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公开(公告)号：US10577295B2
公开(公告)日：2020-03-03
申请号：US15852794
申请日：2017-12-22
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Haiyou Wang , Hsueh Sung Tung
IPC: C07C17/25 , C07C21/18 , B01J27/128 , B01J27/132 , B01J27/10 , B01J27/06 , B01J27/12 , B01J27/138 , B01J21/18 , B01J21/10 , B01J21/04
Abstract: The present invention relates, at least in part, to a process for making chlorotrifluoroethylene (CFO-1113) from 1,2-dichloro-1,1,2-trifluoroethane (HCFC-123a). In certain aspects, the process includes dehydrochlorinating 1,2-dichloro-1,1,2-trifluoroethane (HCFC-123a) in the presence of a catalyst selected from the group consisting of (i) one or more metal halides; (ii) one or more halogenated metal oxides; (iii) one or more zero-valent metals or metal alloys; (iv) combinations thereof.
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公开(公告)号：US10427999B2
公开(公告)日：2019-10-01
申请号：US15450367
申请日：2017-03-06
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Haiyou Wang , Hsueh Sung Tung , Rajiv R. Singh , Ian Shankland
IPC: C07C19/08 , C07C17/04 , C07C17/25 , C07C17/383 , C07C17/395 , C07C21/18
Abstract: The present invention discloses a manufacturing process to produce high purity 1234yf from 245eb, which preferably includes the removal of impurities present in 245eb raw material, the dehydrofluorination of 245eb, and the removal of impurities present in final crude product. The disclosed manufacturing process allows the production of a 1234yf product with lower the levels of 1225ye and/or trifluoropropene, preferably in amounts of less than about 500, and 50 ppm, respectively.
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公开(公告)号：US10414705B2
公开(公告)日：2019-09-17
申请号：US15420574
申请日：2017-01-31
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Haiyou Wang , Hsueh Sung Tung , Rajiv R. Singh , Ian Shankland
IPC: C07C19/08 , C07C17/04 , C07C17/25 , C07C17/383 , C07C17/395 , C07C21/18
Abstract: The present invention discloses a manufacturing process to produce high purity 1234yf from 245eb, which preferably includes the removal of impurities present in 245eb raw material, the dehydrofluorination of 245eb, and the removal of impurities present in final crude product. The disclosed manufacturing process allows the production of a 1234yf product with lower the levels of 1225ye and/or trifluoropropene, preferably in amounts of less than about 500, and 50 ppm, respectively.
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公开(公告)号：US10343962B2
公开(公告)日：2019-07-09
申请号：US15464439
申请日：2017-03-21
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Selma Bektesevic , Daniel C. Merkel , Mario Joseph Nappa , Xuehui Sun , Hsueh Sung Tung , Haiyou Wang
Abstract: The present invention relates, in part, to the discovery that, during the fluorination of certain fluoroolefin starting reagents, particularly, 1,1,2,3-tetrachloropropene (1230xa), oligomerization/polymerization of such starting reagents reduces the conversion process and leads to increased catalyst deactivation. The present invention also illustrates that providing one or more organic co-feed to the fluooolefin starting stream reduces such oligomerization/polymerization and improves catalystic stability.
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45.发明授权公开(公告)号：US10099977B2
公开(公告)日：2018-10-16
申请号：US15267599
申请日：2016-09-16
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Haiyou Wang , Hsueh Sung Tung
IPC: C07C21/18 , C07C17/087 , C07C17/25 , C07C17/389
Abstract: Disclosed is a composition comprised of at least one compound selected from 2,3,3,3-tetrafluoropropene, 1,3,3,3-tetrafluoro-1-propene and 1-chloro-3,3,3-trifluoropropene and halogenated impurity selected from the group consisting of HFO-1141 (CH2═CHF), HCFO-1140 (CH2═CHCl), and HCFO-1131 (CH2═CFCl and/or trans/cis-CHF═CHCl) and combination thereof, said halogenated impurity being present in said composition in an amount of 50 ppm or less.
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Patent Agency Ranking
公开(公告)号：US10011546B2
公开(公告)日：2018-07-03
申请号：US15095247
申请日：2016-04-11
Applicant: Honeywell International Inc.
Inventor： Daniel C. Merkel , Hsueh Sung Tung , Konstantin A. Pokrovski , Haiyou Wang , Stephen A. Cottrell , Hang T. Pham
Abstract: Provided are azeotropic or azeotrope-like mixtures of 1,1,3,3-tetrachloroprop-1-ene (HCO-1230za) and hydrogen fluoride. Such compositions are useful as feed stock in the production of HFC-245fa and HCFO-1233zd.
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公开(公告)号：US09764998B2
公开(公告)日：2017-09-19
申请号：US15088599
申请日：2016-04-01
Applicant: Honeywell International Inc.
Inventor： Haiyou Wang , Hsueh Sung Tung , Stephen A. Cottrell
Abstract: Disclosed is a process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) which includes reacting a propane feedstock comprising tetrachlorofluoropropanes, trichlorodifluoropropanes, dichlorotrifluoropropanes, or a mixture thereof, in the presence of a solid catalyst. The process generally comprises the following four steps: (i) providing a propane feedstock comprising trichlorodifluoropropanes and dichlorotrifluoropropanes, (ii) reacting the feedstock in a vapor phase reactor in the presence of HF and in the presence of a solid catalyst under conditions effective to form a product stream comprising HCFO-1233zd and unconverted starting materials, (iii) recovering or removing HCl and HF, and (iv) isolating HCFO-1233zd(E), HCFO-1233zd(Z), or both.
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48.发明授权Methods for removing halogenated ethylene impurities in 2,3,3,3-tetrafluoropropene product 有权在2,3,3,3-四氟丙烯产物中除去卤代乙烯杂质的方法公开(公告)号：US09447004B2
公开(公告)日：2016-09-20
申请号：US14206026
申请日：2014-03-12
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Haiyou Wang , Hsueh Sung Tung
IPC: C07C17/38 , C07C17/20 , C07C17/00 , C07C17/389 , C07C17/087 , C07C17/25
CPC classification number: C07C21/18 , C07B2200/09 , C07C17/087 , C07C17/25 , C07C17/389 , Y02P20/582 , C07C19/10
Abstract: The present process relates to a process comprising: contacting a mixture comprising 2,3,3,3-tetrafluoropropene and at least one halogenated ethylene impurity with at least one adsorbent or at least one chemisorption catalyst to reduce the concentration of said at least one halogenated ethylene impurity.
Abstract translation: 本方法涉及一种方法，其包括：使包含2,3,3,3-四氟丙烯和至少一种卤代乙烯杂质的混合物与至少一种吸附剂或至少一种化学吸附催化剂接触以降低所述至少一种卤化 乙烯杂质。
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公开(公告)号：US20160237010A1
公开(公告)日：2016-08-18
申请号：US15139778
申请日：2016-04-27
Applicant: Honeywell International, Inc.
Inventor： Daniel C. Merkel , Hsueh Sung Tung , Haiyou Wang , Haluk Kopkalli , Yuon Chiu
CPC classification number: B01J19/24 , B01J4/002 , C07C17/206 , C07C17/25 , C07C21/18
Abstract: The invention relates to a process to prepare tetrahalopropenes, such as 2-chloro-3,3,3-trifluoropropene (1233xf). The process comprises atomizing a feed material, such as 1,1,2,3-tetrachloropropene (1230xa) and the like, and mixing it with superheated HF to form a vaporized composition of feed material and HF with substantially instantaneous contact with a vapor phase fluorination catalyst. The invention extends catalyst life and forestalls catalyst deactivation.
Abstract translation: 本发明涉及制备四卤代丙烯的方法，例如2-氯-3,3,3-三氟丙烯（1233xf）。 该方法包括将原料如1,1,2,3-四氯丙烯（1230xa）等进行雾化，并与过热HF混合以形成与气相基本上瞬时接触的原料和HF的蒸发组合物 氟化催化剂。 本发明延长了催化剂的寿命并阻止了催化剂的失活。
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公开(公告)号：US09416074B2
公开(公告)日：2016-08-16
申请号：US14351688
申请日：2012-10-10
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Haiyou Wang , Hsueh Sung Tung , Daniel C. Merkel
IPC: C07C17/00 , C07C17/38 , C07C17/25 , C07C17/087 , C07C17/20
CPC classification number: C07C17/25 , C07C17/087 , C07C17/202 , C07C19/10 , C07C21/18
Abstract: The present invention relates, in part, to the discovery that the presence of impurities in a reactor for dehydrochlorinating HCFC-244bb to HFO-1234yf results in a reduced conversion rate and/or a selectivity changeover from HFO-1234yf to HCFO-1233xf. By substantially removing such impurities, it is shown that the conversion rate may be improved and selectivity to HFO-1234yf via dehydrochlorination of HCFC-244bb is also improved.
Abstract translation: 本发明部分涉及以下发现，即将HCFC-244bb脱氯化氢反应成HFO-1234yf的反应器中的杂质的存在导致从HFO-1234yf到HCFO-1233xf的转化率和/或选择性转换率降低。 通过基本上除去这些杂质，可以看出可以提高转化率，并且通过HCFC-244bb的脱氯化氢还能改善对HFO-1234yf的选择性。
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