摘要:
Solid polycarbonate is recovered continuously from solutions thereof in organic solvents by a process consisting of:(a) subdividing the polycarbonate solution by steam (water vapor) at either sonic or ultra-sonic speed by means of a De Laval type nozzle;(b) conveying the dispersion thus obtained into a tubular heat exchanger having an increasing cross-section, preferably spirally-shaped or with elbow stretches having a thermal exchange coefficient of 500-1500 Kcal/h.m.sup.2 .degree.C., in which the heat dispersion is kept at 100.degree.-140.degree. C. for periods of time comprised between 0.05 and 5 seconds;(c) separating the solid from the vapors in a cyclone;(d) drying of the solid in a water vapor fluid bed.
摘要:
A fluid bed reactor, suited for recycling a fluidizing gas containing, in suspension, particles of solid material; comprising a gas distributor consisting of a doubleconed body or of a series of concentrical cones provided on their lateral surfaces with ribs or fins forming gas inflow channels shaped in such a way and with such an inclination as to allow the passage of the solid particles entrained in the gas flow, and such as to hinder the outflow of the solid material that has been fluidized, when the flow of the gas is interrupted.