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公开(公告)号：US08043405B2
公开(公告)日：2011-10-25
申请号：US12338827
申请日：2008-12-18
IPC分类号： C22C27/04
CPC分类号： B22F9/22 , B22F1/0011 , B22F1/0014
摘要： Densified molybdenum metal powder. Densified molybdenum metal powder has substantially generally spherical particles, surface-area-to-mass ratio of no more than about 0.5 m2/g as determined by BET analysis, and a flowability greater than about 32 s/50 g as determined by a Hall Flowmeter.
摘要翻译： 致密的钼金属粉末。 致密的钼金属粉末具有通过BET分析确定的基本上通常为球形的颗粒，表面 - 质量比不超过约0.5m 2 / g，并且通过霍尔流量计测定的大于约32s / 50g的流动性 。
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公开(公告)号：US07625421B2
公开(公告)日：2009-12-01
申请号：US11557781
申请日：2006-11-08
IPC分类号： B22F1/00
摘要： Novel forms of molybdenum metal. Novel forms of molybdenum metal are characterized by a surface area of substantially about 2.1 m2/g to substantially about 4.1 m2/g. Novel forms of molybdenum metal are also characterized by a relatively uniform size.
摘要翻译： 新型钼金属。 钼金属的新形式的特征在于基本上约2.1m 2 / g至约4.1m 2 / g的表面积。 钼金属的新形式的特征还在于尺寸相对均匀。
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公开(公告)号：US08147586B2
公开(公告)日：2012-04-03
申请号：US12338779
申请日：2008-12-18
IPC分类号： B22F9/22
CPC分类号： B22F9/22 , B22F1/0011 , B22F1/0014
摘要： Method for producing molybdenum metal powder. The invention includes introducing a supply of ammonium molybdate precursor material into a furnace in a first direction and introducing a reducing gas into a cooling zone in a second direction opposite to the first direction. The ammonium molybdate precursor material is heated at an initial temperature in the presence of the reducing gas to produce an intermediate product that is heated at a final temperature in the presence of the reducing gas, thereby creating the molybdenum metal powder comprising particles having a surface area to mass ratio of between about 1 m2/g and about 4 m2/g, as determined by BET analysis, and a flowability of between about 29 s/50 g and 86 s/50 g as determined by a Hall Flowmeter. The molybdenum metal powder is moved through the cooling zone.
摘要翻译： 钼金属粉末的制造方法。 本发明包括将第一方向的钼酸铵前体材料供应到炉中，并且在与第一方向相反的第二方向上将还原气体引入冷却区。 钼酸铵前体材料在还原气体的存在下在初始温度下加热，以产生在还原气体存在下在最终温度下加热的中间产物，从而产生包含具有表面积的颗粒的钼金属粉末 通过BET分析测定的约1m 2 / g至约4m 2 / g之间的质量比和通过霍尔流量计测定的约29s / 50g和86s / 50g之间的流动性。 钼金属粉末通过冷却区移动。
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公开(公告)号：US20090116995A1
公开(公告)日：2009-05-07
申请号：US12338827
申请日：2008-12-18
IPC分类号： C22C28/00
CPC分类号： B22F9/22 , B22F1/0011 , B22F1/0014
摘要： Densified molybdenum metal powder. Densified molybdenum metal powder has substantially generally spherical particles, surface-area-to-mass ratio of no more than about 0.5 m2/g as determined by BET analysis, and a flowability greater than about 32 s/50 g as determined by a Hall Flowmeter.
摘要翻译： 致密的钼金属粉末。 致密的钼金属粉末具有通过BET分析确定的基本上通常为球形的颗粒，表面 - 质量比不超过约0.5m 2 / g，并且通过霍尔流量计测定的大于约32s / 50g的流动性 。
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公开(公告)号：US20090095131A1
公开(公告)日：2009-04-16
申请号：US12338779
申请日：2008-12-18
IPC分类号： B22F9/04
CPC分类号： B22F9/22 , B22F1/0011 , B22F1/0014
摘要： Method for producing molybdenum metal powder. The invention includes introducing a supply of ammonium molybdate precursor material into a furnace in a first direction and introducing a reducing gas into a cooling zone in a second direction opposite to the first direction. The ammonium molybdate precursor material is heated at an initial temperature in the presence of the reducing gas to produce an intermediate product that is heated at a final temperature in the presence of the reducing gas, thereby creating the molybdenum metal powder comprising particles having a surface area to mass ratio of between about 1 m2/g and about 4 m2/g, as determined by BET analysis, and a flowability of between about 29 s/50 g and 86 s/50 g as determined by a Hall Flowmeter. The molybdenum metal powder is moved through the cooling zone.
摘要翻译： 钼金属粉末的制造方法。 本发明包括将第一方向的钼酸铵前体材料供应到炉中，并且在与第一方向相反的第二方向上将还原气体引入冷却区。 钼酸铵前体材料在还原气体的存在下在初始温度下加热，以产生在还原气体存在下在最终温度下加热的中间产物，从而产生包含具有表面积的颗粒的钼金属粉末 通过BET分析测定的约1m 2 / g至约4m 2 / g之间的质量比和通过霍尔流量计测定的约29s / 50g和86s / 50g之间的流动性。 钼金属粉末通过冷却区移动。
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公开(公告)号：US07276102B2
公开(公告)日：2007-10-02
申请号：US10970456
申请日：2004-10-21
CPC分类号： B22F9/22 , B22F1/0011 , B22F1/0014
摘要： Molybdenum metal powder, and method for production thereof. Molybdenum metal powder has surface-area-to-mass-ratios in a range of between about 1.0 meters2/gram (m2/g) and about 3.0 m2/g, as determined by BET analysis, in combination with a particle size wherein at least 30% of the particles have a particle size larger than a size +100 standard Tyler mesh sieve. In addition, molybdenum metal powder 10 may be further distinguished by flowability in a range of between about 29 seconds/50 grams (s/50 g) and about 64 s/50 g, as determined by a Hall Flowmeter. A method of producing molybdenum powder may comprise providing a supply of ammonium molybdate, heating the ammonium molybdate at an initial temperature in the presence of a reducing gas to produce an intermediate product, and heating the intermediate product at a final temperature in the presence of the reducing gas, producing molybdenum metal powder.
摘要翻译： 钼金属粉末及其制造方法。 钼金属粉末的表面积与质量比在约1.0m 2 / g（m 2 SUP / g以下）范围内，约3.0μm 通过BET分析测定，与颗粒尺寸相结合，其中至少30％的颗粒具有大于+100标准泰勒筛网的粒度。 此外，通过霍尔流量计测定的钼金属粉末10可以进一步区别在约29秒/ 50克（s / 50克）至约64秒/ 50克之间的流动性。 制备钼粉末的方法可以包括提供钼酸铵供应，在还原气体存在下在初始温度下加热钼酸铵以产生中间产物，并在最终温度下在中间产物存在下加热中间产物 还原气体，生产钼金属粉末。
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公开(公告)号：US07097691B2
公开(公告)日：2006-08-29
申请号：US10289027
申请日：2002-11-05
IPC分类号： B01D7/02
CPC分类号： C09B67/0032 , C09B67/0003 , C09B67/0025 , C09B67/0095 , C09B67/0097
摘要： Method for producing pigment nano-particles may include vaporizing a pigment precursor material; drawing the vaporized pigment precursor material into a precipitation conduit; contacting the vapor in the precipitation conduit with a collection fluid at a first location within the precipitation conduit, the contacting cooling the vapor and precipitating pigment nano-particles, the contacting occurring in the absence of a temperature change in the vapor at locations within the precipitation conduit that are upstream of the first location; and collecting the pigment nano-particles in a collection fluid.
摘要翻译： 制备颜料纳米颗粒的方法可包括使颜料前体材料汽化; 将蒸发的颜料前体材料吸入沉淀管道中; 使沉淀管道中的蒸汽与沉淀管道内的第一位置处的收集液体接触，使得蒸气和沉淀颜料纳米颗粒的接触冷却，在不存在沉淀物内部的蒸汽温度变化的情况下发生接触 位于第一位置上游的导管; 并将颜料纳米颗粒收集在收集液中。
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公开(公告)号：US07785390B2
公开(公告)日：2010-08-31
申请号：US11838638
申请日：2007-08-14
CPC分类号： B22F9/22 , B22F1/0011 , B22F1/0014
摘要： Molybdenum metal powder has surface-area-to-mass-ratios in a range of between about 1.0 meters2/gram (m2/g) and about 3.0 m2/g, as determined by BET analysis, in combination with a particle size wherein at least 30% of the particles are larger than a size +100 standard Tyler mesh sieve. A method for producing molybdenum metal powder includes providing a supply of ammonium molybdate and a reducing gas; causing an exothermic reaction between the ammonium molybdate and the reducing gas at a first temperature to produce an intermediate reaction product and a supplemental reducing gas; causing an endothermic reaction between the intermediate reaction product and the reducing gas at a final temperature to produce the molybdenum metal powder.
摘要翻译： 钼金属粉末通过BET分析测定的表面积与质量比在约1.0m 2 / g（m 2 / g）至约3.0m 2 / g之间的范围内，与至少 30％的颗粒大于+100标准泰勒筛网。 一种生产钼金属粉末的方法包括：提供钼酸铵和还原气体; 在第一温度下引起钼酸铵和还原气体之间的放热反应，产生中间反应产物和补充还原气体; 在最终温度下引起中间反应产物和还原气体之间的吸热反应以产生钼金属粉末。
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公开(公告)号：US07575711B2
公开(公告)日：2009-08-18
申请号：US12107641
申请日：2008-04-22
IPC分类号： C22B11/00
CPC分类号： B22F9/12 , B22F2998/00 , C22B9/003 , C22B11/02 , Y02P10/253 , B22F1/0018
摘要： Apparatus for producing silver nano-particle material. The apparatus includes a furnace containing a crucible for vaporizing a precursor material, as well as, a conduit disposed in perpendicular to the crucible. An inlet end of the conduit is open to the mixing region created between the conduit and the crucible. A process gas supply is also operatively associated with the mixing region.
摘要翻译： 用于生产银纳米颗粒材料的设备。 该装置包括含有用于蒸发前体材料的坩埚的炉，以及垂直于坩埚设置的导管。 导管的入口端通向导管和坩埚之间产生的混合区域。 处理气体供应也可操作地与混合区域相关联。
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公开(公告)号：US07384448B2
公开(公告)日：2008-06-10
申请号：US10780239
申请日：2004-02-16
IPC分类号： B22F9/06
CPC分类号： B22F9/12 , B22F2998/00 , C22B9/003 , C22B11/02 , Y02P10/253 , B22F1/0018
摘要： Apparatus for producing silver nano-particle material comprises a furnace and a crucible positioned within the furnace, the crucible containing a quantity of precursor material, the furnace heating the quantity of precursor material contained in the crucible to vaporize the precursor material. A process gas supply operatively associated with the furnace provides a process gas to an interior region of the furnace. A conduit is operatively associated with the furnace so that an inlet end of the conduit is open to the interior region of the furnace. A particle separator system is operatively associated with an outlet end of the conduit. A pump operatively associated with an outlet end of the particle separator system causes a mixture of process gas and vaporized precursor material contained in the interior region of the furnace to be drawn into the inlet end of the conduit, the process gas cooling the vaporized precursor material to precipitate the silver nano-particle material in a carrier stream, the particle separator system separating the silver nano-particle material from the carrier stream.
摘要翻译： 用于生产银纳米颗粒材料的装置包括炉和置于炉内的坩埚，该坩埚含有一定数量的前体材料，该炉加热包含在坩埚中的前体材料的数量以汽化前体材料。 可操作地与炉子相关联的工艺气体供应器将工艺气体提供给炉子的内部区域。 管道与炉子可操作地相关联，使得管道的入口端向炉的内部区域敞开。 颗粒分离器系统与管道的出口端可操作地相关联。 与颗粒分离器系统的出口端可操作地相关联的泵引起包含在炉内部区域中的工艺气体和蒸发的前体材料的混合物被吸入到导管的入口端，该工艺气体冷却蒸发的前体材料 以将银纳米颗粒材料沉淀在载体流中，该颗粒分离器系统将银纳米颗粒材料与载体流分离。
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