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公开(公告)号:US07622233B2
公开(公告)日:2009-11-24
申请号:US11464367
申请日:2006-08-14
CPC分类号: G03G9/0806 , G03G9/0804 , G03G9/08711 , G03G9/08726 , G03G9/08728 , G03G9/08733 , G03G9/08755 , G03G9/08782 , G03G9/08795
摘要: A toner composition includes a styrene-based polymer resin, a crystalline polyester wax, a second wax different from the crystalline polyester wax, a colorant, and a coagulant.
摘要翻译: 调色剂组合物包括苯乙烯基聚合物树脂,结晶聚酯蜡,不同于结晶聚酯蜡的第二蜡,着色剂和凝结剂。
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公开(公告)号:US07615328B2
公开(公告)日:2009-11-10
申请号:US12140738
申请日:2008-06-17
申请人: Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allen K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人: Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allen K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号: G03G5/00
CPC分类号: G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要: A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译: 一种用于制备调色剂颗粒和组合物的方法,所述调色剂颗粒和组合物适用于制备调色剂,所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。 该方法包括形成包含支链聚酯树脂,结晶聚酯树脂,着色剂和任选的蜡的乳液树脂。 树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。 然后将聚集体混合物在高于乳液树脂的Tg约5至约20℃的温度下聚结,以产生所得到的调色剂颗粒。
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公开(公告)号:US07413842B2
公开(公告)日:2008-08-19
申请号:US11208907
申请日:2005-08-22
申请人: Daryl Vanbesien , David J. Sanders , Raj D. Patel , Christine D. Anderson , Patricia Ann Burns , Nam-Suk Ro
发明人: Daryl Vanbesien , David J. Sanders , Raj D. Patel , Christine D. Anderson , Patricia Ann Burns , Nam-Suk Ro
IPC分类号: G03G9/08
CPC分类号: G03G9/0804
摘要: A toner process comprising aggregating or coagulating a latex emulsion comprising a resin, a colorant and wax particles using an amount of polymetal ion coagulant to provide core particles; heating the core particles to provide micron size aggregates; optionally adding a second resin emulsion; adding a sequestering or complexing component and a base to remove the polymetal ion in a controlled manner; further heating the mixture to provide toner particles; and optionally, isolating the toner particles.
摘要翻译: 一种调色剂方法,其包括使用一定量的多金属离子凝结剂聚集或凝结包含树脂,着色剂和蜡颗粒的胶乳乳液,以提供核心颗粒; 加热核心颗粒以提供微米级聚集体; 任选地加入第二树脂乳液; 加入螯合或络合组分和碱,以受控方式除去多金属离子; 进一步加热混合物以提供调色剂颗粒; 并且可选地,分离调色剂颗粒。
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公开(公告)号:US07410750B2
公开(公告)日:2008-08-12
申请号:US10881682
申请日:2004-06-30
申请人: Naveen Chopra , Daniel A. Foucher , Raj D. Patel
发明人: Naveen Chopra , Daniel A. Foucher , Raj D. Patel
IPC分类号: G03C1/00
CPC分类号: C09K9/02 , C09K2211/1011 , C09K2211/1029 , C09K2211/1088 , C09K2211/1092 , G02F1/15 , G03G9/0906 , G03G9/0916
摘要: A multicolored display and process for forming such a display is provided. The multicolored display includes marking particles comprising a mixture of photochromic materials. The photochromic materials each exhibit a first “invisible” photochromic state at a first absorption spectrum and at least a second “visible” photochromic state at a second absorption spectrum. The second “visible” photochromic state of each photochromic material produces a different color relative to the other photochromic materials. In embodiments, the marking particles include a mixture of a spiropyran material and a dithienylethene material.
摘要翻译: 提供了用于形成这种显示器的多彩显示和处理。 多色显示器包括包含光致变色材料的混合物的标记颗粒。 光致变色材料在第一吸收光谱和第二吸收光谱下呈现出至少第二“可见”光致变色状态的第一“不可见”光致变色状态。 每种光致变色材料的第二种“可视”光致变色状态相对于其它光致变色材料产生不同的颜色。 在实施方案中,标记颗粒包括螺吡喃材料和二噻吩乙烯材料的混合物。
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公开(公告)号:US07402371B2
公开(公告)日:2008-07-22
申请号:US10948450
申请日:2004-09-23
申请人: Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人: Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号: G03G9/087
CPC分类号: G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要: A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译: 一种用于制备调色剂颗粒和组合物的方法,所述调色剂颗粒和组合物适用于制备调色剂,所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。 该方法包括形成包含支链聚酯树脂,结晶聚酯树脂,着色剂和任选的蜡的乳液树脂。 树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。 然后将聚集体混合物在乳液树脂T T上方约5至约20℃的温度下聚结,以产生所得调色剂颗粒。
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公开(公告)号:US07214463B2
公开(公告)日:2007-05-08
申请号:US11044456
申请日:2005-01-27
申请人: Raj D. Patel , Karen A. Moffat , Fatima M. Mayer , Allan K. Chen
发明人: Raj D. Patel , Karen A. Moffat , Fatima M. Mayer , Allan K. Chen
IPC分类号: G03G9/087
CPC分类号: G03G9/0806 , G03G9/0804 , G03G9/0833 , G03G9/0837 , G03G9/08704 , G03G9/08708 , G03G9/08711 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要: A toner process comprised of a first heating of a mixture of an acicular magnetite dispersion, a colorant dispersion, a wax dispersion, and a core latex comprised of a first latex containing a vinyl crystalline polyester resin substantially free of crosslinking, and wherein said polyester is substantially dissolved in a vinyl monomer and polymerized to provide said first core latex resin, and which mixture contains a second crosslinked resin containing latex wherein said heating is accomplished in the presence of a coagulant to provide aggregates; adding a shell latex comprised of a polymer substantially free of crosslinking, and further heating said aggregates to provide coalesced toner particles, and wherein said further heating is at a higher temperature than said first heating.
摘要翻译: 一种调色剂方法,其包括:针状磁铁矿分散体,着色剂分散体,蜡分散体和由含有基本上不交联的乙烯基结晶聚酯树脂的第一胶乳组成的芯胶乳的第一次加热,其中所述聚酯为 基本上溶解在乙烯基单体中并聚合以提供所述第一芯胶乳树脂,并且该混合物包含含有胶乳的第二交联树脂,其中所述加热在凝结剂存在下完成以提供聚集体; 添加由基本上不交联的聚合物组成的壳胶乳,并且进一步加热所述聚集体以提供聚结的调色剂颗粒,并且其中所述另外的加热处于比所述第一加热更高的温度。
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公开(公告)号:US06365312B1
公开(公告)日:2002-04-02
申请号:US09864475
申请日:2001-05-24
申请人: Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier , James Wojtyk , Erwin Buncel
发明人: Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier , James Wojtyk , Erwin Buncel
IPC分类号: G03G909
CPC分类号: G03G9/0906 , G03G9/0912 , G03G9/0914
摘要: Disclosed are marking particles comprising a first polymer, a second polymer, a chelating agent, and a spiropyran material of the formula wherein n is an integer representing the number of repeat —CH2— units and R is —H or —CH═CH2. The marking particles comprise a core containing the first polymer in which is dispersed the chelating agent and the spiropyran and encapsulated within a shell of the second polymer formulated by an interfacial polymerization.
摘要翻译: 公开了包含第一聚合物,第二聚合物,螯合剂和糠醛的螺吡喃材料的标记颗粒,n是表示重复-CH 2 - 单元的数目的整数,R是-H或-CH = CH 2。 标记颗粒包含含有第一聚合物的核心,其中分散有螯合剂和螺吡喃并包封在通过界面聚合配制的第二聚合物的壳体内。
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公开(公告)号:US5852140A
公开(公告)日:1998-12-22
申请号:US37192
申请日:1993-03-25
申请人: Michael K. Georges , Raj D. Patel
发明人: Michael K. Georges , Raj D. Patel
摘要: Disclosed is a process for the preparation of a polymer which comprises effecting bulk polymerization of a mixture of at least one monomer, a free radical polymerization initiator, and a stable free radical agent until from about 10 to about 50 weight percent of the monomer has been polymerized; optionally adding additional free radical initiator; optionally adding a colorant; dispersing with a high shear mixer the aforementioned partially polymerized mixture in water containing a stabilizing component selected from the group consisting of non-ionic and ionic water soluble polymeric stabilizers to obtain a suspension of particles with an average diameter of from about 0.1 to about 10 microns; polymerizing the resulting suspension to form said polymer.
摘要翻译: 公开了一种制备聚合物的方法,其包括进行至少一种单体,自由基聚合引发剂和稳定自由基试剂的混合物的本体聚合,直到约10至约50重量%的单体已经 聚合的 任选地加入另外的自由基引发剂; 任选地加入着色剂; 用高剪切混合器将上述部分聚合的混合物在含有选自非离子和离子水溶性聚合物稳定剂的稳定组分的水中分散,以获得平均直径为约0.1至约10微米的颗粒悬浮液 ; 聚合所得悬浮液以形成所述聚合物。
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公开(公告)号:US5688626A
公开(公告)日:1997-11-18
申请号:US628062
申请日:1996-04-08
CPC分类号: G03G9/09733 , G03G9/0804 , G03G9/0815
摘要: A process for the preparation of a combination of color toners comprised of a cyan toner, a magenta toner, a yellow toner, and a black toner, each of said toners being comprised of resin and pigment, and wherein the pigment is cyan, magenta, yellow and black, each of the said pigments are dispersed in a nonionic, or neutral charge surfactant, and wherein each toner in the combination is prepared by (i) preparing a pigment dispersion, which dispersion is comprised of a pigment and nonionic water soluble surfactant; (ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant; (iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates; and (iv) heating said bound toner size aggregates above about the Tg of the resin.
摘要翻译: 一种用于制备由青色调色剂,品红色调色剂,黄色调色剂和黑色调色剂组成的彩色调色剂的组合的方法,每种所述调色剂由树脂和颜料组成,并且其中所述颜料是青色,品红色, 黄色和黑色,每种所述颜料分散在非离子或中性电荷表面活性剂中,并且其中组合中的每种调色剂通过以下制备:(i)制备颜料分散体,该分散体由颜料和非离子水溶性表面活性剂 ; (ii)用由树脂,具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂的胶乳或乳液共混物剪切所述颜料分散体; (iii)将上述剪切混合物加热至低于树脂的玻璃化转变温度(Tg)以形成静电结合的调色剂尺寸聚集体; 和(iv)将所述结合的调色剂尺寸聚集体加热到高于树脂的Tg的高度。
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公开(公告)号:US5658704A
公开(公告)日:1997-08-19
申请号:US663414
申请日:1996-06-17
CPC分类号: G03G9/08755 , G03G9/0804 , G03G9/0812 , Y10S430/105
摘要: A process for the preparation of toner comprised ofi) flushing pigment into a sulfonated polyester resin, and which resin has a degree of sulfonation of from between about 0.5 and about 2.5 mol percent based on the repeat unit of the polymer;ii) dispersing the resulting pigmented sulfonated polyester resin in warm water, which water is at a temperature of from about 40.degree. to about 95.degree. C., and which dispersing is accomplished by a high speed shearing polytron device operating at speeds of from about 100 to about 5,000 revolutions per minute thereby enabling the formation of toner sized particles, and which particles are of a volume average diameter of from about 3 to about 10 microns with a narrow GSD;iii) recovering said toner by filtration;iv) drying said toner by vacuum; andv) optionally adding to said dry toner charge additives and flow aids.
摘要翻译: 一种制备调色剂的方法,其包括:i)将颜料冲洗成磺化聚酯树脂,并且所述树脂的磺化度基于聚合物的重复单元为约0.5至约2.5摩尔%; ii)将得到的着色的磺化聚酯树脂分散在温度为约40℃至约95℃的温水中,并且该分散是通过以约100的速度操作的高速剪切聚酯装置来实现的 至约5,000转/分钟,从而能够形成调色剂尺寸的颗粒,并且哪些颗粒具有约3至约10微米的体积平均直径,具有窄GSD; iii)通过过滤回收所述调色剂; iv)通过真空干燥所述调色剂; 和v)任选地添加到所述干燥调色剂电荷添加剂和流动助剂中。
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