Toner processes
    82.
    发明授权
    Toner processes 失效
    墨粉处理

    公开(公告)号:US5723252A

    公开(公告)日:1998-03-03

    申请号:US707037

    申请日:1996-09-03

    IPC分类号: G03G9/087 G03G9/08

    CPC分类号: G03G9/0804 Y10S977/788

    摘要: A process for the preparation of toner which comprises (i) preparing a pigment dispersion comprised of a pigment dispersed in an ionic surfactant; (ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin particles and a counterionic surfactant; (iii) heating the above sheared blend below the glass transition temperature (Tg) of said resin particles to form electrostatically bound toner size aggregates; (iv) adding a stabilizer of in situ tricalcium phosphate solid particulants generated from a solution of calcium chloride and trisodium phosphate; (v) heating the mixture of (iii) and (iv) above about the Tg of the resin particles to obtain toner size particles comprised of resin and pigment; (vi) washing with an acid to dissolve the trisodium phosphate; and (vii) optionally washing with water, and optionally drying the toner obtained.

    摘要翻译: 一种制备调色剂的方法,其包括(i)制备由分散在离子表面活性剂中的颜料组成的颜料分散体; (ii)用由树脂颗粒和抗衡离子表面活性剂组成的胶乳或乳液共混物剪切所述颜料分散体; (iii)将上述剪切混合物加热到所述树脂颗粒的玻璃化转变温度(Tg)以下以形成静电结合的调色剂尺寸聚集体; (iv)加入由氯化钙和磷酸三钠生成的原位磷酸三钙固体颗粒的稳定剂; (v)加热上述(iii)和(iv)的混合物约树脂颗粒的Tg,得到由树脂和颜料组成的调色剂尺寸颗粒; (vi)用酸洗涤以溶解磷酸三钠; 和(vii)任选地用水洗涤,并任选地干燥获得的调色剂。

    Encapsulated toner process utilizing phase separation
    83.
    发明授权
    Encapsulated toner process utilizing phase separation 失效
    使用相分离的封装墨粉处理

    公开(公告)号:US5302486A

    公开(公告)日:1994-04-12

    申请号:US870375

    申请日:1992-04-17

    摘要: A process for the preparation of an encapsulated toner composition comprised of a core and a shell thereover, which process comprises mixing an organic phase comprised of an olefinic monomer, pigment, and a first resin A soluble in the organic phase; dispersing the organic phase into microdroplets in an aqueous solution comprised of a surfactant; subjecting the resulting mixture to free radical polymerization by heating wherein the olefinic monomer is converted to a second resin B; and wherein said resin B is incompatible with said resin A and phase separates whereby a core and shell results.

    摘要翻译: 一种由芯和壳组成的包封的调色剂组合物的制备方法,该方法包括混合由烯烃单体,颜料和可溶于有机相的第一树脂A组成的有机相; 将有机相分散在由表面活性剂组成的水溶液中的微滴中; 使所得混合物通过加热进行自由基聚合,其中烯属单体转化为第二树脂B; 并且其中所述树脂B与所述树脂A不相容并且相分离,从而产生核和壳。

    Microsuspension processes for toner compositions
    84.
    发明授权
    Microsuspension processes for toner compositions 失效
    调色剂组合物的微悬浮方法

    公开(公告)号:US5290654A

    公开(公告)日:1994-03-01

    申请号:US921165

    申请日:1992-07-29

    IPC分类号: G03G9/087 C08J3/215 G03G9/08

    CPC分类号: C08J3/215 G03G9/0804

    摘要: A process for the preparation of toner compositions which comprises dissolving a polymer, and optionally a pigment in an organic solvent; dispersing the resulting solution in an aqueous media containing a surfactant, or mixture of surfactants; stirring the mixture with optional heating to remove the organic solvent thereby obtaining suspended particles of about 0.05 micron to about 2 microns in volume diameter; subsequently homogenizing the resulting suspension with an optional pigment in water and surfactant; followed by aggregating the mixture by heating thereby providing toner particles with an average particle volume diameter of from between about 3 to about 21 microns when said pigment is present.

    摘要翻译: 一种制备调色剂组合物的方法,其包括将聚合物和任选的颜料溶解在有机溶剂中; 将所得溶液分散在含有表面活性剂或表面活性剂混合物的水性介质中; 在任选加热下搅拌混合物以除去有机溶剂,从而获得体积直径为约0.05微米至约2微米的悬浮颗粒; 随后用任选的颜料在水和表面活性剂中均化得到的悬浮液; 然后通过加热聚集混合物,从而当所述颜料存在时提供具有约3至约21微米的平均颗粒体积直径的调色剂颗粒。

    Photochromic gyricon display
    88.
    发明授权
    Photochromic gyricon display 有权
    光致变色显示屏

    公开(公告)号:US06549327B2

    公开(公告)日:2003-04-15

    申请号:US09864386

    申请日:2001-05-24

    IPC分类号: G09G308

    CPC分类号: G02B26/026 C07D491/10

    摘要: Disclosed is a display comprising an arrangement of a plurality of optically anisotropic rotatable elements, each of the rotatable elements having a surface in contact with an enabling fluid, the rotatable elements being electrically dipolar in the presence of the enabling fluid and thus being subject to rotation upon application of an electric field, the rotatable elements being free to rotate in place but not free to translate substantially so as to disrupt the arrangement of rotatable elements, wherein a first portion of the surface contains a mixture of a chelating agent and a spiropyran material of the formula wherein n is an integer representing the number of repeat —CH2— units and R is —H or —CH═CH2, and wherein a second portion of the surface contains substantially no spiropyran.

    摘要翻译: 公开了一种显示器,其包括多个光学各向异性可旋转元件的布置,每个可旋转元件具有与启用流体接触的表面,可旋转元件在有效流体存在的情况下是电偶极性的,因此被旋转 在施加电场时,可旋转元件可自由旋转到位,但不能自由平移以便基本上平移以便破坏可旋转元件的布置,其中表面的第一部分包含螯合剂和螺吡喃材料的混合物 其中n是表示重复-CH 2 - 单元的数目的整数,并且R是-H或-CH = CH 2,并且其中该表面的第二部分基本上不含螺吡喃。