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1.发明申请SEPARATION IMPROVEMENT IN A METHOD OF PRODUCING ALKYL ESTERS FROM VEGETABLE OR ANIMAL OIL AND AN ALIPHATIC MONOALCOHOL 失效从蔬菜或动物油和阿拉伯糖醇生产碱性酯的方法中的分离改进公开(公告)号：US20100286436A1
公开(公告)日：2010-11-11
申请号：US12667146
申请日：2008-06-09
摘要： The present invention describes a method of producing fatty acid alkyl esters and glycerin implementing, in a reaction section, a set of transesterification reactions between a vegetable or animal oil and an aliphatic monoalcohol, and using a heterogeneous solid catalyst, comprising: a) a glycerin phase introduction stage, b) an excess alcohol evaporation stage, and c) a glycerin phase decantation stage. The supernatant ester phase obtained after decantation is then optionally sent to a coalescer, also allowing separation of the glycerin, then to a purification stage by adsorption on solids. This improved method prevents microemulsion formation.
摘要翻译： 本发明描述了一种生产脂肪酸烷基酯和甘油的方法，其在反应部分中实施植物油或动物油与脂族一元醇之间的一组酯交换反应，并使用非均相固体催化剂，其包括：a）甘油 相引入阶段，b）过量醇蒸发阶段，和c）甘油相倾析阶段。 然后将倾析后获得的上清液相可选地送至聚结器，还允许甘油分离，然后通过吸附在固体上进行纯化阶段。 这种改进的方法防止微乳液形成。
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2.发明授权Separation improvement in a method of producing alkyl esters from vegetable or animal oil and an aliphatic monoalcohol 失效从植物油或动物油和脂肪族一元醇生产烷基酯的方法中的分离改进公开(公告)号：US08519171B2
公开(公告)日：2013-08-27
申请号：US12667146
申请日：2008-06-09
摘要： The present invention describes a method of producing fatty acid alkyl esters and glycerin implementing, in a reaction section, a set of transesterification reactions between a vegetable or animal oil and an aliphatic monoalcohol, and using a heterogeneous solid catalyst, comprising: a) a glycerin phase introduction stage, b) an excess alcohol evaporation stage, and c) a glycerin phase decantation stage. The supernatant ester phase obtained after decantation is then optionally sent to a coalescer, also allowing separation of the glycerin, then to a purification stage by adsorption on solids. This improved method prevents microemulsion formation.
摘要翻译： 本发明描述了一种生产脂肪酸烷基酯和甘油的方法，其在反应部分中实施植物油或动物油与脂族一元醇之间的一组酯交换反应，并使用非均相固体催化剂，其包括：a）甘油 相引入阶段，b）过量醇蒸发阶段，和c）甘油相倾析阶段。 然后将倾析后获得的上清液相可选地送至聚结器，还允许甘油分离，然后通过吸附在固体上进行纯化阶段。 这种改进的方法防止微乳液形成。
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3.发明申请DECANTATION IMPROVEMENT IN A METHOD OF PRODUCING ALKYL ESTERS FROM VEGETABLE OR ANIMAL OIL AND AN ALIPHATIC MONOALCOHOL 失效从蔬菜或动物油和阿拉伯糖醇生产烷基酯的方法中的表征改进公开(公告)号：US20100292493A1
公开(公告)日：2010-11-18
申请号：US12666885
申请日：2008-06-09
摘要： The present invention describes a method of producing fatty acid alkyl esters and glycerin implementing, in a reaction section, a set of transesterification reactions between a vegetable or animal oil and an aliphatic monoalcohol, and using a heterogeneous solid catalyst, comprising: a) a stage of recontacting the effluent coming from the reaction section, and separated from the excess alcohol, with a glycerin phase, b) a stage of mixing said effluent with said glycerin phase, and c) a glycerin phase decantation stage. The supernatent ester phase obtained after decantation is then optionally sent to a coalescer, also allowing separation of the glycerin, then to a purification stage by adsorption on solids.
摘要翻译： 本发明描述了一种生产脂肪酸烷基酯和甘油的方法，其在反应部分中实施植物油或动物油与脂族一元醇之间的一组酯交换反应，并使用非均相固体催化剂，其包括：a） 重新反应来自反应段的流出物，并与过量的醇分离出甘油相，b）将所述流出物与所述甘油相混合的阶段，和c）甘油相倾析阶段。 然后将倾析后获得的上清液相可选地送至聚结器，还允许甘油分离，然后通过在固体上吸附进入纯化阶段。
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4.发明授权Decantation improvement in a method of producing alkyl esters from vegetable or animal oil and an aliphatic monoalcohol 失效从植物油或动物油和脂肪族一元醇生产烷基酯的方法中的倾析改进公开(公告)号：US08350071B2
公开(公告)日：2013-01-08
申请号：US12666885
申请日：2008-06-09
IPC分类号： C11C3/00
摘要： The present invention describes a method of producing fatty acid alkyl esters and glycerin implementing, in a reaction section, a set of transesterification reactions between a vegetable or animal oil and an aliphatic monoalcohol, and using a heterogeneous solid catalyst, comprising: a) a stage of recontacting the effluent coming from the reaction section, and separated from the excess alcohol, with a glycerin phase, b) a stage of mixing said effluent with said glycerin phase, and c) a glycerin phase decantation stage. The supernatent ester phase obtained after decantation is then optionally sent to a coalescer, also allowing separation of the glycerin, then to a purification stage by adsorption on solids.
摘要翻译： 本发明描述了一种生产脂肪酸烷基酯和甘油的方法，其在反应部分中实施植物油或动物油与脂族一元醇之间的一组酯交换反应，并使用非均相固体催化剂，其包括：a） 重新反应来自反应段的流出物，并与过量的醇分离出甘油相，b）将所述流出物与所述甘油相混合的阶段，和c）甘油相倾析阶段。 然后将倾析后获得的上清液相可选地送至聚结器，还允许甘油分离，然后通过在固体上吸附进入纯化阶段。
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