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1.发明授权Method for obtaining ADN crystals through crystallization in a viscous medium 有权通过在粘性介质中结晶获得ADN晶体的方法公开(公告)号：US08491736B2
公开(公告)日：2013-07-23
申请号：US13063614
申请日：2009-09-17
CPC分类号： C06B21/0066 , C01B21/087 , C06B31/00
摘要： The present invention relates to a method for crystallizing ammonium dinitramide (ADN), through spontaneous nucleation and crystal growth, from a solution containing said ammonium dinitramide (AND) dissolved in a solvent. Said solvent characteristically has a viscosity greater than or equal to 0.25 Pa s (250 cP) when said spontaneous nucleation is implemented. The ADN crystals obtained by said method have a median shape factor of 1 to 1.5 and are perfectly suitable for placement in the composition of energy materials.
摘要翻译： 本发明涉及通过自发成核和晶体生长从含有溶解在溶剂中的二硝化铵铵（AND）的溶液中结晶二硝基铵（ADN）的方法。 当实施所述自发成核时，所述溶剂特征性地具有大于或等于0.25Pa·s（250cP）的粘度。 通过所述方法获得的ADN晶体的中值形状因子为1〜1.5，非常适合放置在能量材料的组成中。
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2.发明授权Polyglycidyl azides comprising an acyloxy terminal group and an azide terminal group 有权包含酰氧基端基和叠氮基末端基的多缩水甘油基叠氮化物公开(公告)号：US06323352B1
公开(公告)日：2001-11-27
申请号：US09669470
申请日：2000-09-25
IPC分类号： C07C24700
CPC分类号： C07C247/04 , C06B45/105
摘要： A subject-matter of the present invention is novel polyglycidyl azides of general formula (I): in which: R1 represents an alkylene chain comprising 2 to 4 carbon atoms, R2 represents an alkyl chain comprising 1 to 4 carbon atoms, x represents an integer such that 4≦x≦10. These compounds are not detonatable and are of use in particular as energetic plasticizers in solid pyrotechnic compositions. They can be obtained according to a 3-stage process starting from epichlorohydrin by preliminary synthesis of polyepichlorohydrin with a hydroxyl terminal group of formula (II): then acylation of this compound in order to obtain a polyepichlorohydrin with an acyloxy terminal group of formula (IV): and then azidation of this compound.
摘要翻译： 本发明的主题是通式（I）的新型聚缩水甘油基叠氮化物：其中：R1表示碳原子数2〜4的亚烷基链，R2表示碳原子数1〜4的烷基链，x表示整数 使得这些化合物不可引爆，特别是用作固体烟火组合物中的高能增塑剂。它们可以根据从表氯醇开始的3-阶段方法通过初步合成聚表氯醇与 （II）的羟基端基：然后酰化该化合物，以获得具有式（IV）的酰氧基端基的聚表氯醇：然后将该化合物叠氮化。
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3.发明申请公开(公告)号：US20110171104A1
公开(公告)日：2011-07-14
申请号：US13063614
申请日：2009-09-17
IPC分类号： C01C1/00
CPC分类号： C06B21/0066 , C01B21/087 , C06B31/00
摘要： The present invention relates to a method for crystallizing ammonium dinitramide (ADN), through spontaneous nucleation and crystal growth, from a solution containing said ammonium dinitramide (AND) dissolved in a solvent. Said solvent characteristically has a viscosity greater than or equal to 0.25 Pa s (250 cP) when said spontaneous nucleation is implemented. The ADN crystals obtained by said method have a median shape factor of 1 to 1.5 and are perfectly suitable for placement in the composition of energy materials.
摘要翻译： 本发明涉及通过自发成核和晶体生长从含有溶解在溶剂中的二硝化铵铵（AND）的溶液中结晶二硝基铵（ADN）的方法。 当实施所述自发成核时，所述溶剂特征性地具有大于或等于0.25Pa·s（250cP）的粘度。 通过所述方法获得的ADN晶体的中值形状因子为1〜1.5，非常适合放置在能量材料的组成中。
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