公开(公告)号：US5138108A

公开(公告)日：1992-08-11

申请号：US776018

申请日：1991-10-15

申请人： Gerald C. Tustin ,  Joseph F. Jeter ,  Richard I. Garrity

发明人： Gerald C. Tustin ,  Joseph F. Jeter ,  Richard I. Garrity

IPC分类号： C07B61/00 ,  B01J29/90 ,  B01J38/64 ,  C07C17/12 ,  C07C17/156 ,  C07C25/22

CPC分类号： C07C17/12 ,  B01J29/90 ,  B01J38/64 ,  Y02P20/584

摘要： Disclosed is a process for regeneration of a 13X zeolite catalyst comprising conducting the following steps within the regeneration zone wherein the 13X zeolite is located.(1) Applying vacuum or delivering a source of molecular oxygen or inert gas at a temperature above 100.degree. C. to remove a portion of the volatile compounds from the 13X zeolite,(2) Cooling the 13X zeolite to a temperature below 100 degrees C.,(3) Contacting the 13X zeolite with an aqueous solution having a pH in the range of 7 to 14,(4) Drying the 13X zeolite,(5) Delivering an oxygen containing calcination gas to the regeneration zone and heating the 13X zeolite to a temperature in the range of 350.degree. to 450.degree. C.,(6) Cooling the 13X zeolite to a temperature below 100 degrees C., and(7) Contacting the 13X zeolite with an aqueous solution having a pH in the range of 7 to 14.

摘要翻译： 公开了一种13X沸石催化剂再生方法，包括在13X沸石所在的再生区内进行以下步骤。 （1）在高于100℃的温度下施加真空或输送分子氧或惰性气体源以从13X沸石中除去一部分挥发性化合物，（2）将13X沸石冷却到低于100℃的温度 （3）将13X沸石与pH为7〜14的水溶液接触，（4）干燥13X沸石，（5）将含氧的煅烧气体送入再生区并加热13X沸石 温度在350-450℃的范围内;（6）将13X沸石冷却到低于100℃的温度，和（7）将13X沸石与pH范围内的水溶液接触， 7到14。