公开(公告)号：US07763167B2

公开(公告)日：2010-07-27

申请号：US11572638

申请日：2005-07-27

申请人： Yuzhuo Zhang ,  Geping Shu ,  Jialu Jin ,  Minli Cui ,  Xiuzhang Wu ,  Xiangkun Ren ,  Yaowu Xu ,  Shipu Liang ,  Jianwei Huang ,  Ming Yuan ,  Juzhong Gao ,  Yufei Zhu

发明人： Yuzhuo Zhang ,  Geping Shu ,  Jialu Jin ,  Minli Cui ,  Xiuzhang Wu ,  Xiangkun Ren ,  Yaowu Xu ,  Shipu Liang ,  Jianwei Huang ,  Ming Yuan ,  Juzhong Gao ,  Yufei Zhu

IPC分类号： C10G1/06 ,  C10G1/00

CPC分类号： C10G1/002 ,  C10G1/065 ,  C10G2300/1074 ,  C10G2300/1077 ,  C10G2300/301 ,  C10G2300/4081 ,  C10G2300/42 ,  C10G2300/44

摘要： Process for direct coal liquefaction of coal, including: (1) preparing a coal slurry from raw coal; (2) preheating the coal slurry, then feeding it into reaction system to undergo liquefaction reaction; (3) separating reaction products in a separator to form a liquid phase and a gas phase, wherein the liquid phase is fractionated in an atmospheric tower into a light oil fraction and a bottom product; (4) feeding the atmospheric tower bottom product to a vacuum tower to separate into distillate and vacuum residue; (5) mixing the light oil fraction and the distillate to form a mixture, then feeding the mixture to a suspended bed hydrotreating reactor with forced circulation for hydrogenation; (6) fractionating hydrogenation products into oil products and a hydrogen donor recycling solvent. The process can operate long periods, with higher reactor efficiency and utilization factor, increased liquid oil yield and can supply high-quality feedstock for further processing.

摘要翻译： 煤炭直接煤液化工艺，包括：（1）从原煤制备煤浆; （2）预热煤浆，然后送入反应体系进行液化反应; （3）在分离器中分离反应产物以形成液相和气相，其中将液相在常压塔中分馏成轻油馏分和底部产物; （4）将大气塔底产物供给真空塔分离成馏出物和减压渣油; （5）将轻油馏分和馏出物混合以形成混合物，然后将混合物进料到具有强制循环氢化的悬浮床加氢处理反应器中; （6）将氢化产物分馏成油产物和氢供体回收溶剂。 该工艺可长时间运行，反应器效率更高，利用率更高，液体油产量提高，可供应优质原料进一步加工。

公开(公告)号：US20090152171A1

公开(公告)日：2009-06-18

申请号：US11572638

申请日：2005-07-27

申请人： Yuzhuo Zhang ,  Geping Shu ,  Jialu Jin ,  Minli Cui ,  Xiuzhang Wu ,  Xiangkun Ren ,  Yaowu Xu ,  Shipu Liang ,  Jianwei Huang ,  Ming Yuan ,  Juzhong Gao ,  Yufei Zhu

发明人： Yuzhuo Zhang ,  Geping Shu ,  Jialu Jin ,  Minli Cui ,  Xiuzhang Wu ,  Xiangkun Ren ,  Yaowu Xu ,  Shipu Liang ,  Jianwei Huang ,  Ming Yuan ,  Juzhong Gao ,  Yufei Zhu

IPC分类号： C10G1/06

CPC分类号： C10G1/002 ,  C10G1/065 ,  C10G2300/1074 ,  C10G2300/1077 ,  C10G2300/301 ,  C10G2300/4081 ,  C10G2300/42 ,  C10G2300/44

摘要： Process for direct coal liquefaction of coal, including: (1) preparing a coal slurry from raw coal; (2) preheating the coal slurry, then feeding it into reaction system to undergo liquefaction reaction; (3) separating reaction products in a separator to form a liquid phase and a gas phase, wherein the liquid phase is fractionated in an atmospheric tower into a light oil fraction and a bottom product; (4) feeding the atmospheric tower bottom product to a vacuum tower to separate into distillate and vacuum residue; (5) mixing the light oil fraction and the distillate to form a mixture, then feeding the mixture to a suspended bed hydrotreating reactor with forced circulation for hydrogenation; (6) fractionating hydrogenation products into oil products and a hydrogen donor recycling solvent. The process can operate long periods, with higher reactor efficiency and utilization factor, increased liquid oil yield and can supply high-quality feedstock for further processing.

摘要翻译： 煤炭直接煤液化工艺，包括：（1）从原煤制备煤浆; （2）预热煤浆，然后送入反应体系进行液化反应; （3）在分离器中分离反应产物以形成液相和气相，其中将液相在常压塔中分馏成轻油馏分和底部产物; （4）将大气塔底产物供给真空塔分离成馏出物和减压渣油; （5）将轻油馏分和馏出物混合以形成混合物，然后将混合物进料到具有强制循环氢化的悬浮床加氢处理反应器中; （6）将氢化产物分馏成油产物和氢供体回收溶剂。 该工艺可长时间运行，反应器效率更高，利用率更高，液体油产量提高，可供应优质原料进一步加工。

公开(公告)号：US20090283450A2

公开(公告)日：2009-11-19

申请号：US11572638

申请日：2008-09-03

申请人： Yuzhuo Zhang ,  Geping Shu ,  Jialu Jin ,  Minli Cui ,  Xiuzhang Wu ,  Xiangkun Ren ,  Yaowu Xu ,  Shipu Liang ,  Jianwei Huang ,  Ming Yuan ,  Juzhong Gao ,  Yufei Zhu

发明人： Yuzhuo Zhang ,  Geping Shu ,  Jialu Jin ,  Minli Cui ,  Xiuzhang Wu ,  Xiangkun Ren ,  Yaowu Xu ,  Shipu Liang ,  Jianwei Huang ,  Ming Yuan ,  Juzhong Gao ,  Yufei Zhu

IPC分类号： C10G1/06

CPC分类号： C10G1/002 ,  C10G1/065 ,  C10G2300/1074 ,  C10G2300/1077 ,  C10G2300/301 ,  C10G2300/4081 ,  C10G2300/42 ,  C10G2300/44

摘要： Process for direct coal liquefaction of coal, including: (1) preparing a coal slurry from raw coal; (2) preheating the coal slurry, then feeding it into reaction system to undergo liquefaction reaction; (3) separating reaction products in a separator to form a liquid phase and a gas phase, wherein the liquid phase is fractionated in an atmospheric tower into a light oil fraction and a bottom product; (4) feeding the atmospheric tower bottom product to a vacuum tower to separate into distillate and vacuum residue; (5) mixing the light oil fraction and the distillate to form a mixture, then feeding the mixture to a suspended bed hydrotreating reactor with forced circulation for hydrogenation; (6) fractionating hydrogenation products into oil products and a hydrogen donor recycling solvent. The process can operate long periods, with higher reactor efficiency and utilization factor, increased liquid oil yield and can supply high-quality feedstock for further processing.

摘要翻译： 煤炭直接煤液化工艺，包括：（1）从原煤制备煤浆; （2）预热煤浆，然后送入反应体系进行液化反应; （3）在分离器中分离反应产物以形成液相和气相，其中将液相在常压塔中分馏成轻油馏分和底部产物; （4）将大气塔底产物供给真空塔分离成馏出物和减压渣油; （5）将轻油馏分和馏出物混合以形成混合物，然后将混合物进料到具有强制循环氢化的悬浮床加氢处理反应器中; （6）将氢化产物分馏成油产物和氢供体回收溶剂。 该工艺可长时间运行，反应器效率更高，利用率更高，液体油产量提高，可供应优质原料进一步加工。