公开(公告)号：US06533990B2

公开(公告)日：2003-03-18

申请号：US10180960

申请日：2002-06-26

申请人： Ivaylo Popov ,  Hans-Jürgen Kemmer ,  Harald Scholz

发明人： Ivaylo Popov ,  Hans-Jürgen Kemmer ,  Harald Scholz

IPC分类号： C22B902

CPC分类号： C22B7/003 ,  C22B19/12 ,  Y02P10/212

摘要： In the apparatus for distilling molten baths, substantially comprising a two-part vacuum tank (2), a melting crucible (5) disposed in the bottom housing part (3) of the vacuum tank and surrounded by a heating coil (4), a hat-shaped metal vapor condenser (8) held in the top housing part (6) of the vacuum tank (2), and a draining channel (10) disposed between the melting crucible (5) and the metal vapor condenser (8), a filter element (16) penetrated by a metal vapor thermometer (19) plus probe (20) is provided above the metal vapor condenser (8) in an opening (15) of the top housing part (6), wherein both the filter pot (17) surrounding the filter element (16), as well as the space (22) behind the coil, as well as the top housing part (6) are connected by separate individual vacuum lines (18, 23, 25) to a vacuum source (7).

摘要翻译： 在用于蒸馏熔融浴的装置中，基本上包括两部分真空罐（2），设置在真空罐的底部壳体部分（3）中并被加热线圈（4）围绕的熔化坩埚（5） 保持在真空容器（2）的顶部壳体部分（6）中的帽形金属蒸气冷凝器（8）和设置在熔化坩埚（5）和金属蒸汽冷凝器（8）之间的排水通道（10） 在顶部壳体部分（6）的开口（15）中的金属蒸汽冷凝器（8）的上方设置由金属蒸气温度计（19）加上探头（20）穿透的过滤元件（16），其中两个过滤罐 （17）围绕过滤元件（16）以及线圈后面的空间（22）以及顶部壳体部分（6）通过单独的单独的真空管线（18,23,25）连接到真空 来源（7）。

公开(公告)号：US20130282158A1

公开(公告)日：2013-10-24

申请号：US13880573

申请日：2011-10-06

申请人： Ralf Oehler ,  Harald Scholz ,  Frank-Werner Hoffmann

发明人： Ralf Oehler ,  Harald Scholz ,  Frank-Werner Hoffmann

IPC分类号： G05B23/02

CPC分类号： G05B23/0205 ,  C22B9/20 ,  F27D11/10 ,  F27D21/00 ,  F27D2019/0037 ,  H05B7/144 ,  H05B7/148 ,  Y02P10/256 ,  Y02P10/259

摘要： The invention relates to a method and device (40) for filtering supply network failures (84) out of an electrode signal (82) in a metallurgical electric remelting process, in particular for the electrode gap closed-loop control of a system for closed-loop control of an electrode gap (48) of a melting furnace (10). For this purpose, said device also comprises at least one electrode sensor device (44) for measuring an electrode signal (82), in particular electrode current and/or electrode voltage of the electrode (30), a network sensor device (46) for measuring a network signal, in particular network current and/or network voltage, and a filter device (50) for filtering network failures (84) of the network signal out of the electrode signal (82), such that an electrode signal (80) with no network failures can be emitted.

摘要翻译： 本发明涉及一种用于在冶金电重熔过程中从电极信号（82）中过滤供电网络故障（84）的方法和装置（40），特别是用于封闭系统的系统的电极间隙闭环控制， 对熔化炉（10）的电极间隙（48）进行回路控制。 为此目的，所述装置还包括用于测量电极信号（82）的至少一个电极传感器装置（44），特别是电极（30）的电极电流和/或电极电压，网络传感器装置（46），用于 测量网络信号，特别是网络电流和/或网络电压;以及滤波器装置（50），用于从电极信号（82）中滤出网络信号的网络故障（84），使得电极信号（80） 没有发生网络故障。

公开(公告)号：US4788359A

公开(公告)日：1988-11-29

申请号：US78372

申请日：1987-07-27

申请人： Kurt Schuchardt ,  Harald Scholz ,  Erich Niehus ,  Harald Adam

发明人： Kurt Schuchardt ,  Harald Scholz ,  Erich Niehus ,  Harald Adam

IPC分类号： B01D53/70 ,  B01D53/04 ,  C07C17/00 ,  C07C17/156 ,  C07C17/38 ,  C07C17/389 ,  C07C19/045 ,  C07C67/00 ,  C07C17/15

CPC分类号： C07C17/156 ,  C07C17/389

摘要： 1,2-dichloroethane is continuously and completely removed and recovered from the off-gas obtained during the production of 1,2-dichloroethane by subjecting ethylene to an oxychlorination reaction with hydrogen chloride and oxygen. The off-gas is initially contacted with active carbon, then incinerated at temperatures higher than 900.degree. C. and ultimately freed from hydrogen chloride and chlorine, and the active carbon is freed from 1,2-dichloroethane and regenerated by treating it with hot steam. More particularly, the off-gas loaded with the 1,2-dichloroethane and having a temperature of 1.degree. C. to 10.degree. C. is heated to a temperature at least 20.degree. C. higher than the respective dew point of water and contacted with the active carbon.

摘要翻译： 1,2-二氯乙烷通过使乙烯与氯化氢和氧进行氧氯化反应，在1,2-二氯乙烷生产过程中获得的废气中连续并完全除去并回收。 废气最初与活性炭接触，然后在高于900℃的温度下焚烧，最终从氯化氢和氯中除去，活性炭从1,2-二氯乙烷中脱除，并用热蒸汽处理再生 。 更具体地说，将负载有1,2-二氯乙烷并且具有1℃至10℃温度的废气加热到高于相应露点的水至少20℃并接触的温度 与活性炭。

公开(公告)号：US4265837A

公开(公告)日：1981-05-05

申请号：US33817

申请日：1979-04-27

申请人： Gunter Legutke ,  Harald Scholz ,  Kurt Schuchardt

发明人： Gunter Legutke ,  Harald Scholz ,  Kurt Schuchardt

IPC分类号： B01J21/00 ,  B01J27/122 ,  C07C17/00 ,  C07C17/156 ,  C07C19/045 ,  C07C67/00 ,  C07C17/02

CPC分类号： C07C17/156 ,  Y02P20/582

摘要： The invention provides a process for making 1,2-dichloroethane by subjecting ethylene to an oxychlorination reaction with hydrogen chloride and a gas containing molecular oxygen, in gas phase, at elevated temperature and in contact with a fluidized bed catalyst of copper-II-chloride on a carrier, wherein the reaction gases are cooled under pressure in two condensation stages, condensed 1,2-dichloroethane and water are removed, the bulk of unreacted starting gas and inert gas are recycled, the reaction gases coming from the second condensation stage are delivered to a third condensation stage, cooled therein under pressure down to a temperature within the range 5.degree. to 18.degree. C. and to the extent necessary to retain in the recycle gas 0.5 to 3 volume % of 1,2-dichloroethane, and the recycle gas is admixed, directly upstream of the reactor, with a quantity of pure oxygen necessary to replace consumed oxygen. The present process provides more specifically for preheated hydrogen chloride to be wholly or partially introduced into the recycle gas heated to 150.degree. to 200.degree. C. and for the latter to be then admixed with pure oxygen, the oxygen being admitted at a point lying between the hydrogen chloride feed point and the feed point of the recycle gas into the reactor.

摘要翻译： 本发明提供了一种制备1,2-二氯乙烷的方法，该方法是使乙烯与氯化氢和含有分子氧的气体在升高的温度下进行氧氯化反应，并与氯化铜 - 氯化物的流化床催化剂接触 在载体上，其中反应气体在两个冷凝阶段在压力下冷却，冷凝的1,2-二氯乙烷和水被除去，大部分未反应的起始气体和惰性气体被再循环，来自第二冷凝级的反应气体是 输送到第三冷凝阶段，在压力下冷却到5℃至18℃的温度，并且在必要的程度上保留0.5至3体积％的1,2-二氯乙烷，并且 循环气体直接在反应器的上游与一定量的纯氧混合，以代替消耗的氧气。 本方法更具体地提供了将预热的氯化氢全部或部分引入加热至150℃至200℃的再循环气体中，然后将其与纯氧混合，氧气在位于 氯化氢进料点和进入反应器的循环气体的进料点。