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    Difluorophenyl pyrimidyl pyridine derivatives and the use thereof in liquid crystal mixtures
    13.
    发明授权
    Difluorophenyl pyrimidyl pyridine derivatives and the use thereof in liquid crystal mixtures 失效
    二氟苯基嘧啶基吡啶衍生物及其在液晶混合物中的应用

    公开(公告)号：US6022492A

    公开(公告)日：2000-02-08

    申请号：US91404

    申请日：1999-01-14

    申请人： Toshiaki Nonaka ,  Ji Li ,  Ayako Takeichi ,  Barbara Hornung ,  Javier Manero ,  Wolfgang Schmidt ,  Rainer Wingen

    发明人： Toshiaki Nonaka ,  Ji Li ,  Ayako Takeichi ,  Barbara Hornung ,  Javier Manero ,  Wolfgang Schmidt ,  Rainer Wingen

    IPC分类号： G02F1/13 ,  C07D401/04 ,  C07D405/14 ,  C09K19/02 ,  C09K19/34 ,  C09K19/42 ,  C07D211/72 ,  C07D239/02

    CPC分类号： C07D401/04 ,  C07D405/14 ,  C09K19/0225 ,  C09K19/3003 ,  C09K19/34 ,  C09K19/3466 ,  C09K19/42

    摘要： Difluorophenylpyrimidylpyridine derivatives of the formula (I) ##STR1## wherein X is N and Y is CH or X is CH and Y is N;R.sup.1 and R.sup.2 are identical or different and area) an unbranched or branched alkyl chain having 1 to 20 carbon atoms, whereaa) one or more non-adjacent and non-terminal CH.sub.2 groups may be replaced by --O--, --CO--O--, --O--CO--, --O--CO--O-- or --Si(CH.sub.3).sub.2 --, and/orab) one or more H atoms may be replaced by F, and/orac) the terminal CH.sub.3 group may be replaced by one of the following chiral groups (optically active or racemic): ##STR2## R.sup.3, R.sup.4 and R.sup.5 are identical or different and are hydrogen or a straight-chain or branched alkyl radical having 1-16 carbon atoms (with or without an asymmetrical carbon atom), where, in addition, one or more non-adjacent non-terminal CH.sub.2 groups may be replaced by --O--, and/or where one or more H atoms of the alkyl radical may be substituted by --F; R.sup.4 and R.sup.5 may alternatively together be --(CH.sub.2).sub.4 -- or --(CH.sub.2).sub.5 -- if they are bonded to a dioxolane system,are suitable as components, in particular, of ferroelectric liquid-crystal mixtures.

    摘要翻译： PCT No.PCT / EP96 / 05774 Sec。 371日期1999年1月14日第 102（e）日期1999年1月14日PCT 1996年12月20日PCT公布。 第WO97 / 24351号公报 日期：1997年7月10日，式（I）的二氟苯基嘧啶基吡啶衍生物，其中X为N，Y为CH或X为CH，Y为N; R1和R2相同或不同，并且a）具有1至20个碳原子的无支链或支链烷基链，其中aa）一个或多个非相邻和非末端的CH 2基团可以被-O - ， - CO- O-，-O-CO-，-O-CO-O-或-Si（CH 3）2 - 和/或ab）一个或多个H原子可以被F替代，和/或ac） 可以被以下手性基团（光学活性或外消旋）之一代替：R3，R4和R5相同或不同，是氢或具有1-16个碳原子的直链或支链烷基（具有或不具有不对称的 碳原子），此外，一个或多个非相邻的非末端CH 2基团可被-O-取代，和/或烷基的一个或多个H原子可被-F取代; R4和R5可以一起为 - （CH 2）4 - 或 - （CH 2）5 - 如果它们与二氧杂环戊烷体系结合，则适合作为组分，特别是铁电液晶混合物。

    Fluorinated heterocycles and their use in liquid-crystal mixtures
    16.
    发明授权
    Fluorinated heterocycles and their use in liquid-crystal mixtures 有权

    公开(公告)号：US07026021B2

    公开(公告)日：2006-04-11

    申请号：US10903937

    申请日：2004-07-30

    申请人： Rainer Wingen ,  Barbara Hornung ,  Wolfgang Schmidt

    发明人： Rainer Wingen ,  Barbara Hornung ,  Wolfgang Schmidt

    IPC分类号： C09K19/34 ,  C09K19/32 ,  C07D307/77 ,  C07D307/93 ,  C07C23/08

    CPC分类号： C07D307/93 ,  C09K2019/3408 ,  Y10T428/10

    摘要： Compounds of the general formula (I) where: R1, R2 are each independently a) H b) -M1-A1-R5 c) a straight-chain or branched alkyl radical having from 1 to 16 carbon atoms or a straight-chain or branched alkenyl radical having from 2 to 16 carbon atoms, where c1) one or more nonadjacent and nonterminal CH2 groups may be replaced by —O—, —C(═O)O—, —O—C(═O)—, —O—C(═O)—O—, —C(═O)— or —Si(CH3)2—, and/or c2) one CH2 group may be replaced by —C≡C—, cyclopropane-1,2-diyl, cyclobutane-1,3-diyl, cyclohexane-1,4-diyl or phenylene-1,4-diyl, and/or c3) one or more hydrogen atoms may be replaced by F and/or Cl, p, q are each independently 0 or 1 G1-G2 is —CH2CH—, —CH═C—, —CH2CH2CH— or —CH═CH—CH— M1 is —CO—O—, —O—CO—, —CH2—O—, —O—CH2—, —CF2—O—, —O—CF2—, —CH═CH—, —CF═CF—, —C≡C—, —CH2—CH2—CO—O—, —O—CO—CH2—CH2—, —CH2—CH2—, —CF2—CF2—, —(CH2)4—, —OC(═O)CF═CF— or a single bond, A1 is 1,4-phenylene where one or two hydrogen atoms may be replaced by F, Cl, CN and/or OCF3, or up to three hydrogen atoms may be replaced by fluorine, 1,4-cyclohexylene where one or two hydrogen atoms may be replaced by CH3 and/or F, 1-cyclohexene-1,4-diyl, where one hydrogen atom may be replaced by CH3 or F, or 1,3-dioxane-2,5-diyl, R5 has the same possible definitions as R1 and R2, with the exception of -M1-A1-R5 with the provisos that: a) at least one of p, q is 1, b) R1 and R2 must not at the same time be H. are used in liquid-crystal mixtures.

    Fluorinated heterocycles and their use in liquid-crystal mixtures
    18.
    发明申请
    Fluorinated heterocycles and their use in liquid-crystal mixtures 有权
    氟化杂环及其在液晶混合物中的应用

    公开(公告)号：US20050258399A1

    公开(公告)日：2005-11-24

    申请号：US11117280

    申请日：2005-04-28

    申请人： Wolfgang Schmidt ,  Rainer Wingen ,  Barbara Hornung

    发明人： Wolfgang Schmidt ,  Rainer Wingen ,  Barbara Hornung

    IPC分类号： C07C25/00 ,  C07D307/91 ,  C09K19/00 ,  C09K19/32 ,  C09K19/34

    CPC分类号： C07D307/91 ,  C09K2019/3408 ,  Y10T428/10

    摘要： In the compound of the formula (I), where: R1, R2 are each independently, for example, H or a straight-chain or branched alkyl radical p, q are each independently 0 or 1, i.e. at the value zero, —H is present at the appropriate position instead of —F M1 is —CO—O—, —O—CO—, —CH2—O—, —O—CH2—, —CF2—O—, —O—CF2—, —CH═CH—, —CF═CF—, —C≡C—, —CH2—CH2—CO——O—,—O—CO—CH2—CH2—, —CH2—CH2—, —CF2—CF2—, —(CH2)4—, —OC(═O)CF═CF— or a single bond A1 is, for example, 1,4-phenylene R5 has the same possible definitions as specified for R1 and R2, with the exception of -M1-A1-R5, but independently of the definition of R1 and R2 X is H, F, OF3, CF3, OCF2H with the following provisos: a) at least one of p, q has to be 1 b) R1 and R2 must not at the same time be H c) R2 and X must not at the same time be H.

    摘要翻译： 在式（I）的化合物中，其中：R 1，R 2各自独立地为例如H或直链或支链烷基p， q各自独立地为0或1，即在零值时，-H存在于适当的位置，而不是-FM 1是-CO-O-，-O-CO-，-CH O 2，-O-CH 2 - ， - CO 2 -O - ， - O-CF 2 -O - ， - O-CH 2 > - ， - CH-CH-，-CF-CF-，-C≡C-， - CH 2 -CH 2 -CO-O - ， - O -CO-CH 2 -CH 2 - ， - CH 2 -CH 2 - ， - CFF - （CH 2）4 - ， - OC（-O）CF-CF-（CH 2）2 - 或单键A 1，例如，1,4-亚苯基R 5具有与R 1和R 2相同的可能定义， R＆lt; 2＆gt;除了-M 1以上的1〜5，但与定义 R 1，R 2，X 2是H，F 3，CF 3，OCF 3， 2 H，具有以下条件：a）至少 p，q中的一​​个必须为1b）R 1和R 2不能同时为H c）R 2和/或 X不能同时为H.

    Fluorinated polycycles and their use in liquid-crystal mixtures
    19.
    发明授权
    Fluorinated polycycles and their use in liquid-crystal mixtures 有权

    公开(公告)号：US06955838B2

    公开(公告)日：2005-10-18

    申请号：US10903082

    申请日：2004-07-30

    申请人： Rainer Wingen ,  Barbara Hornung ,  Wolfgang Schmidt

    发明人： Rainer Wingen ,  Barbara Hornung ,  Wolfgang Schmidt

    IPC分类号： C07D307/77 ,  C09K19/34 ,  C09K19/52 ,  C07C23/46 ,  C07D549/457 ,  C09K19/61 ,  C09K19/62

    CPC分类号： C07D307/77 ,  C09K2019/3408 ,  Y10T428/10

    摘要： Compounds of the formula (I) where: R1, R2 are each independently a) H b) -M1-A1-R5 c) a straight-chain or branched alkyl radical having from 1 to 16 carbon atoms or a straight-chain or branched alkenyl radical having from 2 to 16 carbon atoms, where c1) one or more nonadjacent and nonterminal CH2 groups may be replaced by —O—, —C(═O)O—, —O—C(═O)—, —O—C(═O)—O—, —C(═O)— or —Si(CH3)2—, and/or c2) one CH2 group may be replaced by —C≡C—, cyclopropane-1,2-diyl, cyclobutane-1,3-diyl, cyclohexane-1,4-diyl or phenylene-1,4-diyl, and/or c3) one or more hydrogen atoms may be replaced by F and/or Cl, p, q, r are each independently 0 or 1 M1—is —CO—O—, —O—CO—, —CH2—O—, —O—CH2—, —CF2—O—, —O—CF2—, —CH═CH—, —CF═CF—, —C≡C—, —CH2—CH2—CO—O—, —O—CO—CH2—CH2—, —CH2—CH2—, —CF2—CF2—, —(CH2)4—, —OC(═O)CF═CF— or a single bond, A1 is 1,4-phenylene where one or two hydrogen atoms may be replaced by F, Cl, CN and/or OCF3, or up to three hydrogen atoms may be replaced by fluorine, 1,4-cyclohexylene where one or two hydrogen atoms may be replaced by CH3 and/or F, 1-cyclohexene-1,4-diyl where one hydrogen atom may be replaced by CH3 or F, or 1,3-dioxane-2,5-diyl, R5 has the same possible definitions as R1 and R2 with the exception of -M1-A1-R5, with the provisos that: a) at least one of p, q, r is 1 b) R1 and R2 must not at the same time be H are used in liquid-crystal mixtures.