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    Method for Producing Nanoparticulate Lanthanoide/Boron Compounds or Solid Substance Mixtures Containing Nanoparticulate Lanthanoide/Boron Compounds
    2.
    发明申请
    Method for Producing Nanoparticulate Lanthanoide/Boron Compounds or Solid Substance Mixtures Containing Nanoparticulate Lanthanoide/Boron Compounds 审中-公开
    含有纳米颗粒镧系元素/硼化合物的纳米颗粒镧系元素/硼化合物或固体物质混合物的制备方法

    公开(公告)号：US20090041647A1

    公开(公告)日：2009-02-12

    申请号：US11917650

    申请日：2006-06-14

    申请人： Julian Prolss ,  Kirill Bramnik ,  Norbert Wagner ,  Gero Nordmann ,  Markus Hammermann ,  Alexander Benohr

    发明人： Julian Prolss ,  Kirill Bramnik ,  Norbert Wagner ,  Gero Nordmann ,  Markus Hammermann ,  Alexander Benohr

    IPC分类号： C01F17/00

    CPC分类号： B01J19/126 ,  B01J19/088 ,  B01J2219/0886 ,  B01J2219/0894 ,  C01B35/04 ,  C01B35/1036

    摘要： The present invention relates to a process for preparing essentially isometric nanoparticulate lanthanide-boron compounds or solid mixtures comprising essentially isometric nanoparticulate lanthanide-boron compounds, which comprises a) mixing i) one or more lanthanide compounds selected from the group consisting of lanthanide hydroxides, lanthanide hydrides, lanthanide chalcogenides, lanthanide halides, lanthanide borates and mixed compounds of the lanthanide compounds mentioned, ii) one or more compounds selected from the group consisting of crystalline boron, amorphous boron, boron carbides, boron hydrides and boron halides and iii) if appropriate one or more reducing agents selected from the group consisting of hydrogen, carbon, organic compounds, alkaline earth metals and alkaline earth metal hydrides dispersed in an inlet carrier gas with one another, b) reacting the mixture of the components i), ii) and, if appropriate, iii) in the inert solvent by means of thermal treatment within a reaction zone, c) subjecting the reaction product obtained by means of thermal treatment in step b) to rapid cooling and d) subsequently separating off the reaction product which has been cooled in step c), with the cooling conditions in step c) being selected so that the reaction product consists of essentially isometric nanoparticulate lanthanide-boron compounds or comprises essentially isometric nanoparticulate lanthanide-boron compounds.

    摘要翻译： 本发明涉及一种制备基本上等长的纳米颗粒镧系元素硼化合物或包含基本上等长的纳米颗粒镧系元素硼化合物的固体混合物的方法，其包括a）混合i）一种或多种镧系元素化合物，其选自镧系元素氢氧化物，镧系元素 氢化物，镧系元素硫属化物，镧系元素卤化物，镧系元素硼酸盐和所述镧系元素化合物的混合化合物，ii）一种或多种选自结晶硼，无定形硼，碳化硼，硼氢化物和卤化硼的化合物，以及iii）如果合适 一种或多种选自分散在入口载体气体中的氢，碳，有机化合物，碱土金属和碱土金属氢化物的还原剂，b）将组分i），ii）和 如果合适，iii）在惰性溶剂中通过热处理 在反应区中，c）使步骤b）中通过热处理获得的反应产物经历快速冷却，d）随后将步骤c）中已冷却的反应产物分离，步骤c）中的冷却条件， 被选择使得反应产物由基本上等长的纳米颗粒镧系元素硼化合物组成或包含基本上等长的纳米颗粒镧系元素 - 硼化合物。