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公开(公告)号：US4101551A
公开(公告)日：1978-07-18
申请号：US702045
申请日：1976-07-02
IPC分类号： C09B25/00 , C09B62/523 , C07D215/22
CPC分类号： C09B62/523 , C09B25/00 , Y10S8/922 , Y10S8/924
摘要： The invention relates to water-insoluble quinophthalone dyestuffs of the formula ##STR1## in which T represents W--Ar or ##STR2## and Ar denotes aryl,W denotes oxygen, sulphur or N--R,R denotes hydrogen or alkyl,A denotes alkylene, O R.sub.1 denotes alkyl or aryl,R.sub.2 denotes hydrogen or alkyl,X denotes halogen, alkyl, alkoxy, nitro or acylamino,Y denotes hydrogen or halogen,Z denotes hydrogen, alkyl or halogen andn denotes a number from 0 to 3The new dyestuffs and their mixtures are distinguished by good affinity to polyester fibres and good general fastness properties.
摘要翻译： 本发明涉及式“IMAGE”的水不溶性喹酞酮染料，其中T代表W-Ar或者“IMA”，Ar表示芳基，W表示氧，硫或NR，R表示氢或烷基，A表示亚烷基，O R1表示烷基或芳基，R2表示氢或烷基，X表示卤素，烷基，烷氧基，硝基或酰氨基，Y表示氢或卤素，Z表示氢，烷基或卤素，N表示0至3的数字新染料和 它们的混合物通过对聚酯纤维的亲和力和良好的通用牢度性质来区分。
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公开(公告)号：US4076736A
公开(公告)日：1978-02-28
申请号：US693038
申请日：1976-06-04
IPC分类号： C09B1/22 , C07C20060101 , C07C225/34 , C09B1/00 , C09B1/20 , C07C97/24
CPC分类号： C07C225/34
摘要： In the reaction of a nitroanthraquinone with ammonia in a solvent at elevated temperature to produce the corresponding aminoanthraquinone, the improvement which comprises effecting the reaction in the presence of an ammonium halide. Advantageously, the nitroanthraquinone is an .alpha.-nitroanthraquinone, the ammonium halide is at least one of ammonium chloride and ammonium bromide, and the solvent comprises at least one member selected from the group consisting of water, nitrobenzene, a glycol, an acid amide and sulfolane.
摘要翻译： 在硝基蒽醌与氨在溶剂中在升高的温度下反应产生相应的氨基蒽醌，其改进包括在卤化铵存在下进行反应。 有利地，硝基蒽醌是α-硝基蒽醌，卤化铵是氯化铵和溴化铵中的至少一种，溶剂包括选自水，硝基苯，二醇，酰胺和环丁砜的至少一种 。
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公开(公告)号：US4220779A
公开(公告)日：1980-09-02
申请号：US920778
申请日：1978-06-30
IPC分类号： C07D215/48 , C07D215/04 , C07D215/20 , C07D215/36 , C07D215/54 , C07D219/02 , C07D215/12 , C07D215/14 , C07D215/18
CPC分类号： C07D215/04 , C07D215/20 , C07D215/36 , C07D215/54 , C07D219/02
摘要： Quinoline derivatives, especially those of the formula ##STR1## wherein X represents halogen, nitro or CF.sub.3,Z represents hydrogen, alkyl or aryl,Y represents hydrogen, OH, CN, COR or SO.sub.3 H,R represents alkyl, alkoxy or aryl andn represents an integer from 0 to 4,are obtained in high yields when corresponding aromatic orthodichloromethyl isocyanates are converted by hydrolysis and decarboxylation into the corresponding ortho-aminoaldehydes and these are subjected to a condensation reaction with carbonyl compounds containing an active .alpha.-methylene group.The process products are starting materials for dyestuffs, insecticides and others.
摘要翻译： 喹啉衍生物，特别是式
的那些，其中X表示卤素，硝基或CF 3，Z表示氢，烷基或芳基，Y表示氢，OH，CN，COR或SO 3 H，R表示烷基，烷氧基或芳基，n表示 当相应的芳族二氯甲基异氰酸酯通过水解和脱羧转化成相应的邻氨基醛时，以高产率获得0-4的整数，并且它们与含有活性α-亚甲基的羰基化合物进行缩合反应。 工艺产品为染料，杀虫剂等原料。 -
4.发明授权
公开(公告)号：US4179450A
公开(公告)日：1979-12-18
申请号：US794143
申请日：1977-05-05
IPC分类号： C07C225/34 , C07C233/07 , C07C233/33 , C07C233/43 , C09B1/22 , C09B1/36 , C07C97/24 , C07C103/75
摘要： The invention relates to a novel process for the preparation of 1-acylamino-5(8)-chloroanthraquinones, which are starting materials for the preparation of vat dyes. It is characterized in that 1,5(8)-dichloroanthraquinones is reacted with ammonia at temperatures of 190.degree. to 240.degree. C., the amino groups in the reaction mixture are completely acylated and the more sparingly soluble diacylaminoanthraquinone is separated off from the more readily soluble monoacylaminochloroanthraquinone.The new process yields reaction products which are purer and cheaper than those which are obtained by conventional methods. Moreover there are smaller waste water problems.
摘要翻译： 本发明涉及一种制备1-酰基氨基-5（8） - 氯蒽醌的新方法，它是制备还原染料的起始原料。 其特征在于，在190〜240℃的温度下，使1,5（8） - 二氯蒽醌与氨反应，反应混合物中的氨基被完全酰化，并且更多的微溶于二酰基氨基蒽醌与更多的 易溶单酰基氨基氯蒽醌。 新方法产生的反应产物比通过常规方法获得的产物更纯净和便宜。 此外还有较小的废水问题。
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公开(公告)号：US4105662A
公开(公告)日：1978-08-08
申请号：US775894
申请日：1977-03-09
CPC分类号： C09B62/22
摘要： Reactive dyestuffs of the formula ##STR1## WHEREIN R.sub.1, R.sub.2, R.sub.3, X, Y and Z have the meaning given in the description and their use for the dyeing and printing of materials which contain hydroxyl groups and materials which contain N, such as cotton, wool and the like, by the customary processes.
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