: H01M10/0565 , H01M2300/0082
Abstract: The present disclosure discloses a method for plasma modification of sodium super ionic conductor type solid electrolyte, which comprises: dielectric barrier discharge plasma modification of sodium super ionic conductor solid electrolyte particles to obtain activated sodium super ionic conductor solid electrolyte particles; weigh the polymer and the activated sodium super ionic conductor solid electrolyte particles in a predetermined proportion, dissolve the polymer and the activated sodium super ionic conductor solid electrolyte particles in an organic solvent to obtain a mixed solution, then pour the mixed solution into a preset mold, and then dry it to remove the organic solvent and form a composite solid electrolyte film. The composite solid electrolyte film is taken out of the mold and rolled to obtain the composite solid electrolyte film after rolling treatment.
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Patent Agency Ranking
公开(公告)号：US10982299B2
公开(公告)日：2021-04-20
申请号：US16357369
申请日：2019-03-19
Inventor： Bin Yang , Dachun Liu , Wenlong Jiang , Guozheng Zha , Baoqiang Xu , Weiping Dai , Yifu Li , Qingchun Yu , Xiumin Chen , Hongwei Yang , Yang Tian , Yong Deng , Fei Wang , Heng Xiong , Jia Yang , Tao Qu , Lingxin Kong
Abstract: A method for comprehensively processing noble lead provided and utilizes two instances of vacuum distillation to realize an open circuit of arsenic, lead, antimony and bismuth and the high-efficiency enrichment of precious metals of gold and silver, and can obtain elemental arsenic, a lead-bismuth-antimony alloy, a silver alloy and a copper alloy, respectively. The lead-bismuth-antimony alloy, the silver alloy and the copper alloy are processed by oxidation refining, electrorefining and chlorination refining to obtain refined lead, refined antimony, antimony trioxide, electrolytic silver and electrolytic copper, and to realize gold enrichment. The entire process has advantages of high metal direct yield, low energy consumption, short flow chart, simple equipment, etc., and vacuum distillation belongs to a physical process in which the alloy can be separated only by means of the difference in saturated vapor pressure between the metals, without generation of wastewater, waste gas and waste residue.
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公开(公告)号：US20240401169A1
公开(公告)日：2024-12-05
申请号：US18799957
申请日：2024-08-09
Applicant: Kunming University of Science and Technology
Inventor： Yang Tian , Haosong Yu , Bin Yang , Xiumin Chen , Baoqiang Xu , Wenlong Jiang , Yifu Li , Fei Wang , Yong Deng , Lipeng Wang , Dong Liang , Dong Wang
Abstract: The present disclosure relates to a device and method for recovering arsenic and gallium. A closed furnace body is in communication with a vacuuming pipe, and the vacuuming pipe is connected to a vacuuming mechanism. The closed furnace body includes a first furnace body, a second furnace body and a third furnace body. A first heating mechanism and a graphite crucible are arranged inside the first furnace body, the first heating mechanism being used for heating the graphite crucible. A first collection cylinder is in communication with a second collection cylinder. The device for recovering arsenic and gallium of the present disclosure is arranged with a structure for realizing directional condensation of gallium arsenide clusters and arsenic vapor, respectively, to realize high-purity recovery of arsenic and gallium.
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公开(公告)号：US20230089884A1
公开(公告)日：2023-03-23
申请号：US17993893
申请日：2022-11-24
Applicant: KUNMING UNIVERSITY OF SCIENCE AND TECHNOLOGY , JIANGSU FENGCHI CARBON-BASED NEW MATERIALS RESEARCH INSTITUTE CO., LTD.
Inventor： FENG LIANG , Minjie Hou , Da Zhang , Tao Zhang , Sunzu Xiang , Wenlong Jiang , Baoqiang Xu , Bin Yang
IPC: H01M10/0565
Abstract: The present disclosure discloses a method for plasma modification of sodium super ionic conductor type solid electrolyte, which comprises: dielectric barrier discharge plasma modification of sodium super ionic conductor solid electrolyte particles to obtain activated sodium super ionic conductor solid electrolyte particles; weigh the polymer and the activated sodium super ionic conductor solid electrolyte particles in a predetermined proportion, dissolve the polymer and the activated sodium super ionic conductor solid electrolyte particles in an organic solvent to obtain a mixed solution, then pour the mixed solution into a preset mold, and then dry it to remove the organic solvent and form a composite solid electrolyte film. The composite solid electrolyte film is taken out of the mold and rolled to obtain the composite solid electrolyte film after rolling treatment.
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公开(公告)号：US12230799B1
公开(公告)日：2025-02-18
申请号：US18816719
申请日：2024-08-27
Applicant: KUNMING UNIVERSITY OF SCIENCE AND TECHNOLOGY
Inventor： Feng Liang , Pan Liu , Minjie Hou , Da Zhang , Bin Yang
IPC: H01M4/583 , H01M4/02 , H01M4/04 , H01M10/054
Abstract: A method for preparing a carbon nanotube sodiophilic metal anode-free sodium metal battery electrode material is provided, and the method includes the following steps: the carbon nanotubes are modified by a dielectric barrier plasma device; the modified carbon nanotubes are mixed and stirred with a sodiophilic metal salt to obtain a precursor slurry; the precursor slurry is dried, placed in a tube furnace after drying, and heated by introducing a reducing gas to react, thereby obtaining a carbon nanotube sodiophilic metal anode-free sodium metal battery electrode material. The electrode material prepared by the method has a stable structure, excellent electrical conductivity, and excellent sodium affinity, and can be applied to anode-free sodium metal battery electrode materials. The entire preparation process is controllable, the synthesis cycle is short, and the operation is simple.
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10.发明申请公开(公告)号：US20190284658A1
公开(公告)日：2019-09-19
申请号：US16352199
申请日：2019-03-13
Applicant: Kunming University of Science and Technology
Inventor： Yifu Li , Zhenghao Pu , Bin Yang , Baoqiang Xu , Dachun Liu , Yang Tian , Wenlong Jiang , Neng Xiong , Huan Zhang
Abstract: A device is provided for fractional condensation of an arsenic-lead vapor mixture and an application method thereof. The device includes a vacuumizing device, a flange, temperature measuring devices, a graded vacuum furnace body, a quartz tube, a push rod, a control cabinet, a heating zone and recycled foil. The length of the quartz tube is 1.2-2 m; the length of the heating zone is 0.15-0.25 m; and the quartz tube is provided with one temperature measuring device every 2-3 cm. The device forms a certain temperature gradient in the quartz tube, so that a material condenses in the corresponding temperature range, thereby achieving the purpose of high-efficiency separation.
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