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    Method for controlling the molecular weight during poly(arylene vinylene) synthesis, and polymers produced therewith
    21.
    发明授权
    Method for controlling the molecular weight during poly(arylene vinylene) synthesis, and polymers produced therewith 失效
    用于控制聚（亚芳基亚乙烯基）合成期间的分子量的方法和由其制备的聚合物

    公开(公告)号：US07884175B2

    公开(公告)日：2011-02-08

    申请号：US10553534

    申请日：2004-04-13

    申请人： Hubert Spreitzer ,  Heinrich Becker ,  Elfriede Hufsky

    发明人： Hubert Spreitzer ,  Heinrich Becker ,  Elfriede Hufsky

    IPC分类号： C08G75/00 ,  C08G61/00

    CPC分类号： C08G61/10 ,  H01L51/0038

    摘要： The present invention relates to a process in which addition of certain bis(methyl)aryl compounds which have a further substituent other than hydrogen and on which at least one of the two methyl groups bears a leaving group, the molecular weight in the synthesis of poly(arylenevinylenes) is controlled reproducibly and can be deduced by the GILCH polymerization or by the sulfinyl precursor route, and to the polymers obtainable by means of the process according to the invention.

    摘要翻译： 本发明涉及一种方法，其中加入某些具有除氢以外的取代基的双（甲基）芳基化合物，其中两个甲基中的至少一个带有离去基团，聚合物中的分子量 （亚芳基亚乙烯基）可以重复地控制，并且可以通过GILCH聚合或亚磺酰基前体途径以及通过本发明的方法获得的聚合物来推导。

    RHODIUM COMPLEXES AND IRIDIUM COMPLEXES
    22.
    发明申请
    RHODIUM COMPLEXES AND IRIDIUM COMPLEXES 审中-公开
    RHODIUM复合物和IRIDIUM复合物

    公开(公告)号：US20100113779A1

    公开(公告)日：2010-05-06

    申请号：US12613198

    申请日：2009-11-05

    申请人： Philipp Stössel ,  Ingrid Bach ,  Hubert Spreitzer ,  Heinrich Becker

    发明人： Philipp Stössel ,  Ingrid Bach ,  Hubert Spreitzer ,  Heinrich Becker

    IPC分类号： C07F15/00

    CPC分类号： C07F15/0073 ,  C07F15/0033 ,  H01L51/0085 ,  H01L51/5012 ,  Y02E10/549 ,  Y02P70/521 ,  Y10S428/917

    摘要： The present invention describes novel organometallic compounds which are phosphorescence emitters. Such compounds can, as active constituents (=functional materials), be used in a number of different applications, which in the broadest sense can be classed as belonging to the electronics industry.The compounds according to the invention are described by the formulas (I), (Ia), (II), (IIa), (III), (IIIa), (IV) and (IVa).

    摘要翻译： 本发明描述了作为磷光发射体的新型有机金属化合物。 作为活性组分（=功能材料），这些化合物可以用于许多不同的应用中，其在最广泛的意义上可被归类为属于电子工业。 根据本发明的化合物由式（I），（Ia），（II），（IIa），（III），（IIIa），（IV）和（IVa）描述。

    Aryl-substituted poly (p-arylene-vinylenes), process for their preparation and their use in electroluminescence components
    24.
    发明授权
    Aryl-substituted poly (p-arylene-vinylenes), process for their preparation and their use in electroluminescence components 失效
    芳基取代的聚（对亚芳基 - 亚乙烯基），其制备方法及其在电致发光组分中的应用

    公开(公告)号：US06458909B1

    公开(公告)日：2002-10-01

    申请号：US08991559

    申请日：1997-12-16

    申请人： Hubert Spreitzer ,  Willi Kreuder ,  Heinrich Becker ,  Harmannus Schoo ,  Robert Demandt

    发明人： Hubert Spreitzer ,  Willi Kreuder ,  Heinrich Becker ,  Harmannus Schoo ,  Robert Demandt

    IPC分类号： C08F13800

    CPC分类号： H01L51/5012 ,  C08G61/02 ,  C09B69/105 ,  C09K11/06 ,  H01L51/0038

    摘要： Poly(p-arylene-vinylenes) comprising repeating units of the formula (I), where the symbols and indices have the following meanings: Y1, Y2, Y3: identical or different, CH, N; Aryl: an aryl group having from 4 to 14 carbon atoms; R′, R″: identical or different, each a straight-chain or branched or cyclic alkyl or alkoxy group having from 1 to 20 carbon atoms, where one or more non-adjacent CH2 groups may be replaced by —O—, —S—, —CO—, —COO—, —O—CO—, —NR1—, —(NR2R3)+—A−, or —CONR4— and one or more H atoms may be replaced by F, or else CN, F, Cl or an aryl group having from 4 to 14 carbon atoms which may be substituted by one or more nonaromatic radicals R′; R1, R2, R3, R4: identical or different, aliphatic or aromatic hydrocarbon radicals having from 1 to 20 carbon atoms or else H; A−: a singly charged anion or its equivalent; m: 0, 1 or 2; n: 1, 2, 3, 4 or 5; are suitable as electroluminescence materials.

    摘要翻译： 包含式（I）重复单元的聚（对亚芳基 - 烯烃），其中符号和指数具有以下含义：Y1，Y2，Y3：相同或不同，CH，N;芳基：具有4 至14个碳原子; R'，R“：相同或不同，各自为具有1至20个碳原子的直链或支链或环状烷基或烷氧基，其中一个或多个不相邻的CH 2基团可以被 -O-，-S-，-CO-，-COO-，-O-CO-，-NR1-， - （NR2R3）+ -A-或-CONR4-，一个或多个H原子可被F ，或CN，F，Cl或具有4至14个碳原子的芳基，其可以被一个或多个非芳族基团R 1取代; R 1，R 2，R 3，R 4：相同或不同的脂族或芳族烃基，其具有 1至20个碳原子或H; A-：单电荷阴离子或其等价物; m：0,1或2; n：1,2,3,4或5;适合作为电致发光材料。

    Rhodium and iridium complexes
    25.
    发明授权
    Rhodium and iridium complexes 失效
    铑和铱络合物

    公开(公告)号：US07534853B2

    公开(公告)日：2009-05-19

    申请号：US11272404

    申请日：2005-11-10

    申请人： Philipp Stössel ,  Hubert Spreitzer ,  Heinrich Becker

    发明人： Philipp Stössel ,  Hubert Spreitzer ,  Heinrich Becker

    IPC分类号： C08G73/06 ,  B32B9/00

    CPC分类号： C07F15/008 ,  C07F15/004 ,  Y10S428/917

    摘要： The present invention describes novel organometallic compounds which are phosphorescence emitters. Such compounds can be used as active components (=functional materials) in a series of different types of application which can be classed within the electronics industry in the broadest sense.The compounds according to the invention are described by the formulae (I), (Ia), (II) and (IIa).

    摘要翻译： 本发明描述了作为磷光发射体的新型有机金属化合物。 这些化合物可以用作一系列不同类型应用中的活性组分（=功能材料），其可以在最广泛的意义上在电子工业中分类。 根据本发明的化合物由式（I），（Ia），（II）和（IIa）描述。

    Method for producing olefin-substituted aromatic or heteroaromatic compounds
    26.
    发明授权
    Method for producing olefin-substituted aromatic or heteroaromatic compounds 失效
    制备烯烃取代芳族或杂芳族化合物的方法

    公开(公告)号：US07402717B2

    公开(公告)日：2008-07-22

    申请号：US10343291

    申请日：2001-08-01

    申请人： Hubert Spreitzer ,  Philipp Stössel ,  Heinrich Becker

    发明人： Hubert Spreitzer ,  Philipp Stössel ,  Heinrich Becker

    IPC分类号： C07C2/72 ,  C07C2/64 ,  C07C2/68

    CPC分类号： C07C29/44 ,  C07B37/04 ,  C07C1/26 ,  C07C2603/18 ,  C07C2603/94 ,  C07C13/72 ,  C07C33/28

    摘要： Both low molecular weight and high molecular weight aromatic and heteroaromatic compounds which are substituted by olefins play an important role in industry, for instance as assistants and additives in cosmetic preparations, for example in sunscreens, various fine and electronics chemicals, and precursors for pharmaceuticals and agrochemicals. Also, particularly in the rapidly growing field of organic semiconductors (for example applications in organic or polymeric light emitting diodes, organic solar cells, organic ICs), precisely these compounds are of outstanding significance.The present invention relates to a process for preparing such olefin-substituted aromatics or heteroaromatics by reacting a functional aryl or heteroaryl compound with an olefin derivative which has at least one hydrogen atom on the double bond in the presence of a simple palladium compound, optionally in the presence of a nitrogen additive, and of a base in a solvent, to form a C—C bond and formally cleave off the functional group of the aryl or heteroaryl derivative and a hydrogen atom of the olefin compound, characterized by the presence of at least one metal additive other than palladium.

    摘要翻译： 由烯烃取代的低分子量和高分子量芳族和杂芳族化合物在工业中起重要作用，例如作为化妆品制剂中的助剂和添加剂，例如防晒剂，各种精细和电子化学品以及用于药物和 农药。 此外，特别是在快速增长的有机半导体领域（例如有机或聚合物发光二极管中的应用，有机太阳能电池，有机IC）中，精确地这些化合物具有突出的意义。 本发明涉及通过使官能的芳基或杂芳基化合物与单键钯化合物存在下在双键上具有至少一个氢原子的烯烃衍生物反应来制备这种烯烃取代芳族化合物或杂芳族化合物的方法，任选地 在溶剂中存在氮添加剂和碱，以形成CC键并正式地断开芳基或杂芳基衍生物的官能团和烯烃化合物的氢原子，其特征在于存在至少一种 除钯以外的金属添加剂。

    Substituted poly(arylenevinylenes), process for their preparation, and their use in electroluminescent elements
    29.
    发明授权
    Substituted poly(arylenevinylenes), process for their preparation, and their use in electroluminescent elements 有权
    取代的聚（亚芳基亚乙烯基），其制备方法及其在电致发光元件中的应用

    公开(公告)号：US06638646B2

    公开(公告)日：2003-10-28

    申请号：US10185061

    申请日：2002-06-28

    申请人： Hubert Spreitzer ,  Willi Kreuder ,  Heinrich Becker ,  Hermann Schenk ,  Nu Yu

    发明人： Hubert Spreitzer ,  Willi Kreuder ,  Heinrich Becker ,  Hermann Schenk ,  Nu Yu

    IPC分类号： H05B3300

    CPC分类号： H01L51/0038 ,  C08G61/02 ,  C09K11/06 ,  H01B1/128 ,  H01L51/5012 ,  H05B33/14 ,  Y10S428/917

    摘要： Poly(arylenevinylenes) comprising at least 20% of recurring units of the formula (I), where the symbols and indices have the following meanings: Aryl: is an aryl group having 4 to 14 carbon atoms; R′: is a substituent which is either in the labeled phenylene position 5 or 6 and is CN, F, Cl, N(R1R2) or a straight-chain, branched or cyclic alkyl, alkoxy or thioalkoxy group having 1 to 20 carbon atoms, in which, in addition, one or more H atoms may be replaced by F; R″: are identical or different and are CN, F, Cl or a straight-chain, branched or cyclic alkyl or alkoxy group having 1 to 20 carbon atoms, where one or more non-adjacent CH2 groups may be replaced by —O—, —S—, —CO—, —COO—, —O—CO—, —NR1—, —(NR2R3)+—A− or —CONR4—, and where one or more H atoms may be replaced by F, or an aryl group having 4 to 14 carbon atoms, which may be substituted by one or more non-aromatic radicals R′; R1, R2, R3, R4 are identical or different and are H or an aliphatic or aromatic hydrocarbon radical having 1 to 20 carbon atoms; A−: is a singly charged anion or an equivalent thereof; and n: is 0, 1, 2, 3, 4 or 5, are suitable as electroluminescent material.

    摘要翻译： 包含至少20％式（I）的重复单元的聚（亚芳基亚乙烯基烯烃），其中符号和指数具有以下含义：芳基：具有4至14个碳原子的芳基; R'是 在标记的亚苯基位置5或6中，是CN，F，Cl，N（R 1 R 2）或具有1至20个碳原子的直链，支链或环烷基，烷氧基或硫代烷氧基， 其中，另外一个或多个H原子可被F取代; R“：相同或不同，为CN，F，Cl或具有1至20个碳的直链，支链或环状烷基或烷氧基 原子，其中一个或多个不相邻的CH 2基团可被-O - ， - S - ， - CO - ， - COO - ， - O-CO - ， - NR 1 - ， - （NR 2） R 3）+ - 或-CONR 4 - ，并且其中一个或多个H原子可以被F取代，或者可以被4〜14个碳原子的芳基取代，可以被 一个或多个非芳族基团R'; R 1，R 2，R 3，R 4相同或不同，为H或脂族或芳族氢 具有1至20个碳原子的羰基; A 1是单电荷阴离子或其等同物; 和n为0,1,2,3,4或5，适合作为电致发光材料。