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    Production of high-purity niobium monoxide and capacitor production therefrom
    1.
    发明申请
    Production of high-purity niobium monoxide and capacitor production therefrom 审中-公开
    生产高纯度铌氧化物和电容器生产

    公开(公告)号：US20070081937A1

    公开(公告)日：2007-04-12

    申请号：US11548753

    申请日：2006-10-12

    Applicant: Charles Motchenbacher ,  James Robison ,  Brian Higgins ,  Thomas Fonville

    Inventor： Charles Motchenbacher ,  James Robison ,  Brian Higgins ,  Thomas Fonville

    IPC: C01G31/02

    CPC classification number: H01G9/0525 ,  C01G33/00 ,  C01P2002/72 ,  C01P2004/03 ,  C01P2004/51 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/17 ,  C01P2006/40 ,  C01P2006/80

    Abstract: The present invention relates to high-purity niobium monoxide powder (NbO) produced by a process of combining a mixture of higher niobium oxides and niobium metal powder or granules; heating and reacting the compacted mixture under controlled atmosphere to achieve temperatures greater than about 1800° C., at which temperature the NbO is liquid; solidifying the liquid NbO to form a body of material; and fragmenting the body to form NbO particles suitable for application as e.g., capacitor anodes. The NbO product is unusually pure in composition and crystallography, highly dense, and can be used for capacitors and for other electronic applications. The method of production of the NbO is robust, does not require high-purity feedstock, and can reclaim value from waste streams associated with the processing of NbO electronic components.

    Abstract translation: 本发明涉及通过组合高铌氧化物和铌金属粉末或颗粒的混合物的方法制备的高纯度一氧化铌粉末（NbO）; 在受控气氛下加热和使压实的混合物反应以达到高于约1800℃的温度，在该温度下NbO是液体; 固化液体NbO以形成材料体; 并且使体部分分裂以形成适用于例如电容器阳极的NbO颗粒。 NbO产品在组成和结晶学中非常纯净，高密度，可用于电容器和其他电子应用。 NbO的生产方法是坚固的，不需要高纯度原料，并且可以从与NbO电子部件的加工相关的废物流中回收价值。

    Production of high-purity niobium monoxide and capacitor production therefrom
    2.
    发明申请
    Production of high-purity niobium monoxide and capacitor production therefrom 审中-公开
    生产高纯度铌氧化物和电容器生产

    公开(公告)号：US20050002854A1

    公开(公告)日：2005-01-06

    申请号：US10834427

    申请日：2004-04-29

    Applicant: Charles Motchenbacher ,  James Robison ,  Brian Higgins ,  Thomas Fonville

    Inventor： Charles Motchenbacher ,  James Robison ,  Brian Higgins ,  Thomas Fonville

    IPC: C01G33/00 ,  H01G9/052

    CPC classification number: H01G9/0525 ,  C01G33/00 ,  C01P2002/72 ,  C01P2004/03 ,  C01P2004/51 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/17 ,  C01P2006/40 ,  C01P2006/80

    Abstract: The present invention relates to high-purity niobium monoxide powder (NbO) produced by a process of combining a mixture of higher niobium oxides and niobium metal powder or granules; heating and reacting the compacted mixture under controlled atmosphere to achieve temperature greater than about 1945° C., at which temperature the NbO is liquid; solidifying the liquid NbO to form a body of material; and fragmenting the body to form NbO particles suitable for application as capacitor anodes. The NbO product is unusually pure in composition and crystallography, and can be used for capacitors and for other electronic applications. The method of production of the NbO is robust, does not require high-purity feedstock, and can reclaim value from waste streams associated with the processing of NbO electronic components. The method of production also can be used to make high-purity NbO2 and mixtures of niobium metal/niobium monoxide and niobium monoxide/niobium dioxide. The method further is ideal for doping of the product oxides to enhance particular characteristics of the materials. The method further allows the production of single crystal or directionally-solidified ingots. In contrast to the spongy, highly porous agglomerates produced by other techniques, the present invention produces solid, non-porous ingots that can be fragmented to fine, non-porous angular particles suitable for electronic applications.

    Abstract translation: 本发明涉及通过组合高铌氧化物和铌金属粉末或颗粒的混合物的方法制备的高纯度一氧化铌粉末（NbO）; 在受控气氛下加热和反应压实的混合物以达到大于约1945℃的温度，在该温度下NbO是液体; 固化液体NbO以形成物体; 并破碎机体以形成适合用作电容器阳极的NbO颗粒。 NbO产品在组成和晶体学中非常纯净，可用于电容器和其他电子应用。 NbO的生产方法是坚固的，不需要高纯度原料，并且可以从与NbO电子部件的加工相关的废物流中回收价值。 生产方法也可用于制备高纯NbO2和铌金属/一氧化铌和一氧化铌/二氧化铌的混合物。 该方法进一步理想地用于掺杂产物氧化物以增强材料的特定特性。 该方法还允许生产单晶或定向固化的锭。 与通过其它技术生产的海绵状，高度多孔的聚集体相反，本发明产生固体，非多孔的锭，其可以碎裂成适合于电子应用的精细的非多孔角度颗粒。

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