High pressure reaction vessel for growing diamond on diamond seed and
method therefor
    31.
    发明授权
    High pressure reaction vessel for growing diamond on diamond seed and method therefor 失效
    用于在钻石种子上生长钻石的高压反应容器及其方法

    公开(公告)号:US4322396A

    公开(公告)日:1982-03-30

    申请号:US148213

    申请日:1980-05-09

    Abstract: Reaction vessel construction is described for suppressing spontaneous diamond nucleation and simultaneously reducing the flaw content in the main body of diamond grown from diamond seed material by the process broadly disclosed in U.S. Pat. No. 3,297,407 to Wentorf, Jr.In the reaction vessel construction the body of catalyst-solvent metal is formed with at least one small tip projecting from the underside thereof. A single diamond seed is placed in contact with this (or each) tip. The underside of the plug of catalyst-solvent metal is in contact with a nucleation-suppressing disc, or layer, of a material different from the catalyst-solvent and selected from a specific group of materials. In each case the tip of catalyst-solvent metal projects through a hole in the disc or layer to make contact with the diamond seed material.

    Abstract translation: 描述了用于抑制自发金刚石成核并同时降低由金刚石种子材料生长的金刚石的主体中的缺陷含量的反应容器结构,这通过美国专利中广泛公开的方法。 在Wentorf,Jr.的第3,297,407号中,在反应容器结构中,催化剂 - 溶剂金属体形成有从其下侧突出的至少一个小尖端。 单个金刚石种子与该(或每个)尖端接触。 催化剂 - 溶剂金属的塞子的下侧与不同于催化剂 - 溶剂并选自特定材料组的材料与成核抑制盘或层接触。 在每种情况下,催化剂 - 溶剂金属的尖端通过盘或层中的孔突出以与金刚石种子材料接触。

    Process for synthesizing diamonds
    33.
    发明授权
    Process for synthesizing diamonds 失效
    合成钻石的工艺

    公开(公告)号:US4128625A

    公开(公告)日:1978-12-05

    申请号:US841715

    申请日:1977-10-13

    Inventor: Hiroshi Ishizuka

    CPC classification number: B01J3/062 B01J2203/061 B01J2203/0655 B01J2203/068

    Abstract: A process for synthesizing larger size diamonds wherein a raw material carbon substance and a solvent-catalyst metal initially isolated from the carbon substance by a metal having no affinity to carbon are subjected to high pressure-high temperature conditions within a diamond-stable region calculated and defined by a specific combination of the carbon substance and solvent-catalyst metal to temporarily restrict nucleation at the reaction earlier stage to control the number of diamond crystal nucleuses.

    Abstract translation: 一种合成大尺寸金刚石的方法,其中原料碳物质和最初通过不与碳的亲合性的金属从碳物质分离的溶剂 - 催化剂金属在计算的金刚石稳定区域内经受高压高温条件, 由碳物质和溶剂 - 催化剂金属的特定组合限定,以暂时限制反应较早阶段的成核以控制金刚石晶核的数目。

    Method for producing synthetic diamonds
    34.
    发明授权
    Method for producing synthetic diamonds 失效
    生产合成钻石的方法

    公开(公告)号:US4005180A

    公开(公告)日:1977-01-25

    申请号:US543871

    申请日:1975-01-24

    CPC classification number: C01B31/06 B01J3/062 B01J2203/0655 B01J2203/068

    Abstract: This invention relates to the synthesis of diamond by subjecting a carbon-containing composition substantially free of carbon-hydrogen covalent bonds to conditions of temperature and pressure such as to cause decomposition of the composition to release carbon atoms or groups of carbon atoms and effect conversion of the released carbon atoms or groups of carbon atoms into diamond. The preferred compositions are halogenated compounds, particularly hexachlorobenzene, hexachloroethane and tetrachloroquinone.

    Abstract translation: 本发明涉及通过使基本上不含碳 - 氢共价键的含碳组合物在温度和压力条件下进行合成,以使组合物分解以释放碳原子或碳原子基团并实现转化 释放出的碳原子或碳原子团成金刚石。 优选的组合物是卤代化合物,特别是六氯苯,六氯乙烷和四氯醌。

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