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1.发明授权Method and apparatus for determining the length of single-walled carbon nanotubes 失效用于确定单壁碳纳米管长度的方法和装置公开(公告)号：US06962092B2
公开(公告)日：2005-11-08
申请号：US10836551
申请日：2004-04-30
申请人： Matteo Pasquali , Virginia A. Davis , Ingrid Stepanek-Basset , A. Nicholas G. Parra-Vasquez , Robert H. Hauge
发明人： Matteo Pasquali , Virginia A. Davis , Ingrid Stepanek-Basset , A. Nicholas G. Parra-Vasquez , Robert H. Hauge
CPC分类号： B82Y30/00 , B82Y15/00 , B82Y40/00 , C01B32/15 , C01B2202/02 , C01B2202/34 , G01N11/00 , Y10S977/88
摘要： The present invention is directed to at least one method and at least one apparatus for determining the length of single-wall carbon nanotubes (SWNTs). The method generally comprises the steps of: dispersing a sample of SWNTs into a suitable dispersing medium to form a solvent-suspension of solvent-suspended SWNTs; determining the mean SWNT diameter of the solvent-suspended SWNTs; introducing the solvent-suspended SWNTs into a viscosity-measuring device; obtaining a specific viscosity for the SWNT solvent-suspension; and determining the length of the SWNTs based upon the specific viscosity by solving, for example, the Kirkwood-Auer equation corrected by Batchelor's formula for the drag on a slender cylinder for “L,” to determine the length of the SWNTs. The apparatus generally comprises: a SWNT sample introduction mechanism; a dispersal chamber; a SWNT radius-determination chamber; and a viscosity determining chamber, wherein the SWNT sample introduction mechanism, the dispersal chamber, the SWNT radius-determination chamber, and the viscosity determination chamber are each operatively connected to at least one of the others.
摘要翻译： 本发明涉及用于确定单壁碳纳米管（SWNT）的长度的至少一种方法和至少一种装置。 该方法通常包括以下步骤：将SWNT样品分散到合适的分散介质中以形成溶剂悬浮的SWNT的溶剂 - 悬浮液; 确定溶剂悬浮的SWNT的平均SWNT直径; 将溶剂悬浮的SWNT引入粘度测量装置中; 获得SWNT溶剂 - 悬浮液的比粘度; 以及通过解决例如通过Batchelor公式修正的Kirkwood-Auer方程式来确定SWNTs的长度，以便通过在“L”的细长圆筒上拖动来确定SWNT的长度。 该装置通常包括：SWNT样品引入机构; 分散室; SWNT半径测定室; 和粘度确定室，其中SWNT样品引入机构，分散室，SWNT半径确定室和粘度确定室各自可操作地连接到至少其中之一。
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2.发明申请METHOD AND APPARATUS FOR DETERMINING THE LENGTH OF SINGLE-WALLED CARBON NANOTUBES 失效用于确定单壁碳纳米管长度的方法和装置公开(公告)号：US20050160798A1
公开(公告)日：2005-07-28
申请号：US10836551
申请日：2004-04-30
申请人： Matteo Pasquali , Virginia Davis , Ingrid Stepanek-Basset , A. Nicholas Parra-Vasquez , Robert Hauge
发明人： Matteo Pasquali , Virginia Davis , Ingrid Stepanek-Basset , A. Nicholas Parra-Vasquez , Robert Hauge
CPC分类号： B82Y30/00 , B82Y15/00 , B82Y40/00 , C01B32/15 , C01B2202/02 , C01B2202/34 , G01N11/00 , Y10S977/88
摘要： The present invention is directed to at least one method and at least one apparatus for determining the length of single-wall carbon nanotubes (SWNTs). The method generally comprises the steps of: dispersing a sample of SWNTs into a suitable dispersing medium to form a solvent-suspension of solvent-suspended SWNTs; determining the mean SWNT diameter of the solvent-suspended SWNTs; introducing the solvent-suspended SWNTs into a viscosity-measuring device; obtaining a specific viscosity for the SWNT solvent-suspension; and determining the length of the SWNTs based upon the specific viscosity by solving, for example, the Kirkwood-Auer equation corrected by Batchelor's formula for the drag on a slender cylinder for “L,” to determine the length of the SWNTs. The apparatus generally comprises: a SWNT sample introduction mechanism; a dispersal chamber; a SWNT radius-determination chamber; and a viscosity determining chamber, wherein the SWNT sample introduction mechanism, the dispersal chamber, the SWNT radius-determination chamber, and the viscosity determination chamber are each operatively connected to at least one of the others.
摘要翻译： 本发明涉及用于确定单壁碳纳米管（SWNT）的长度的至少一种方法和至少一种装置。 该方法通常包括以下步骤：将SWNT样品分散到合适的分散介质中以形成溶剂悬浮的SWNT的溶剂 - 悬浮液; 确定溶剂悬浮的SWNT的平均SWNT直径; 将溶剂悬浮的SWNT引入粘度测量装置中; 获得SWNT溶剂 - 悬浮液的比粘度; 以及通过解决例如通过Batchelor公式修正的Kirkwood-Auer方程式来确定SWNTs的长度，以便通过在“L”的细长圆筒上拖动来确定SWNT的长度。 该装置通常包括：SWNT样品引入机构; 分散室; SWNT半径测定室; 和粘度确定室，其中SWNT样品引入机构，分散室，SWNT半径确定室和粘度确定室各自可操作地连接到至少其中之一。
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