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818 条记录 (耗时 0.021 秒)

    Method of preparing tricyclo-hexylidene peroxide
    121.
    发明授权
    Method of preparing tricyclo-hexylidene peroxide 失效
    制备三羟甲基过氧化物的方法

    公开(公告)号：US3781303A

    公开(公告)日：1973-12-25

    申请号：US3781303D

    申请日：1970-06-29

    申请人： STORY CHEM CORP

    发明人： STORY P ,  BUSCH P

    IPC分类号： C07C409/22 ,  C07D315/00 ,  C07D323/00 ,  C07D323/04 ,  C07D19/00

    CPC分类号： C07D315/00 ,  C07D323/00 ,  C07D323/04

    摘要： A METHOD FOR THE PREPARATION OF MIXED TRICYCLOHEXYLIDENE PEROXIDE AND DICYCLOHEXYLIDENE PEROXIDE OR DICYCLOHEXYLIDENE PEROXIDE ALONE COMPRISING R EACTING A PEROXIDE SELECTED FROM THE GROUP CONSISTING OF 1-HYDROPEROXY 1''-HYDROXYDICYCLOHEXYL PEROXIDE AND 1,1''-DIHYDROPEROXYDICYCLOHEXYL PEROXIDE WITH AN ORGANIC SOLVENT AND A STRONG ACID CATALYST. ANOTHER METHOD IS DISCLOSED FOR THE PREPARATION OF TRICYCLOHEXYLIDENE PEROXIDE AND DICYCLOHEXYLIDENE PEROXIDE OR TRICYCLOHEXYLIDENE ALONE COMPRISING REACTING A PEROXIDE SELECTED FROM THE GROUP CONSISTING OF 1-HYDROPEROXY 1''-HYDROXYDICYCLOHEXYL PEROXIDE AND 1,1''-DIHYDROPEROXYDICYCLOHEXYL PEROXIDE WITH A LIQUID CARBOXYLIC ACID AND STRONG ACID CATALYST. ALSO DISCLOSED ARE NEW AND USEFUL IMPROVEMENTS IN THE METHOD FOR THE PREPARATION OF 1-HYDROPEROXY-1''-HYDROXYDICYCLOHEXYL PEREOXIDE COMPRISING REACTING C YCLOHEXANONE WITH AQUEOUS HYDROGEN PEROXIDE AND A STRONG ACID-CATALYST.

    Photochemical process for preparing a bicyclic lactone
    122.
    发明授权
    Photochemical process for preparing a bicyclic lactone 失效
    用于制备双相乳液的光化学方法

    公开(公告)号：US3674663A

    公开(公告)日：1972-07-04

    申请号：US3674663D

    申请日：1969-11-28

    申请人： ZOECON CORP

    发明人： SIDDALL JOHN B

    IPC分类号： C07C57/18 ,  C07D311/94 ,  C07D315/00 ,  B01J1/10

    CPC分类号： C07D315/00 ,  C07C57/18 ,  C07D311/94

    摘要： Synthesis of cis 2-(1''-methyl-2''-isopropenylcyclobutyl)ethanol, a component of the boll weevil sex attractant, and intermediates therefor, in which 5-hydroxy-pent-2-ynoic acid or ethers thereof is methylated followed by cyclization to yield 3-methylpent-2eno-5-lactone which is irradiated in presence of ethylene to yield 2,3-cycloethylene-3-methylpentano-5-lactone which is cleaved and converted into 2-(1''-methyl-2''isopropenylcyclobutyl)ethanol.

    摘要翻译： 顺式2-（1'-甲基-2'-异丙烯基环丁基）乙醇的合成，其为5-位羟基 - 戊-2-炔酸或其醚甲基化，然后是其中的5-羟基 - 戊-2-炔酸或其醚， 在乙烯存在下照射3-甲基戊-2-烯-5-内酯，得到2,3-环亚乙基-3-甲基戊-5-烯酮，将其切割并转化为2-（1'-甲基 - 2'-异丙烯基环丁基）乙醇。

    Photochemical preparation of a bicyclic lactone
    123.
    发明授权
    Photochemical preparation of a bicyclic lactone 失效
    双相乳液的光化学制备

    公开(公告)号：US3627660A

    公开(公告)日：1971-12-14

    申请号：US3627660D

    申请日：1969-12-08

    申请人： ZOECON CORP

    发明人： SIDDAL JOHN B

    IPC分类号： C07D311/94 ,  C07D315/00 ,  B01J1/10

    CPC分类号： C07D315/00 ,  C07D311/94

    摘要： Synthesis of cis 2-(1''-methyl-2''-isopropenylcyclobutyl)ethanol, a component of the boll weevil sex attractant, and intermediates therefor, in which 5-hydroxy-pent-2-ynoic acid ester or ethers thereof is methylated followed by cyclization to yield 3methylpent-2-eno-5-lactone which is irradiated in presence of ethylene to yield 2,3-cycloethylene-3-methylpentano-5-lactone which is cleaved and converted into 2-(1''-methyl-2''isopropenylcyclobutyl)ethanol.

    Preparation of lactones such as substituted delta valerolactones
    124.
    发明授权
    Preparation of lactones such as substituted delta valerolactones 失效
    乳液的制备如取代的三氯甲烷

    公开(公告)号：US3607885A

    公开(公告)日：1971-09-21

    申请号：US3607885D

    申请日：1968-08-15

    申请人： UNIVERSAL OIL PROD CO

    发明人： DOMBRO ROBERT A

    IPC分类号： C07D315/00 ,  C07D7/06

    CPC分类号： C07D315/00

    摘要： Lactones may be prepared from alcohols by treating said alcohol with methyl alcohol in the presence of an alkaline substance and an oxidizing agent at an elevated temperature to prepare the desired product. Examples of such lactones are dimethyl, diphenyl, dicyclohexyl and di-p-tolyl-delta-valerolactones. These compounds have utility as solvents and as starting monomers in the preparation of polyester formulations, among other uses.

    Preparation of angelica lactone
    125.
    发明授权
    Preparation of angelica lactone 失效
    黑麦草的制备

    公开(公告)号：US3564020A

    公开(公告)日：1971-02-16

    申请号：US3564020D

    申请日：1968-07-17

    申请人： UNION OIL CO

    发明人： FENTON DONALD M

    IPC分类号： C07D315/00 ,  C07D5/06

    CPC分类号： C07D315/00

    摘要： CONJUGATED DILEFINS BEARING A HALOGEN ON AN UNSATURATED CARBON ARE REACTED WITH CARBON MONOXIDE AND WATER IN THE PRESENCE OF A GROUP VIII NOBLE METAL CATALYST TO PREPARE UNSATURATED LACTONES. A SPECIFIC EMBODIMENT COMPRISES THE PREPARATION OF ANGELICA LACTONE FROM 2-HALO BUTADIENE.