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1.发明授权Facile and effective method of preparing 1,4-bis(chlorodifluoromethyl)benzene 有权制备1,4-双（氯二氟甲基）苯的方便有效的方法公开(公告)号：US08816139B2
公开(公告)日：2014-08-26
申请号：US13477188
申请日：2012-05-22
Applicant: Chun Hsu Lin , Hung Cheng Yin , Chien Yi Sun , Yung Yu Yin , Chuan Yu Chou
Inventor： Chun Hsu Lin , Hung Cheng Yin , Chien Yi Sun , Yung Yu Yin , Chuan Yu Chou
Abstract: The present invention relates to a facile method of preparing 1,4-bis(chlorodifluoromethyl)benzene, comprising the steps of: (A) providing a reactant liquid of 1,4-bis(difluoromethyl)benzene; optionally (B) providing a light source for UV radiation; and (C) introducing chlorine gas into the reactant liquid at a temperature of 50-90° C. under a pressure above 1 atm to obtain 1,4-Bis(chlorodifluoromethyl)benzene. The invented facile method can be utilized in a batch process or a continuous process for effective production of 1,4-bis(chlorodifluoromethyl)benzene.
Abstract translation: 本发明涉及一种制备1,4-双（氯二氟甲基）苯的简便方法，包括以下步骤：（A）提供1,4-双（二氟甲基）苯的反应液; 任选地（B）提供用于UV辐射的光源; 和（C）在高于1大气压的压力下，在50-90℃的温度下将氯气引入反应液中，得到1,4-双（氯二氟甲基）苯。 本发明的简便方法可以用于分批方法或用于有效生产1,4-双（氯二氟甲基）苯的连续方法。
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2.发明申请FACILE AND EFFECTIVE METHOD OF PREPARING 1,4-BIS(CHLORODIFLUOROMETHYL)BENZENE 有权制备1,4-BIS（氯代二甲苯）苯的方法和有效方法公开(公告)号：US20130116482A1
公开(公告)日：2013-05-09
申请号：US13477188
申请日：2012-05-22
Applicant: Chun-Hsu LIN , Hung-Cheng Yin , Chien-Yi Sun , Yung-Yu Yin , Chuan-Yu Chou
Inventor： Chun-Hsu LIN , Hung-Cheng Yin , Chien-Yi Sun , Yung-Yu Yin , Chuan-Yu Chou
Abstract: The present invention relates to a facile method of preparing 1,4-bis(chlorodifluoromethyl)benzene, comprising the steps of: (A) providing a reactant liquid of 1,4-bis(difluoromethyl)benzene; optionally (B) providing a light source for UV radiation; and (C) introducing chlorine gas into the reactant liquid at a temperature of 50-90° C. under a pressure above 1 atm to obtain 1,4-Bis(chlorodifluoromethyl)benzene. The invented facile method can be utilized in a batch process or a continuous process for effective production of 1,4-bis(chlorodifluoromethyl)benzene.
Abstract translation: 本发明涉及一种制备1,4-双（氯二氟甲基）苯的简便方法，包括以下步骤：（A）提供1,4-双（二氟甲基）苯的反应液; 任选地（B）提供用于UV辐射的光源; 和（C）在高于1大气压的压力下，在50-90℃的温度下将氯气引入反应液中，得到1,4-双（氯二氟甲基）苯。 本发明的简便方法可以用于分批方法或用于有效生产1,4-双（氯二氟甲基）苯的连续方法。
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