公开(公告)号：US20130140722A1

公开(公告)日：2013-06-06

申请号：US13309783

申请日：2011-12-02

申请人： Raymond J. Zinobile ,  Ashok Rakhe

发明人： Raymond J. Zinobile ,  Ashok Rakhe

IPC分类号： B01F3/04 ,  B23P17/00

CPC分类号： B01D3/32 ,  Y10T29/49716

摘要： A distillation column is provided with a downcomer having an enlarged upper region to increase a processing rate for the removal of permanganate reducing compounds (PRCs) formed by the carbonylation of methanol in the presence of a catalyst to produce acetic acid. The distillation column includes a vertically extending distillation housing; and a plurality of tray assemblies, at least one of which includes a horizontally extending tray panel and a downcomer having, in a downward direction, an enlarged, funnel-shaped upper region defined by a top downcomer panel oriented at an angle to the vertical, and a lower region of substantially constant cross-sectional area defined by a vertically-oriented bottom downcomer panel.

摘要翻译： 蒸馏塔设有具有扩大的上部区域的降液管，以增加在催化剂存在下甲醇羰基化形成的高锰酸盐还原化合物（PRC）的加工速率以产生乙酸。 蒸馏塔包括垂直延伸的蒸馏壳体; 以及多个托盘组件，其中至少一个包括水平延伸的托盘面板和降液管，所述降液管在向下的方向上具有由垂直于一定角度定向的顶层降液管板限定的扩大的漏斗状上部区域， 以及由垂直定向的底部降液管板限定的基本上恒定的横截面积的下部区域。

公开(公告)号：US20120157710A1

公开(公告)日：2012-06-21

申请号：US12970315

申请日：2010-12-16

申请人： Raymond Zinobile ,  Michael Lakin ,  Ashok Rakhe ,  Ronald Shaver

发明人： Raymond Zinobile ,  Michael Lakin ,  Ashok Rakhe ,  Ronald Shaver

IPC分类号： C07C51/12

CPC分类号： C07C51/12 ,  Y02P20/582 ,  Y02P20/584 ,  C07C53/08

摘要： Eductor mixers are used to mix the reaction medium in a carbonylation reactor. A portion of the reaction solution withdrawn from the reactor and directed through a pump around loop. The pump around loop is fed back to the reactor through the eductor mixers. In addition, a pump around loop may pass through one or more steam generators and/or heat exchangers.

摘要翻译： 电解质混合器用于将反应介质混合在羰基化反应器中。 反应溶液的一部分从反应器中排出并引导通过循环的泵。 循环泵通过喷射混合器反馈回反应器。 另外，循环泵可以通过一个或多个蒸汽发生器和/或热交换器。

公开(公告)号：US09079121B2

公开(公告)日：2015-07-14

申请号：US13309783

申请日：2011-12-02

申请人： Raymond J. Zinobile ,  Ashok Rakhe

发明人： Raymond J. Zinobile ,  Ashok Rakhe

IPC分类号： B01F3/04 ,  B01D3/32

CPC分类号： B01D3/32 ,  Y10T29/49716

摘要： A distillation column is provided with a downcomer having an enlarged upper region to increase a processing rate for the removal of permanganate reducing compounds (PRCs) formed by the carbonylation of methanol in the presence of a catalyst to produce acetic acid. The distillation column includes a vertically extending distillation housing; and a plurality of tray assemblies, at least one of which includes a horizontally extending tray panel and a downcomer having, in a downward direction, an enlarged, funnel-shaped upper region defined by a top downcomer panel oriented at an angle to the vertical, and a lower region of substantially constant cross-sectional area defined by a vertically-oriented bottom downcomer panel.

摘要翻译： 蒸馏塔设有具有扩大的上部区域的降液管，以增加在催化剂存在下甲醇羰基化形成的高锰酸盐还原化合物（PRC）的加工速率以产生乙酸。 蒸馏塔包括垂直延伸的蒸馏壳体; 以及多个托盘组件，其中至少一个包括水平延伸的托盘面板和降液管，所述降液管在向下的方向上具有由垂直于一定角度定向的顶层降液管板限定的扩大的漏斗状上部区域， 以及由垂直定向的底部降液管板限定的基本上恒定的横截面积的下部区域。

公开(公告)号：US08563773B2

公开(公告)日：2013-10-22

申请号：US12970315

申请日：2010-12-16

申请人： Raymond Zinobile ,  Michael Lakin ,  Ashok Rakhe ,  Ronald Shaver

发明人： Raymond Zinobile ,  Michael Lakin ,  Ashok Rakhe ,  Ronald Shaver

IPC分类号： C07C51/12 ,  C07C51/10

CPC分类号： C07C51/12 ,  Y02P20/582 ,  Y02P20/584 ,  C07C53/08

摘要： Eductor mixers are used to mix the reaction medium in a carbonylation reactor. A portion of the reaction solution withdrawn from the reactor and directed through a pump around loop. The pump around loop is fed back to the reactor through the eductor mixers. In addition, a pump around loop may pass through one or more steam generators and/or heat exchangers.

摘要翻译： 电解质混合器用于将反应介质混合在羰基化反应器中。 反应溶液的一部分从反应器中排出并引导通过循环的泵。 循环泵通过喷射混合器反馈回反应器。 另外，循环泵可以通过一个或多个蒸汽发生器和/或热交换器。