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    Gamut toner aggregation processes
    1.
    发明授权
    Gamut toner aggregation processes 失效
    色域调色剂聚集过程

    公开(公告)号：US5688626A

    公开(公告)日：1997-11-18

    申请号：US628062

    申请日：1996-04-08

    申请人： Raj D. Patel ,  Grazyna E. Kmiecik-Lawrynowicz ,  Richard P. N. Veregin ,  Maria N. V. McDougall

    发明人： Raj D. Patel ,  Grazyna E. Kmiecik-Lawrynowicz ,  Richard P. N. Veregin ,  Maria N. V. McDougall

    IPC分类号： G03G9/08 ,  G03G9/097 ,  G03G9/09

    CPC分类号： G03G9/09733 ,  G03G9/0804 ,  G03G9/0815

    摘要： A process for the preparation of a combination of color toners comprised of a cyan toner, a magenta toner, a yellow toner, and a black toner, each of said toners being comprised of resin and pigment, and wherein the pigment is cyan, magenta, yellow and black, each of the said pigments are dispersed in a nonionic, or neutral charge surfactant, and wherein each toner in the combination is prepared by (i) preparing a pigment dispersion, which dispersion is comprised of a pigment and nonionic water soluble surfactant; (ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant; (iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates; and (iv) heating said bound toner size aggregates above about the Tg of the resin.

    摘要翻译： 一种用于制备由青色调色剂，品红色调色剂，黄色调色剂和黑色调色剂组成的彩色调色剂的组合的方法，每种所述调色剂由树脂和颜料组成，并且其中所述颜料是青色，品红色， 黄色和黑色，每种所述颜料分散在非离子或中性电荷表面活性剂中，并且其中组合中的每种调色剂通过以下制备：（i）制备颜料分散体，该分散体由颜料和非离子水溶性表面活性剂 ; （ii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂的胶乳或乳液共混物剪切所述颜料分散体; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg）以形成静电结合的调色剂尺寸聚集体; 和（iv）将所述结合的调色剂尺寸聚集体加热到高于树脂的Tg的高度。

    Toner processes
    2.
    发明授权
    Toner processes 失效
    墨粉处理

    公开(公告)号：US5650256A

    公开(公告)日：1997-07-22

    申请号：US720646

    申请日：1996-10-02

    申请人： Richard P. N. Veregin ,  Maria N. V. McDougall ,  Francisco E. Torres ,  Raj D. Patel ,  Grazyna E. Kmiecik-Lawrynowicz ,  T. Hwee Ng ,  Arthur Helbrecht

    发明人： Richard P. N. Veregin ,  Maria N. V. McDougall ,  Francisco E. Torres ,  Raj D. Patel ,  Grazyna E. Kmiecik-Lawrynowicz ,  T. Hwee Ng ,  Arthur Helbrecht

    IPC分类号： G03G9/08 ,  G03G9/087

    CPC分类号： G03G9/0804 ,  G03G9/0815

    摘要： A process for the preparation of toner comprising:(i) preparing a pigment dispersion, which dispersion is comprised of a pigment, and an ionic surfactant;(ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant, and wherein said resin contains an acid functionality;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates;(iv) adding anionic surfactant to stabilize the aggregates obtained in (iii);(v) coalescing said aggregates by heating said bound aggregates above about the Tg of the resin;(vi) reacting said resin of (v) with acid functionality with a base to form an acrylic acid salt, and which salt is ion exchanged in water with a base or a salt, optionally in the presence of metal oxide particles, to control the toner triboelectrical charge, which toner is comprised of resin and pigment; and(vii) optionally drying the toner obtained.

    摘要翻译： 一种制备调色剂的方法，包括：（i）制备颜料分散体，该分散体由颜料和离子表面活性剂组成; （ii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂组成的胶乳或乳液共混物剪切所述颜料分散体，并且其中所述树脂含有酸官能团; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg）以形成静电结合的调色剂尺寸聚集体; （iv）加入阴离子表面活性剂以稳定（iii）中获得的聚集体; （v）通过将所述结合的聚集体加热到约树脂的Tg附近来聚结所述聚集体; （vi）将所述（ⅴ）的酸性官能团的树脂与碱反应形成丙烯酸盐，并且任选地在金属氧化物颗粒存在下，盐与碱或盐在水中进行离子交换，以控制 调色剂摩擦电荷，调色剂由树脂和颜料组成; 和（vii）任选地干燥获得的调色剂。

    Aggregation processes
    3.
    发明授权
    Aggregation processes 失效
    汇总流程

    公开(公告)号：US5744520A

    公开(公告)日：1998-04-28

    申请号：US684955

    申请日：1996-07-19

    申请人： Grazyna E. Kmiecik-Lawrynowicz ,  Richard P. N. Veregin ,  Raj D. Patel ,  Michael A. Hopper ,  Maria V. McDougall

    发明人： Grazyna E. Kmiecik-Lawrynowicz ,  Richard P. N. Veregin ,  Raj D. Patel ,  Michael A. Hopper ,  Maria V. McDougall

    IPC分类号： C08J3/215 ,  G03G9/113 ,  C08K9/08 ,  C08K3/22 ,  C08K5/41 ,  C08L1/26

    CPC分类号： C08J3/215 ,  G03G9/1131 ,  G03G9/1133 ,  G03G9/1138 ,  G03G9/1139

    摘要： A process for the preparation of polymer compositions which comprises mixing a conductive component with an anionic polymeric latex containing a polymer; adding a cationic surfactant, or flocculant whereby the aggregation of the latex particles and the conductive component particles results; subsequently adding colloidal stabilizer, followed by the addition of a base to obtain a pH of from about 7 to about 12; heating above about the polymer glass transition temperature thereby enabling the severage, or breakage of the formed aggregated particles; further heating above about the polymer glass transition temperature enabling the coalescence of the polymer and conductive component particles; and optionally washing and drying the resulting coalesced product.

    摘要翻译： 一种制备聚合物组合物的方法，其包括将导电组分与含有聚合物的阴离子聚合物胶乳混合; 加入阳离子表面活性剂或絮凝剂，由此导致胶乳颗粒和导电组分颗粒的聚集; 随后加入胶体稳定剂，然后加入碱以获得约7至约12的pH; 加热高于聚合物玻璃化转变温度，从而能够形成聚集的颗粒的覆盖或破裂; 进一步加热高于聚合物玻璃化转变温度，使聚合物和导电组分颗粒聚结; 并任选地洗涤和干燥所得的聚结产物。

    Coated carriers by aggregation processes
    4.
    发明授权
    Coated carriers by aggregation processes 失效
    通过聚合过程的涂层载体

    公开(公告)号：US5565296A

    公开(公告)日：1996-10-15

    申请号：US497737

    申请日：1995-07-03

    申请人： Grazyna E. Kmiecik-Lawrynowicz ,  Richard P. N. Veregin ,  Raj D. Patel ,  Michael A. Hopper ,  Maria V. McDougall

    发明人： Grazyna E. Kmiecik-Lawrynowicz ,  Richard P. N. Veregin ,  Raj D. Patel ,  Michael A. Hopper ,  Maria V. McDougall

    IPC分类号： C08J3/215 ,  G03G9/113

    CPC分类号： C08J3/215 ,  G03G9/1131 ,  G03G9/1133 ,  G03G9/1138 ,  G03G9/1139

    摘要： A process for the preparation of polymer compositions which comprises mixing a conductive component with an anionic polymeric latex containing a polymer; adding a cationic surfactant, or flocculant whereby the aggregation of the latex particles and the conductive component particles results; subsequently adding colloidal stabilizer, followed by the addition of a base to obtain a pH of from about 7 to about 12; heating above about the polymer glass transition temperature thereby enabling the severage, or breakage of the formed aggregated particles; further heating above about the polymer glass transition temperature enabling the coalescence of the polymer and conductive component particles; and optionally washing and drying the resulting coalesced product.

    摘要翻译： 一种制备聚合物组合物的方法，其包括将导电组分与含有聚合物的阴离子聚合物胶乳混合; 加入阳离子表面活性剂或絮凝剂，由此导致胶乳颗粒和导电组分颗粒的聚集; 随后加入胶体稳定剂，然后加入碱以获得约7至约12的pH; 加热高于聚合物玻璃化转变温度，从而能够形成聚集的颗粒的覆盖或破裂; 进一步加热高于聚合物玻璃化转变温度，使聚合物和导电组分颗粒聚结; 并任选地洗涤和干燥所得的聚结产物。

    Toner processes
    6.
    发明授权
    Toner processes 失效
    墨粉处理

    公开(公告)号：US5723252A

    公开(公告)日：1998-03-03

    申请号：US707037

    申请日：1996-09-03

    申请人： Raj D. Patel ,  Grazyna E. Kmiecik-Lawrynowicz ,  Anthony J. Paine ,  T. Hwee Ng

    发明人： Raj D. Patel ,  Grazyna E. Kmiecik-Lawrynowicz ,  Anthony J. Paine ,  T. Hwee Ng

    IPC分类号： G03G9/087 ,  G03G9/08

    CPC分类号： G03G9/0804 ,  Y10S977/788

    摘要： A process for the preparation of toner which comprises (i) preparing a pigment dispersion comprised of a pigment dispersed in an ionic surfactant; (ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin particles and a counterionic surfactant; (iii) heating the above sheared blend below the glass transition temperature (Tg) of said resin particles to form electrostatically bound toner size aggregates; (iv) adding a stabilizer of in situ tricalcium phosphate solid particulants generated from a solution of calcium chloride and trisodium phosphate; (v) heating the mixture of (iii) and (iv) above about the Tg of the resin particles to obtain toner size particles comprised of resin and pigment; (vi) washing with an acid to dissolve the trisodium phosphate; and (vii) optionally washing with water, and optionally drying the toner obtained.

    摘要翻译： 一种制备调色剂的方法，其包括（i）制备由分散在离子表面活性剂中的颜料组成的颜料分散体; （ii）用由树脂颗粒和抗衡离子表面活性剂组成的胶乳或乳液共混物剪切所述颜料分散体; （iii）将上述剪切混合物加热到所述树脂颗粒的玻璃化转变温度（Tg）以下以形成静电结合的调色剂尺寸聚集体; （iv）加入由氯化钙和磷酸三钠生成的原位磷酸三钙固体颗粒的稳定剂; （v）加热上述（iii）和（iv）的混合物约树脂颗粒的Tg，得到由树脂和颜料组成的调色剂尺寸颗粒; （vi）用酸洗涤以溶解磷酸三钠; 和（vii）任选地用水洗涤，并任选地干燥获得的调色剂。

    Toner compositions and processes thereof
    7.
    发明授权
    Toner compositions and processes thereof 失效
    调色剂组合物及其工艺

    公开(公告)号：US5604076A

    公开(公告)日：1997-02-18

    申请号：US595143

    申请日：1996-02-01

    申请人： Raj D. Patel ,  Guerino G. Sacripante ,  Grazyna E. Kmiecik-Lawrynowicz ,  Michael A. Hopper ,  Francisco E. Torres

    发明人： Raj D. Patel ,  Guerino G. Sacripante ,  Grazyna E. Kmiecik-Lawrynowicz ,  Michael A. Hopper ,  Francisco E. Torres

    IPC分类号： G03G9/08 ,  G03G9/087 ,  G03G9/097

    CPC分类号： G03G9/0806

    摘要： A process for the preparation of toner compositions comprising:(i) preparing a latex or emulsion resin comprised of a polyester core encapsulated within a styrene based resin shell by heating said polyester emulsion containing an anionic surfactant with a mixture of monomers of styrene and acrylic acid, and with potassium persulfate, ammonium persulfate, sodium bisulfite, or mixtures thereof;(ii) adding a pigment dispersion, which dispersion is comprised of a pigment, a cationic surfactant, and optionally a charge control agent, followed by the sharing of the resulting blend;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution; and(iv) heating said electrostatically bound aggregates above about the Tg of the resin.

    摘要翻译： 一种制备调色剂组合物的方法，包括：（i）通过将含有阴离子表面活性剂的聚酯乳液与苯乙烯和丙烯酸的单体混合物加热，制备由包封在苯乙烯基树脂壳内的聚酯芯构成的胶乳或乳液树脂 和过硫酸钾，过硫酸铵，亚硫酸氢钠或其混合物; （ii）添加颜料分散体，该分散体由颜料，阳离子表面活性剂和任选的电荷控制剂组成，然后共享所得共混物; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; 和（iv）将所述静电结合的聚集体加热到高于树脂的Tg的高度。