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71.发明授权Films from aqueous dispersions of block copolymers having hydrogenated conjugated diene block 失效具有氢化共轭二烯嵌段的嵌段共聚物的水性分散体的膜
公开(公告)号：US5567760A
公开(公告)日：1996-10-22
申请号：US339862
申请日：1994-11-15
申请人： Brian W. Walther , Gary R. Marchand
发明人： Brian W. Walther , Gary R. Marchand
CPC分类号： C08J5/18 , C08J3/07 , C08L53/02 , C08J2353/02
摘要： Aqueous dispersions, and films prepared therefrom, comprising an organic phase of block copolymers and optional extenders wherein the block copolymers corresponds to the formula:A-B-X.sub.m -(B-A).sub.nwherein each A is a polymer block of a monovinylidene aromatic monomer and conjugated dienes, each B is a polymer block of one or more conjugated dienes and, optionally, one or more monovinylidene aromatic monomers, X is the remnant of a multifunctional coupling agent, m is 0 or 1, and n is an integer from 1 to 5. Each A polymer block has a weight average molecular weight from 4,000 to 15,000 Daltons. Each B polymer block has a weight average molecular weight from 20,000 to 200,000 Daltons. The total monovinylidene monomer content is from 6 to 30 percent by weight of the organic phase. The effective phase volume of the A polymer block in the organic phase is from 8 to 20 percent. Thin elastomeric articles prepared from the emulsions have improved tensile strength properties. Also claimed is a process for the preparation of such films.
摘要翻译： 水分散体和由其制备的膜包含嵌段共聚物和任选的增量剂的有机相，其中嵌段共聚物对应于下式：AB-Xm-（BA）n，其中每个A是单亚乙烯基芳族单体和共轭二烯的聚合物嵌段， 每个B是一种或多种共轭二烯和任选的一种或多种单亚乙烯基芳族单体的聚合物嵌段，X是多官能偶联剂的残余物，m是0或1，n是1至5的整数。 聚合物嵌段具有4,000至15,000道尔顿的重均分子量。 每个B聚合物嵌段的重均分子量为20,000至200,000道尔顿。 总亚乙烯基单体含量为有机相重量的6至30％。 有机相中的A聚合物嵌段的有效相体积为8〜20％。 由乳液制备的薄弹性制品具有改进的拉伸强度性能。 还要求的是制备这种膜的方法。
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公开(公告)号：US5286457A
公开(公告)日：1994-02-15
申请号：US858812
申请日：1992-03-27
CPC分类号： B01J19/002 , B01J19/18 , B01J2219/00094 , B01J2219/00768 , B01J2219/185
摘要： A reactor for the solution polymerization of volatile monomers equipped with an agitator to cause splashing and droplet formation to reduce volatile monomer accumulation in the vapor space.
摘要翻译： 用于溶液聚合的反应器，用于配备搅拌器的挥发性单体以引起飞溅和液滴形成，以减少挥发性单体在蒸气空间中积累。
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公开(公告)号：US5225493A
公开(公告)日：1993-07-06
申请号：US936188
申请日：1992-08-26
摘要： A process for anionic polymerization of polymerizable monomers with an organo lithium initiator followed by polymerization termination characterized in that terminated reaction products are neutralized by contacting with sulfuric acid, phosphoric acid or a mixture thereof.
摘要翻译： 一种可聚合单体与有机锂引发剂进行阴离子聚合的方法，随后进行聚合终止，其特征在于通过与硫酸，磷酸或其混合物的接触中和终止的反应产物。
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公开(公告)号：US5120805A
公开(公告)日：1992-06-09
申请号：US710632
申请日：1991-06-05
CPC分类号： B01J19/002 , B01J19/18 , B01J2219/00094 , B01J2219/00768 , B01J2219/185
摘要： A process for the solution polymerization of volatile monomers in a reactor equipped with an agitator to cause splashing and droplet formation to reduce volatile monomer accumulation in the vapor space.
摘要翻译： 在装有搅拌器的反应器中使挥发性单体溶液聚合以引起飞溅和液滴形成以减少挥发性单体在蒸气空间中积累的方法。
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公开(公告)号：US5089572A
公开(公告)日：1992-02-18
申请号：US395176
申请日：1989-08-18
CPC分类号： C07B61/00 , C08F8/42 , Y10S526/912
摘要： A process for blanking a reaction mixture utilizing as a blanking agent a difunctional lithium composition.
摘要翻译： 使用二官能锂组合物作为消隐剂冲洗反应混合物的方法。
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公开(公告)号：US5045612A
公开(公告)日：1991-09-03
申请号：US510492
申请日：1990-04-18
CPC分类号： C08F10/00
摘要： Olefins are polymerized under solution polymerization conditions in the presence of the solid catalytic product resulting from removing the liquid components from the product resulting from admixing in an inert diluent and in an atmosphere which excludes moisture and oxygen (A) at least one hydrocarbon soluble organomagnesium compound; (B) at least one organic hydroxyl-containing compound; (C) at least one reducing halide source; (D) at least one transition metal (Tm) alkoxide.
摘要翻译： 烯烃在溶液聚合条件下在固体催化剂存在下进行聚合，这是由惰性稀释剂和不含水分和氧气的气氛中除去来自产物的液体组分得到的（A）至少一种可溶于烃的有机镁化合物 ; （B）至少一种含有机羟基化合物; （C）至少一种还原卤素源; （D）至少一种过渡金属（Tm）醇盐。
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77.发明授权Polymerization of olefins in the presence of a catalyst prepared from an inorganic oxide which has not been heat or chemically treated, organomagnesium compound, organic hydroxyl-containing compound, reducing halide and transition metal compound 失效在由尚未加热或化学处理的无机氧化物制备的催化剂存在下烯烃的聚合，有机镁化合物，含有机羟基化合物，还原卤化物和过渡金属化合物
公开(公告)号：US4910272A
公开(公告)日：1990-03-20
申请号：US277624
申请日：1988-11-29
CPC分类号： C08F10/00
摘要： A catalyst for polymerizing olefins is the product resulting from mixing in an inert hydrocarbon diluent, a mixture of (A) an inorganic oxide, (B) an organomagnesium material, (C) an organic hydroxyl-containing material, (D) a reducing halide source, and (E) a transistion metal compound.
摘要翻译： 用于聚合烯烃的催化剂是通过在惰性烃稀释剂中混合的产物，（A）无机氧化物，（B）有机镁材料，（C）含有机羟基材料的混合物，（D）还原卤化物 源和（E）转移金属化合物。
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