摘要:
A cryogenic rectification system for producing lower purity oxygen comprising a double column with a third column reboiled by feed air at an intermediate level and, optionally, in a staged manner at the bottom level.
摘要:
A unit capable of simultaneously producing nitrogen of ultra high purity and liquid oxygen of ultra high purity, is provided. The inside of the first rectification column 6 is demarcated to an upper rectifying part 12, and upper-stage middle rectifying part 13, a lower-stage middle rectifying part 14 and a lower rectifying part 15. To the upper part 11 above the upper rectifying part 12 is connected a nitrogen condenser 8. A second rectification column 7 is demarcated to an upper rectifying part 22 and a lower rectifying part 23, and has a reboiler 25 provided under its lower rectifying part 22. Ultra high purity liquid nitrogen is recovered from between the upper rectifying part 12 and upper-stage middle rectifying part 13 of the first rectification column 6, and ultra high purity liquid oxygen is recovered from below the lower rectifying part 23 of the second rectification column 7.
摘要:
A cryogenic rectification system wherein additional stripping vapor for the lower pressure column of a double column is produced from higher pressure column bottoms and feed for the argon column is taken from the upper portion of the lower pressure column and first processed through a stripping column. Lower purity oxygen is recovered either directly from the lower pressure column or after first being processed in an auxiliary column which additionally produces higher purity oxygen.
摘要:
A double column cryogenic rectification system for producing low purity oxygen and high purity nitrogen, preferably at elevated pressure, wherein nitrogen-rich vapor from the higher pressure column is turboexpanded and condensed against lower pressure column intermediate liquid prior to being passed into the lower pressure column.
摘要:
A cryogenic rectification system employing a double column and an auxiliary side column in which product lower purity oxygen is produced wherein the side column is driven by condensing compressed feed air enabling the system to operate with lower head pressure and thus lower operating costs.
摘要:
A generator produces ultra-high purity nitrogen and ultra-high purity oxygen simultaneously by the liquefaction and rectification of feed air. Feed air is rectified in a first rectification column, and nitrogen gas separated to the top of that column is liquefied, in a nitrogen condenser, by oxygen-enriched liquid air separated to the bottom portion of the first rectification column. The oxygen-enriched liquid is fed to the upper portion of a second rectification column having a reboiler at its bottom, so that through rectification oxygen gas is fed from above a liquid reservoir to the lower portion of a third rectification column. Through rectification of the oxygen gas in the third rectification column, high purity oxygen gas, from which impurities having boiling points higher than that of oxygen have been removed by liquefaction, is fed to the center portion of a fourth rectification column which has a condenser in its top portion and a reboiler in its bottom portion. Through rectification of the high purity oxygen gas in the fourth rectification column, impurities having boiling points lower than that of oxygen are exhausted from the top portion thereof as non-condensed gas and ultra-high purity liquid oxygen is separated to the bottom thereof.
摘要:
A process is set forth for producing a krypton/xenon enriched stream from a cryogenic nitrogen generator. Distillation of the oxygen product stream at the top of the low pressure column is suggested in order to concentrate krypton and xenon while rejecting the majority of methane in the oxygen product stream.
摘要:
Air separation, in particular apparatus and method for reducing the loss of krypton and xenon during air separation by cryogenic distillation. The invention provides a method of separating air by cryogenic distillation, including forming a first liquid oxygen stream, and a second liquid oxygen stream having a lower concentration of krypton and xenon than said first stream, withdrawing the second stream as product, and subjecting the first stream to further separation to enrich it in krypton and xenon.
摘要:
A process which produces a krypton-xenon concentrate from a liquid feed while also producing a liquid product substantially free of rare gases. The process employs an integral heat pump circuit to carry out the separation in an energy-efficient manner.
摘要:
A process for producing krypton and xenon. The concentrations of krypton and xenon contained in liquid oxygen are not highly increased in a concentrating column to produce concentrated liquid having a relatively low concentration of methane, which is stripped of methane by contact with oxygen gas in a methane purging column to reduce the methane concentration and the methane-purged liquid is then concentrated at the lower part of the purging column. Then, the concentrated liquid is vaporized and purified by catalitic combustion and adsorption, and thereafter a mixture of krypton and xenon is separated from the purified gas in a second concentrating column.