Hydroxygallium phthalocyanine crystal, and electro-photographic
photoreceptor containing the same
    41.
    发明授权
    Hydroxygallium phthalocyanine crystal, and electro-photographic photoreceptor containing the same 失效
    羟基镓酞菁晶体和含有它们的电照相感光体

    公开(公告)号:US5756247A

    公开(公告)日:1998-05-26

    申请号:US862704

    申请日:1997-05-23

    摘要: Hydroxygallium phthalocyanine crystals having intense diffraction peaks at Bragg angles (2.theta..+-.0.2.degree.) of 7.5.degree., 9.9.degree., 12.5.degree., 16.3.degree., 18.6.degree., 25.1.degree. and 28.3.degree. in Cuk.alpha. characteristic X-ray diffractometry, a process for producing the same, and an electrophotographic photoreceptor containing the same are disclosed. The hydroxygallium phthalocyanine crystals are obtained by once preparing impurity-free hydroxygallium phthalocyanine having intense X-ray diffraction peaks at specific Bragg angles, followed by a solvent treatment for crystal transformation, in which the impurity-free crystals are prepared by using excess phthalocyanine ring-forming compound in the synthesis of starting gallium phthalocyanine or by removing insoluble matter from the acid paste of starting gallium phthalocyanine.

    摘要翻译: 在Cuk alpha特征X射线衍射中,在7.5°,9.9°,12.5°,16.3°,18.6°,25.1°和28.3°的布拉格角(2θ+/- 0.2°)处具有强衍射峰的羟基镓酞菁晶体, 公开了含有该电子照相感光体的电子照相感光体。 羟基镓酞菁晶体通过一次制备在特定布拉格角具有强X射线衍射峰的无杂质的羟基镓酞菁,然后进行晶体转变的溶剂处理,其中通过使用过量的酞菁环 - 在起始镓酞菁的合成中形成化合物,或者从起始镓酞菁的酸性糊中除去不溶物。

    Electrophotographic toner, manufacture of the same, electrostatic latent image developer, and image forming method
    44.
    发明授权
    Electrophotographic toner, manufacture of the same, electrostatic latent image developer, and image forming method 有权
    电子照相调色剂,其制造,静电潜像显影剂和成像方法

    公开(公告)号:US06864029B2

    公开(公告)日:2005-03-08

    申请号:US10307313

    申请日:2002-12-02

    IPC分类号: G03G9/08 G03G9/087 G03G15/20

    摘要: The present invention uses a crystalline resin as a binding resin and provides a toner insuring excellent storability of a resulting image, a method of manufacturing the toner, an electrostatically charged image developer containing the toner, and an image forming method. In the electrophotographic toner containing toner mother particles comprising at least a binding resin and a colorant, a main component of said binding resin comprises a crystalline resin with a melting point in the range from 50 to 120° C. and an average volume particle size in the range from 3.0 to 7.5 μm, while an average value of the BET specific areas of said toner mother particles is in the range from 0.6 to 3.0 m2/g. The electrophotographic toner manufacturing method comprises the steps of coalescing or associating the binding resin particles with colorant particles, and cooling the aggregated particles at the rate of at least 1° C. per minute or more to a temperature below the crystallizing temperature of the binding resin to generate toner particles.

    摘要翻译: 本发明使用结晶树脂作为粘合树脂,并提供确保所得图像的优异保存性的调色剂,调色剂的制造方法,含有调色剂的带静电电荷的图像显影剂和图像形成方法。 在含有至少包含粘合树脂和着色剂的调色剂母体颗粒的电子照相调色剂中,所述粘合树脂的主要成分包括熔点在50-120℃范围内的结晶树脂,平均体积粒径 3.0至7.5μm的范围,而所述调色剂母粒的BET比表面积的平均值在0.6-3.0m 2 / g的范围内。 电子照相调色剂制造方法包括以下步骤:将结合树脂颗粒与着色剂颗粒聚结或结合,并且以至少1℃/分钟或更高的速率将聚集颗粒冷却至低于粘合树脂的结晶温度的温度 以产生调色剂颗粒。

    Hydroxygallium phthalocyanine crystal, process for producing the same,
and electrophotographic photoreceptor containing the same
    46.
    发明授权
    Hydroxygallium phthalocyanine crystal, process for producing the same, and electrophotographic photoreceptor containing the same 失效
    羟基镓酞菁晶体,其制造方法和含有它们的电子照相感光体

    公开(公告)号:US5663327A

    公开(公告)日:1997-09-02

    申请号:US536786

    申请日:1995-09-29

    摘要: Hydroxygallium phthalocyanine crystals having intense diffraction peaks at Bragg angles (2.theta..+-.0.2.degree.) of 7.5.degree., 9.9.degree., 12.5.degree., 16.3.degree., 18.6.degree., 25.1.degree. and 28.3.degree. in CuK.alpha. characteristic X-ray diffractometry, a process for producing the same, and an electrophotographic photoreceptor containing the same are disclosed. The hydroxygallium phthalocyanine crystals are obtained by once preparing impurity-free hydroxygallium phthalocyanine having intense X-ray diffraction peaks at specific Bragg angles, followed by a solvent treatment for crystal transformation, in which the impurity-free crystals are prepared by using excess phthalocyanine ring-forming compound in the synthesis of starting gallium phthalocyanine or by removing insoluble matter from the acid paste of starting gallium phthalocyanine.

    摘要翻译: 在CuKα特征X射线衍射中,在7.5°,9.9°,12.5°,16.3°,18.6°,25.1°和28.3°的布拉格角(2θ+/- 0.2°)处具有强衍射峰的羟基镓酞菁晶体, 公开了含有该电子照相感光体的电子照相感光体。 羟基镓酞菁晶体通过一次制备在特定布拉格角具有强X射线衍射峰的无杂质的羟基镓酞菁,然后进行晶体转变的溶剂处理,其中通过使用过量的酞菁环 - 在起始镓酞菁的合成中形成化合物,或者从起始镓酞菁的酸性糊中除去不溶物。