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    POLYCYCLIC FUSED RING TYPE PI-CONJUGATED ORGANIC MATERIAL, INTERMEDIATE THEREFOR, PROCESS FOR PRODUCING POLYCYCLIC FUSED RING TYPE PI-CONJUGATED ORGANIC MATERIAL, AND PROCESS FOR PRODUCING INTERMEDIATE OF POLYCYCLIC FUSED RING TYPE PI-CONJUGATED ORGANIC MATERIAL
    1.
    发明申请
    POLYCYCLIC FUSED RING TYPE PI-CONJUGATED ORGANIC MATERIAL, INTERMEDIATE THEREFOR, PROCESS FOR PRODUCING POLYCYCLIC FUSED RING TYPE PI-CONJUGATED ORGANIC MATERIAL, AND PROCESS FOR PRODUCING INTERMEDIATE OF POLYCYCLIC FUSED RING TYPE PI-CONJUGATED ORGANIC MATERIAL 有权
    多环式熔融型PI结合有机材料，其中间体，生产聚合环状结合有机物质的方法，以及生产多环式熔融型PI结合有机材料中间体的方法

    公开(公告)号：US20090143605A1

    公开(公告)日：2009-06-04

    申请号：US10578352

    申请日：2004-11-05

    申请人： Shigehiro Yamaguchi ,  Caihong Xu

    发明人： Shigehiro Yamaguchi ,  Caihong Xu

    IPC分类号： C07F7/08

    CPC分类号： H05B33/14 ,  C07F7/0807 ,  C09K11/06 ,  C09K2211/1096

    摘要： A polycyclic fused ring type π-conjugated organic material (VIIa, VIIb, VIIc, VIId) is obtained in the following manner. That is, as shown in Scheme 1 below, a starting material (I) is dimetalated with an organometallic base. The starting material (I) thus dimetalated is trapped with an organosilicon reagent (i: (1) n-BuLi or t-BuLi; (2) HMe2SiCl). As a result, an intermediate is obtained. Thereafter, the intermediate is allowed to react with a metal reductant. This causes an intramolecular reductive cyclization reaction to proceed. As a result, a dianion intermediate is produced. The dianion intermediate is trapped with an electrophile (ii: (1) LiNaph, THF, rt, 5 min; (2) electrophile or NH4Cl) In this way, the polycyclic fused ring type π-conjugated organic material is obtained. The polycyclic fused ring type π-conjugated organic material, an intermediate therefor, a method for producing the polycyclic fused ring type π-conjugated organic material, and a method for producing the intermediate make it possible to provide a polycyclic fused ring type π-conjugated organic material having excellent light-emitting and charge-transporting properties.

    摘要翻译： 以下列方式获得多环稠环型π-共轭有机材料（VIIa，VIIb，VIIc，VIId）。 也就是说，如下面的方案1所示，起始原料（I）用有机金属碱进行二价金属化。 用二氧化硅原料（I：（1）n-BuLi或t-BuLi;（2）HMe 2 SiCl）捕集由此得到的原料（I）。 结果得到中间体。 然后使中间体与金属还原剂反应。 这导致进行分子内还原环化反应。 结果，产生二价阴离子中间体。 将二价阴离子中间体与亲电子试剂（ii：（1）LiNaph，THF，rt，5分钟;（2）亲电子试剂或NH 4 Cl）捕获。以这种方式，获得多环稠环型π-共轭有机材料。 多环稠环型π-共轭有机材料，其中间体，多环稠环型π-共轭有机材料的制造方法和中间体的制造方法，可以提供多环稠环型π-共轭有机材料 有机材料具有优异的发光和电荷传输性能。

    Polycyclic fused ring type π-conjugated organic material, intermediate therefor, process for producing polycyclic fused ring type π-conjugated organic material, and process for producing intermediate of polycyclic fused ring type π-conjugated organic material
    2.
    发明授权
    Polycyclic fused ring type π-conjugated organic material, intermediate therefor, process for producing polycyclic fused ring type π-conjugated organic material, and process for producing intermediate of polycyclic fused ring type π-conjugated organic material 有权
    多环稠环型共轭有机材料，其中间体，多环稠环型共轭有机材料的制备方法，多环稠环型共轭有机物中间体的制备方法

    公开(公告)号：US07973190B2

    公开(公告)日：2011-07-05

    申请号：US10578352

    申请日：2004-11-05

    申请人： Shigehiro Yamaguchi ,  Caihong Xu

    发明人： Shigehiro Yamaguchi ,  Caihong Xu

    IPC分类号： C07F7/08

    CPC分类号： H05B33/14 ,  C07F7/0807 ,  C09K11/06 ,  C09K2211/1096

    摘要： A polycyclic fused ring type π-conjugated organic material (VIIa, VIIb, VIIc, VIId) is obtained in the following manner. That is, as shown in Scheme 1 below, a starting material (I) is dimetalated with an organometallic base. The starting material (I) thus dimetalated is trapped with an organosilicon reagent (i: (1) n-BuLi or t-BuLi; (2) HMe2SiCl). As a result, an intermediate is obtained. Thereafter, the intermediate is allowed to react with a metal reductant. This causes an intramolecular reductive cyclization reaction to proceed. As a result, a dianion intermediate is produced. The dianion intermediate is trapped with an electrophile (ii: (1) LiNaph, THF, rt, 5 min; (2) electrophile or NH4Cl) In this way, the polycyclic fused ring type π-conjugated organic material is obtained. The polycyclic fused ring type π-conjugated organic material, an intermediate therefor, a method for producing the polycyclic fused ring type π-conjugated organic material, and a method for producing the intermediate make it possible to provide a polycyclic fused ring type π-conjugated organic material having excellent light-emitting and charge-transporting properties.

    摘要翻译： 以下列方式获得多环稠环型共轭有机材料（VIIa，VIIb，VIIc，VIId）。 也就是说，如下面的方案1所示，起始原料（I）用有机金属碱进行二价金属化。 用二氧化硅原料（I：（1）n-BuLi或t-BuLi;（2）HMe 2 SiCl）捕集由此得到的原料（I）。 结果得到中间体。 然后使中间体与金属还原剂反应。 这导致进行分子内还原环化反应。 结果，产生二价阴离子中间体。 将二价阴离子中间体用亲电子试剂（ii：（1）LiNaph，THF，rt，5分钟;（2）亲电子试剂或NH 4 Cl）捕获。以这种方式，获得多环稠环型共轭有机材料。 多环稠环型共轭有机材料，其中间体，多环稠环型共轭有机材料的制造方法以及中间体的制造方法可以提供多环稠环型＆pgr 具有优异的发光和电荷传输性能的共轭有机材料。

    Condensed polycyclic π-conjugated organic material, intermediate product therefor, and method of manufacturing condensed polycyclic π-conjugated organic material
    3.
    发明授权
    Condensed polycyclic π-conjugated organic material, intermediate product therefor, and method of manufacturing condensed polycyclic π-conjugated organic material 有权
    稠合多环和共轭有机材料，其中间产物和制备缩合多环和共轭有机材料的方法

    公开(公告)号：US07705174B2

    公开(公告)日：2010-04-27

    申请号：US10525221

    申请日：2003-08-20

    申请人： Shigehiro Yamaguchi ,  Caihong Xu ,  Kohei Tamao

    发明人： Shigehiro Yamaguchi ,  Caihong Xu ,  Kohei Tamao

    IPC分类号： C07F7/08

    CPC分类号： C07F7/0807 ,  C07F7/0812 ,  C08G61/123 ,  C08G77/60

    摘要： The invention provides condensed polycyclic π-conjugated organic materials and manufacturing methods for the materials. A metal reducing agent is reacted with a straight-chain, triple bond-containing hydrocarbon (aryl acetylene compound, phenyl acetylene compound), the hydrocarbon being a benzene ring with an organic silicon as a substituent, so as to allow an intramolecular reductive cyclization reaction to proceed between the silicon and the triple-bond carbon. The reaction produces condensed polycyclic π-conjugated organic materials of the invention. The invention provides light-emitting materials applicable for organic electroluminescent devices, condensed polycyclic π-conjugated organic materials applicable for charge transport materials, their intermediate products, and a manufacture method for condensed polycyclic π-conjugated organic materials.

    摘要翻译： 本发明提供了缩合多环和共轭有机材料及其制备方法。 使金属还原剂与直链，含三键的烃（芳基乙炔化合物，苯基乙炔化合物）反应，该烃为具有有机硅作为取代基的苯环，以使分子内还原环化反应 在硅和三键碳之间进行。 该反应产生本发明的缩合多环和共轭有机材料。 本发明提供适用于有机电致发光器件，适用于电荷传输材料的冷凝多环和共轭有机材料及其中间产物以及冷凝多环和共轭有机材料的制造方法的发光材料。

    n-conjugated organic material of polycyclic fused ring type,intermediate therefor, and process for producing n-conjugated organic material of polycyclic fused ring type
    4.
    发明申请
    n-conjugated organic material of polycyclic fused ring type,intermediate therefor, and process for producing n-conjugated organic material of polycyclic fused ring type 有权
    多环稠环型的正共轭有机材料，其中间体，以及多环稠环类的共轭有机材料的制造方法

    公开(公告)号：US20060100433A1

    公开(公告)日：2006-05-11

    申请号：US10525221

    申请日：2003-08-20

    申请人： Shigehiro Yamaguchi ,  Caihong Xu ,  Kohei Tamao

    发明人： Shigehiro Yamaguchi ,  Caihong Xu ,  Kohei Tamao

    IPC分类号： C07F7/02 ,  C07F9/02

    CPC分类号： C07F7/0807 ,  C07F7/0812 ,  C08G61/123 ,  C08G77/60

    摘要： The invention provides condensed polycyclic π-conjugated organic materials and manufacturing methods for the materials. A metal reducing agent is reacted with a straight-chain, triple bond-containing hydrocarbon (aryl acetylene compound, phenyl acetylene compound), the hydrocarbon being a benzene ring with an organic silicon as a substituent, so as to allow an intramolecular reductive cyclization reaction to proceed between the silicon and the triple-bond carbon. The reaction produces condensed polycyclic π-conjugated organic materials of the invention. The invention provides light-emitting materials applicable for organic electroluminescent devices, condensed polycyclic π-conjugated organic materials applicable for charge transport materials, their intermediate products, and a manufacture method for condensed polycyclic π-conjugated organic materials.

    摘要翻译： 本发明提供稠合多环式π共轭有机材料及其制备方法。 使金属还原剂与直链，含三键的烃（芳基乙炔化合物，苯基乙炔化合物）反应，该烃为具有有机硅作为取代基的苯环，以使分子内还原环化反应 在硅和三键碳之间进行。 该反应产生本发明的稠合多环π-共轭有机材料。 本发明提供适用于有机电致发光元件的发光材料，适用于电荷输送材料的缩合多环π共轭有机材料及其中间产物，以及冷凝多环π共轭有机材料的制造方法。