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    Isolation of &agr;-ethynyl carbinols by distillation
    15.
    发明授权
    Isolation of &agr;-ethynyl carbinols by distillation 失效
    通过蒸馏分离α-乙炔基甲醇

    公开(公告)号：US06316680B1

    公开(公告)日：2001-11-13

    申请号：US09455161

    申请日：1999-12-06

    申请人： Ralf-Thomas Rahn ,  Harald Rust ,  Thomas Rühl ,  Jochem Henkelmann ,  Susanne Stutz

    发明人： Ralf-Thomas Rahn ,  Harald Rust ,  Thomas Rühl ,  Jochem Henkelmann ,  Susanne Stutz

    IPC分类号： C07C2726

    CPC分类号： C07C29/80 ,  C07C33/042 ,  C07C33/048

    摘要： In a process for isolating &agr;-ethynyl carbinols from the liquid reaction mixture from the addition of acetylene onto &agr;,&bgr;-unsaturated carbonyl compounds by distillation, the distillation is carried out continuously, the feed stream is introduced into the middle section of a distillation column (K), the major part of the water is distilled off azeotropically together with the solvent at the top of the column, and the &agr;-ethynyl carbinol target product is taken off below the feed point to the column.

    摘要翻译： 在通过蒸馏从乙炔加入到α，β-不饱和羰基化合物中的液体反应混合物中分离α-乙炔基甲醇的方法中，蒸馏连续进行，将进料流引入蒸馏塔的中间部分 （K）中，将大部分水与塔顶部的溶剂一起共沸蒸馏，并将α-乙炔基甲醇目标产物从柱的进料点以下取出。

    Mixture for the treatment of urea-containing fertilizers
    16.
    发明授权
    Mixture for the treatment of urea-containing fertilizers 有权
    混合物用于处理含尿素肥料

    公开(公告)号：US08603211B2

    公开(公告)日：2013-12-10

    申请号：US12809847

    申请日：2008-12-18

    申请人： Ralf-Thomas Rahn ,  Gerd Buehler ,  Alexander Wissemeier ,  Wolfgang Weigelt

    发明人： Ralf-Thomas Rahn ,  Gerd Buehler ,  Alexander Wissemeier ,  Wolfgang Weigelt

    IPC分类号： C05C9/00 ,  C05F11/00 ,  C09K3/00

    CPC分类号： C05C9/005 ,  C05G3/0041 ,  C05G3/08 ,  Y02P60/218

    摘要： A mixture for the treatment of urea-containing fertilizers comprises a) at least one (thio)phosphoric acid triamide of the general formula (I) R1R2N—P(X)(NH2)2 and/or (thio)phosphoric acid diamide of the general formula (II) R1O—P(X)(NH2)2, X denoting oxygen or sulfur, R1 and R2 independently from each other being hydrogen, substituted or unsubstituted 2-nitrophenyl, C1-10-alkyl, C3-10-cycloalkyl, C3-10-heterocycloalkyl, C6-10-aryl, C6-10-heteroaryl or diaminocarbonyl, where R1 and R2 together with the nitrogen atom connecting them can also form a 5 or 6-membered saturated or unsaturated heterocyclic group, which optionally may also comprise one or two additional heteroatoms selected from the group consisting of nitrogen, oxygen, and sulfur, as component A, and b) at least one compound comprising an amino group having a boiling point of more than 100° C. as component B.

    摘要翻译： 用于处理含尿素肥料的混合物包括a）通式（I）的至少一种（硫代）磷酸三酰胺R1R2N-P（X）（NH2）2和/或（硫代）磷酸二酰胺 通式（II）R1O-P（X）（NH2）2，X表示氧或硫，R1和R2彼此独立地为氢，取代或未取代的2-硝基苯基，C1-10烷基，C3-10-环烷基 ，C 3-10 - 杂环烷基，C 6-10 - 芳基，C 6-10 - 杂芳基或二氨基羰基，其中R 1和R 2与连接它们的氮原子一起也可以形成5或6元饱和或不饱和的杂环基， 还包含一个或两个另外的选自氮，氧和硫的杂原子作为组分A，和b）至少一种包含沸点高于100℃的氨基的化合物作为组分B.

    MIXTURE FOR THE TREATMENT OF UREA-CONTAINING FERTILIZERS
    19.
    发明申请
    MIXTURE FOR THE TREATMENT OF UREA-CONTAINING FERTILIZERS 有权
    用于治疗含尿素肥料的混合物

    公开(公告)号：US20110154874A1

    公开(公告)日：2011-06-30

    申请号：US12809847

    申请日：2008-12-18

    申请人： Ralf-Thomas Rahn ,  Gerd Buehler ,  Alexander Wissemeier ,  Wolfgang Weigelt

    发明人： Ralf-Thomas Rahn ,  Gerd Buehler ,  Alexander Wissemeier ,  Wolfgang Weigelt

    IPC分类号： C05C9/00 ,  C05F3/00

    CPC分类号： C05C9/005 ,  C05G3/0041 ,  C05G3/08 ,  Y02P60/218

    摘要： A mixture for the treatment of urea-containing fertilizers comprises a) at least one (thio)phosphoric acid triamide of the general formula (I) R1R2N—P(X)(NH2)2 and/or (thio)phosphoric acid diamide of the general formula (II) R1O—P(X)(NH2)2, X denoting oxygen or sulfur, R1 and R2 independently from each other being hydrogen, substituted or unsubstituted 2-nitrophenyl, C1-10-alkyl, C3-10-cycloalkyl, C3-10-heterocycloalkyl, C6-10-aryl, C6-10-heteroaryl or diaminocarbonyl, where R1 and R2 together with the nitrogen atom connecting them can also form a 5 or 6-membered saturated or unsaturated heterocyclic group, which optionally may also comprise one or two additional heteroatoms selected from the group consisting of nitrogen, oxygen, and sulfur, as component A, and b) at least one compound comprising an amino group having a boiling point of more than 100° C. as component B.

    摘要翻译： 用于处理含尿素肥料的混合物包括a）通式（I）的至少一种（硫代）磷酸三酰胺R1R2N-P（X）（NH2）2和/或（硫代）磷酸二酰胺 通式（II）R1O-P（X）（NH2）2，X表示氧或硫，R1和R2彼此独立地为氢，取代或未取代的2-硝基苯基，C1-10烷基，C3-10-环烷基 ，C 3-10 - 杂环烷基，C 6-10 - 芳基，C 6-10 - 杂芳基或二氨基羰基，其中R 1和R 2与连接它们的氮原子一起也可以形成5或6元饱和或不饱和的杂环基， 还包含一个或两个另外的选自氮，氧和硫的杂原子作为组分A，和b）至少一种包含沸点高于100℃的氨基的化合物作为组分B.