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1.发明授权Method for the separation of chlorosilanes from a gaseous mixture containing hydrogen chloride and hydrogen 失效从含有氯化氢和氢气的气体混合物中分离氯硅烷的方法
公开(公告)号：US4490343A
公开(公告)日：1984-12-25
申请号：US561163
申请日：1983-12-14
IPC分类号： C01B33/107 , C01B3/52 , C01B7/07 , C01B33/03 , C01B33/12
CPC分类号： C01B33/03
摘要： A method for separating chlorosilanes from a gaseous mixture which additionally contains hydrogen and hydrogen chloride by washing the gaseous mixture with saturated hydrochloric acid is disclosed. The resulting chlorosilane hydrolysis products can remain in the hydrochloric acid serving as washing liquid, without interfering with the purifying action. The suspended hydrolysis products are easily filtrable, and can be periodically separated from the hydrochloric acid. In a preferred embodiment, the hydrochloric acid is recirculated and injected into the gas stream being washed.
摘要翻译： 公开了一种通过用饱和盐酸洗涤气体混合物来另外含有氢和氯化氢的气态混合物中分离氯硅烷的方法。 得到的氯硅烷水解产物可以保留在作为洗涤液体的盐酸中，而不会干扰净化作用。 悬浮的水解产物易于过滤，并且可以与盐酸周期性地分离。 在优选的实施方案中，将盐酸再循环并注入待洗涤的气流中。
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公开(公告)号：US4234503A
公开(公告)日：1980-11-18
申请号：US971966
申请日：1978-12-21
CPC分类号： C07F7/1892
摘要： A process for preparing a gamma amino propyl alkoxy silane of the formula ##STR1## wherein R is an alkyl moiety of 1 to 4 carbon atoms, R' is methyl or phenyl, and y is 0, 1 or 2 which comprises contacting the corresponding gamma-chloropropyl alkoxy silane with ammonia under pressure at a temperature between 50.degree. and 90.degree. C. while stirring the reaction mixture.
摘要翻译： 一种制备式IMAMA的γ-氨基丙基烷氧基硅烷的方法，其中R是1至4个碳原子的烷基部分，R'是甲基或苯基，y是0,1或2，其包括使相应的γ 氯丙基烷氧基硅烷与氨在压力下在50至90℃的温度下搅拌反应混合物。
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公开(公告)号：US4234502A
公开(公告)日：1980-11-18
申请号：US961311
申请日：1978-11-16
CPC分类号： C07F7/1892
摘要： An improved process for the production of an aminoalkylsilane by reaction of a chloroalkylsilane with ammonia or alkylamine at an elevated temperature or pressure wherein the chloroalkylsilane is added in a less than stoichiometric ratio to the ammonia or alkylamine preheated in a pressure vessel at a temperature between 50.degree. and 200.degree. C. Thereafter the reaction is carried out in a known manner within the temperature range of 50.degree. to 200.degree. C. By this manipulative technique, a higher yield of aminoalkylsilane is obtained per unit of time and the aminoalkylsilane is obtained in a greater purity.
摘要翻译： 通过氯烷基硅烷与氨或烷基胺在升高的温度或压力下反应制备氨基烷基硅烷的改进方法，其中氯代烷基硅烷以低于化学计量比与在压力容器中预热的氨或烷基胺以50℃ DEG和200℃。此后，反应在50〜200℃的温度范围内以已知的方式进行。通过该操作技术，每单位时间获得较高的氨基烷基硅烷的产率，氨基烷基硅烷 纯度更高。
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公开(公告)号：US4178295A
公开(公告)日：1979-12-11
申请号：US902201
申请日：1978-05-02
IPC分类号： C07D307/88
CPC分类号： C07D307/88
摘要： An improvement in a process for preparing phthalide by reacting chlorophthalide with hydrogen in the presence of a catalyst at a temperature between 50.degree. and 350.degree. C., the improvement residing in carrying out the process in the absence of a hydrogen chloride acceptor, flowing the chlorophthalide continuously in fluid form through a solid catalyst bed in a reactor, passing the hydrogen through in such an excess so as to sweep off the hydrogen chloride formed and withdrawing phthalide in fluid form.
摘要翻译： 在催化剂存在下，在50〜350℃的温度下，使氯苯酞与氢气反应制备苯并膦的方法的改进，改进在不存在氯化氢受体的情况下进行该方法， 氯代酞酸盐通过反应器中的固体催化剂床连续流动，使氢气过量通过，以便清除形成的氯化氢并以流体形式抽出苯酞。
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