METHODS AND DEVICES FOR DETECTING MERCURY ISOTOPES IN CRUDE OIL

    公开(公告)号:US20200132659A1

    公开(公告)日:2020-04-30

    申请号:US16389481

    申请日:2019-04-19

    Abstract: The present disclosure relates to a method and device for detecting mercury isotopes in crude oil. The device comprises an enrichment-absorption system and a secondary purification-enrichment system for mercury isotopes, wherein the enrichment-absorption system includes an air-background mercury absorption system, a pyrolysis/cracking system, a mercury-sample absorption system connected in series with pipe lines, and a vacuum pump, and the vacuum pump is connected to the mercury-sample absorption system through a pipe line; the secondary purification-enrichment system includes a nitrogen-gas cylinder, a collection bottle with potassium permanganate absorption liquid, and a secondary enrichment-absorption bottle connected in series with pipe lines, wherein the secondary purification-enrichment system further includes a stannous-chloride storage bottle, which is connected to a pipe line between the nitrogen-gas cylinder and the collection bottle with potassium-permanganate absorption liquid via a peristaltic pump and through a pipe line.

    Nanostructured titanic acid salts and preparation process and use thereof

    公开(公告)号:US20200071183A1

    公开(公告)日:2020-03-05

    申请号:US16554862

    申请日:2019-08-29

    Abstract: The present invention provides a nanostructured titanic acid salt and a preparation process and use thereof. The process comprises preparing a dispersion containing titanium peroxy complex; slowly adding a metal compound to the dispersion containing the titanium peroxy complex to form a solution; adding an alcohol to the solution under normal temperature and normal pressure to produce the nanostructured titanic acid salt precursor precipitate in the solution, and separating the precipitate to obtain the titanic acid salt precursor; drying the precursor, and then heat treating it to obtain the nanostructured titanic acid salt product. The present invention provides a process for preparing a titanic acid salt with simple preparation process, easy control for process parameters and easy large-scale industrial production.

    Diverting Agent For Diversion Acidizing In Water Injection Wells And A Preparation Method Thereof

    公开(公告)号:US20190276731A1

    公开(公告)日:2019-09-12

    申请号:US16240107

    申请日:2019-01-04

    Abstract: The present disclosure provides a diverting agent for diversion acidizing in water injection wells and a preparation method thereof. The diverting agent for diversion acidizing in water injection wells has a raw material composition including: 3%-6% of ethylenediamine, 12%-25% of bromododecane, 10%-20% of a solvent, 10%-20% of an assistant, 14%-28% of oleic acid, 5%-10% of stearic acid salt, 1%-2% of a dispersing agent and a balance of water. The present disclosure also provides a method for preparing the above-mentioned diverting agent for diversion acidizing in water injection wells. The diverting agent for diversion acidizing in water injection wells of the present disclosure can be used for temporary plugging diverting of acid solution in on-line acidification of water injection wells or in acidification operation of oil reservoir with a greater heterogeneity, which has good compatibility with the acid solution and can be used for temporary plugging of high-permeability zones.

    METHOD FOR OBTAINING CONVERSION RELATIONSHIP BETWEEN DYNAMIC AND STATIC ELASTIC PARAMETERS

    公开(公告)号:US20190265142A1

    公开(公告)日:2019-08-29

    申请号:US16062309

    申请日:2017-04-19

    Abstract: A method for obtaining a conversion relationship between dynamic and static elastic parameters includes: Step S1, acquiring horizontal cores at different depths of the destination formation; Step S2, measuring the dynamic elastic parameters of the horizontal core under different pressures; Step S3, measuring the static elastic parameters of the horizontal core under different pressures; Step S4, measuring the clay content of the horizontal core; Step S5 establishing a function relationship of the ratio between the dynamic and static elastic parameters with the formation pressure and clay content; and completing the conversion between the dynamic and static elastic parameters. The technical solution provided by the present invention takes full account of the influence of the formation stress and the clay content on the conversion rule of dynamic and static elastic parameters and is of great significance for improving the logging evaluation accuracy of rock mechanical parameters.

    Nano-Silica Dispersion Having Amphiphilic Properties And A Double-Particle Structure And Its Production Method

    公开(公告)号:US20190046939A1

    公开(公告)日:2019-02-14

    申请号:US15941712

    申请日:2018-03-30

    Abstract: The present invention provides a nano-silica dispersion having amphiphilic properties and a double-particle structure and its production method. The production method comprises: producing a lipophilically modified nano-silica alcosol which is denoted as a first reaction solution by adding a silane coupling agent containing a lipophilic group to a nano-silica alcosol as a raw material; producing a hydrophilically modified nano-silica alcosol which is denoted as a second reaction solution by adding a silane coupling agent containing a hydrophilic group into a nano-silica alcosol as a raw material; producing the nano-silica dispersion having amphiphilic properties and a double-particle structure by adding 3-aminopropyltriethoxysilane to the first reaction solution, stirring, then mixing the resultant with the second reaction solution. The present invention further provides a nano-silica dispersion having amphiphilic properties and a double-particle structure produced by the above production method. It has both hydrophilic and lipophilic properties, and has the double-particle structure, with a particle size of less than 100 nm. The production process is simple and low in cost.

    MONITORING SYSTEM FOR DEFORMATIONS AND DESTRUCTIONS OF GAS STORAGE

    公开(公告)号:US20180372892A1

    公开(公告)日:2018-12-27

    申请号:US16016710

    申请日:2018-06-25

    Abstract: The invention discloses a monitoring system for deformations and destructions of a gas storage, including an acoustic emission sensor installed in a borehole of a monitored rock mass and a ground workstation. The acoustic emission sensor includes an acoustic emission probe and a probe installation mechanism for installing the acoustic emission probe and a transmission mechanism for transmitting the probe installation mechanism. The probe installation mechanism includes a shell, a probe sleeve and two sets of pistons hydro-cylinder components. The present invention realizes the control of the moving direction of the shell and the probe sleeve by the piston hydro-cylinder component and the hydraulic pump, thus solving the problem of effective installation and coupling of the acoustic emission probe, ensuring the effective coupling between the acoustic emission probe and the wall of the borehole.

    STRATUM COMPONENT OPTIMIZATION DETERMINATION METHOD AND DEVICE

    公开(公告)号:US20180246999A1

    公开(公告)日:2018-08-30

    申请号:US15749290

    申请日:2016-10-10

    Abstract: The present invention provides a stratum component optimization determination method and device, which fall within the technical field of oil-gas exploration well logging. The method comprises: establishing a stratum rock component model according to core analysis data and geological conditions of a stratum to be detected, and determining a well logging curve determined by a participation model; determining a well logging response equation expression corresponding to the well logging curve determined by the participation model; parsing, recording and storing the well logging response equation expression, establishing a target function of an optimization problem, and solving the target function through an iteration algorithm to determine an optimal component content of the stratum to be detected. By establishing the stratum rock component model, determining corresponding well logging response equation, and parsing through an expression parsing method and recording and storing the well logging response equation expression, and then, establishing the target function of the optimization problem, and obtaining the optimal component content of the stratum to be detected through the iteration algorithm, the present invention can not only optimizes the self-defined well logging response equation expression of the user, but achieves a high processing precision.

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