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    Isocyanate-reactive formulation for rigid polyurethane foam
    13.
    发明授权
    Isocyanate-reactive formulation for rigid polyurethane foam 有权

    公开(公告)号：US10144797B2

    公开(公告)日：2018-12-04

    申请号：US15557518

    申请日：2016-03-02

    Applicant: Dow Global Technologies LLC

    Inventor： Davide Micheletti ,  Rossella Riccio ,  Jean-Paul Masy ,  Vanni Parenti

    IPC: C08G18/48 ,  C08G18/50 ,  C08G18/76 ,  C08G18/16 ,  C08G101/00

    Abstract: A storage stable isocyanate-reactive composition includes a reactive component including (a) 5 wt % to 30 wt % of at least one Novolac-type polyoxypropylene polyether polyol having a hydroxyl functionality from 2 to 5 and a hydroxyl number from 130 to 450 mg KOH/g, (b) 20 wt % to 60 wt % of at least one high functional polyether polyol having a hydroxyl functionality from 6 to 8 and a hydroxyl number from 300 to 700 mg KOH/g, (c) 2 wt % to 30 wt % of at least one low functional polyether polyol having a hydroxyl functionality from 2 to 5 and a hydroxyl number from 50 to 400 mg KOH/g, (d) 2 wt % to 30 wt % of at least one amine initiated polyol having a hydroxyl number from 250 to 600 mg KOH/g, and (e) 1 wt % to 25 wt % of one or more additives; and a hydrocarbon physical blowing agent component in an amount of at least 10 parts by weight for each 100 parts by weight of the reactive component.

    DUAL CATALYST SYSTEM FOR HIGH PRIMARY HYDROXYL POLYOLS
    14.
    发明申请
    DUAL CATALYST SYSTEM FOR HIGH PRIMARY HYDROXYL POLYOLS 有权

    公开(公告)号：US20170240702A1

    公开(公告)日：2017-08-24

    申请号：US15504368

    申请日：2015-10-19

    Applicant: Dow Global Technologies LLC

    Inventor： Arjun Raghuraman ,  Matthias Schaefer ,  Jean-Paul Masy ,  David S. Laitar

    IPC: C08G65/26

    CPC classification number: C08G65/269 ,  B01J23/75 ,  B01J27/26 ,  C08G65/2654 ,  C08G65/266 ,  C08G65/2663 ,  C08G65/2696

    Abstract: A method of producing a high primary hydroxyl group content and a high number average molecular weight polyol includes preparing a mixture that includes a double metal cyanide catalyst and a low molecular weight polyether polyol having a number average molecular weight of less than 1,000 g/mol, the polyether polyol is derived from propylene oxide, ethylene oxide, or butylene oxide, setting the mixture to having a first temperature, adding at least one selected from propylene oxide, ethylene oxide, and butylene oxide to the mixture at the first temperature, allowing the mixture to react to form a reacted mixture, adding a Lewis acid catalyst to the reacted mixture, setting the reaction mixture including the second catalyst to have a second temperature that is less than the first temperature, and adding additional at least one selected from propylene oxide, ethylene oxide, and butylene oxide to the reacted mixture at the second temperature such that a resultant polyol having a primary hydroxyl group content of at least 60% and a number average molecular weight greater than 2,500 g/mol is formed.

    Method for Making Poly(Butylene Oxide) Polyols
    15.
    发明申请
    Method for Making Poly(Butylene Oxide) Polyols 有权
    制备聚（环氧丁烷）多元醇的方法

    公开(公告)号：US20160215091A1

    公开(公告)日：2016-07-28

    申请号：US15024096

    申请日：2014-08-16

    Applicant: DOW GLOBAL TECHNOLOGIES LLC

    Inventor： Jean-Paul Masy ,  Myriam Linke ,  David A. Babb ,  John W. Weston

    IPC: C08G65/12

    CPC classification number: C08G65/12 ,  C08G65/2606 ,  C08G65/2609 ,  C08G65/2663 ,  C08G65/2696

    Abstract: 1,2-butylene oxide is homopolymerized or randomly copolymerized in the presence of a double metal cyanide catalyst such as a zinc hexacyanocobaltate catalyst complex. The polymers unexpectedly contain significant amounts of monofunctional impurities, which can be partially controlled through selection of polymerization conditions.

    Abstract translation: 1,2-二氧化环在双金属氰化物催化剂如六氰基钴酸锌催化剂络合物的存在下均聚或无规共聚。 聚合物意外地含有大量的单官能杂质，其可以通过选择聚合条件来部分控制。

    Macromer and Process for Making Polymer Polyols
    16.
    发明申请
    Macromer and Process for Making Polymer Polyols 有权
    大分子单体和制备聚合物多元醇的方法

    公开(公告)号：US20150274952A1

    公开(公告)日：2015-10-01

    申请号：US14429154

    申请日：2013-09-23

    Applicant: DOW GLOBAL TECHNOLOGIES LLC

    Inventor： Ricco B. Borella ,  Sven Claessens ,  Jean-Paul Masy ,  Stijn De Loos

    IPC: C08L25/12 ,  C08J9/12 ,  C08J9/00

    CPC classification number: C08L25/12 ,  C08G18/4072 ,  C08G18/632 ,  C08G18/636 ,  C08G2101/0008 ,  C08G2101/005 ,  C08G2101/0083 ,  C08G2650/58 ,  C08J9/0061 ,  C08J9/12 ,  C08J2375/08 ,  C08J2425/12

    Abstract: Polymer polyols are made by polymerizing an ethylenically unsaturated monomer in a continuous polyol phase. The polymerization is stabilized with a macromer or a pre-formed polymer made by polymerizing or copolymerizing the macromer. The macromer is a random polymer of propylene oxide and ethylene oxide in defined ratios, which also contains polymerization carbon-carbon double or triple bond. Polymer polyols made in the process exhibit little viscosity rise when blended with water. Flexible polyurethane foam made from the polymer polyol exhibits excellent hardness, have good surface characteristics and, when pigmented, exhibit good, uniform coloration.

    Abstract translation: 聚合物多元醇通过在连续多元醇相中聚合烯属不饱和单体制备。 用大分子单体或通过聚合或共聚大分子单体制备的预形成聚合物稳定聚合。 大分子单体是一定比例的环氧丙烷和环氧乙烷的无规聚合物，其还含有聚合碳 - 碳双键或三键。 当与水混合时，在该方法中制备的聚合物多元醇几乎没有粘度上升。 由聚合物多元醇制成的柔性聚氨酯泡沫体显示出优异的硬度，具有良好的表面特性，并且当着色时表现出良好的均匀着色。

    PROCESS FOR MAKING POLYETHER DIOLS
    18.
    发明申请
    PROCESS FOR MAKING POLYETHER DIOLS 审中-公开

    公开(公告)号：US20200181326A1

    公开(公告)日：2020-06-11

    申请号：US16313516

    申请日：2017-06-12

    Applicant: Dow Global Technologies LLC

    Inventor： Jean-Paul Masy ,  Oguz Türünç

    IPC: C08G65/26 ,  B01J23/75 ,  C08G65/334

    Abstract: Polyether diols characterized by a hydroxyl number of 56 or lower, high average functionality and high primary hydroxyl content are prepared by alkoxylating an unsaturated alcohol in multiple steps to form a polyether monol that contains 39% or more primary hydroxyl groups, and then reacting the polyether monol with a mercaptoalcohol that has a primary hydroxyl group.

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