Method for reducing heat treatment residual stresses in super-solvus solutioned nickel-base superalloy articles
    1.
    发明授权
    Method for reducing heat treatment residual stresses in super-solvus solutioned nickel-base superalloy articles 有权
    超溶剂镍基超级合金制品中热处理残余应力的降低方法

    公开(公告)号:US07138020B2

    公开(公告)日:2006-11-21

    申请号:US10685640

    申请日:2003-10-15

    CPC classification number: C22F1/10

    Abstract: In accordance with an embodiment of the present invention, a method for reducing residual stress in a nickel-base superalloy article comprising about 40–70% of gamma prime phase and having a gamma prime solvus temperature is disclosed. The method comprises the steps of super-solvus heat treating the superalloy article about 5–40° F. (3–22° C.) above the gamma prime solvus temperature; and holding at the super-solvus heat treatment temperature for about 0.25–2 hours, wherein the heat-treated superalloy article has reduced residual stress.

    Abstract translation: 根据本发明的一个实施方案,公开了一种减少镍基超级合金制品中残留应力的方法,该方法包括约40-70%的γ原相并具有γ'固溶体温度。 该方法包括以下步骤:将超合金制品在伽马质子溶质温度以上约5-40°F(3-22℃)进行超溶剂热处理; 并在超溶剂热处理温度下保持约0.25-2小时,其中热处理的超合金制品具有降低的残余应力。

    Method of controlling final grain size in supersolvus heat treated nickel-base superalloys and articles formed thereby
    3.
    发明授权
    Method of controlling final grain size in supersolvus heat treated nickel-base superalloys and articles formed thereby 有权
    控制超级热处理镍基超级合金中的最终粒度的方法及由此形成的制品

    公开(公告)号:US07763129B2

    公开(公告)日:2010-07-27

    申请号:US11379203

    申请日:2006-04-18

    CPC classification number: C22F1/10 C22C19/056 C22C19/057

    Abstract: A method of forming a component from a gamma-prime precipitation-strengthened nickel-base superalloy so that, following a supersolvus heat treatment the component characterized by a uniformly-sized grain microstructure. The method includes forming a billet having a sufficiently fine grain size to achieve superplasticity of the superalloy during a subsequent working step. The billet is then worked at a temperature below the gamma-prime solvus temperature of the superalloy so as to form a worked article, wherein the billet is worked so as to maintain strain rates above a lower strain rate limit to control average grain size and below an upper strain rate limit to avoid critical grain growth. Thereafter, the worked article is heat treated at a temperature above the gamma-prime solvus temperature of the superalloy for a duration sufficient to uniformly coarsen the grains of the worked article, after which the worked article is cooled at a rate sufficient to reprecipitate gamma-prime within the worked article.

    Abstract translation: 一种从γ-Q析出强化的镍基超级合金形成组分的方法,使得在超溶解热处理之后,其特征在于均匀尺寸的晶粒微结构。 该方法包括形成具有足够细的晶粒尺寸的坯料,以在随后的工作步骤中实现超级合金的超塑性。 然后将坯料在低于超合金的γ'固溶温度的温度下加工,以形成加工制品,其中加工坯料以使应变速率保持在较低的应变速率极限以上以控制平均晶粒尺寸和低于 上限应变速率限制,以避免临界晶粒生长。 此后,将加工制品在高于合金的γ'溶解温度的温度下进行热处理,持续时间足以使加工制品的颗粒均匀地粗化,之后将加工制品以足以再沉淀γ- 在工作文章中。

    Isothermal forging of nickel-base superalloys in air
    5.
    发明授权
    Isothermal forging of nickel-base superalloys in air 有权
    空气中镍基超级合金的等温锻造

    公开(公告)号:US06908519B2

    公开(公告)日:2005-06-21

    申请号:US10199186

    申请日:2002-07-19

    CPC classification number: C22F1/10 C22C19/056

    Abstract: A superalloy made of a forging nickel-base superalloy such as Rene™ 88DT or ME3 is forged in a forging press having forging dies made of a die nickel-base superalloy. The forging is accomplished by heating to a forging temperature of from about 1700° F. to about 1850° F., and forging at that forging temperature and at a nominal strain rate. The die nickel-base superalloy is selected to have a creep strength of not less than a flow stress of the forging nickel-base superalloy at the forging temperature and strain rate.

    Abstract translation: 在具有由模具镍基超合金制成的锻造模具的锻压机中锻造由锻造镍基超级合金如Rene TM 88DT或ME3制成的超合金。 锻造通过加热至约1700°F至约1850°F的锻造温度并在该锻造温度和标称应变速率下锻造来实现。 选择模具镍基超级合金在锻造温度和应变速率下具有不小于锻造镍基超级合金的流动应力的蠕变强度。

    Method for preparing a nickel-base superalloy article using a two-step salt quench
    7.
    发明授权
    Method for preparing a nickel-base superalloy article using a two-step salt quench 有权
    使用两步盐淬制备镍基超级合金制品的方法

    公开(公告)号:US07033448B2

    公开(公告)日:2006-04-25

    申请号:US10662586

    申请日:2003-09-15

    CPC classification number: C22F1/10

    Abstract: An article made of a nickel-base superalloy strengthened by the presence of a gamma-prime phase is prepared by solution heat treating the nickel-base superalloy at a solutionizing temperature above a gamma-prime solvus temperature of the nickel-base superalloy, thereafter first quenching the nickel-base superalloy in a first molten salt bath maintained at a temperature of from the gamma-prime solvus temperature to about 100° F. below the gamma-prime solvus temperature, thereafter second quenching the nickel-base superalloy in a second molten salt bath maintained at a temperature below an aging temperature of the nickel-base superalloy, and thereafter precipitation heat treating the nickel-base superalloy at the aging temperature to precipitate an aged microstructure having gamma prime phase in a nickel-base matrix.

    Abstract translation: 通过在γ-基相存在下强化的镍基超级合金制成的制品是通过在高于镍基超级合金的γ'固溶温度的溶解温度下对镍基超级合金进行固溶热处理,之后首先 将镍基超级合金淬火在保持在伽马提取溶剂温度至约100°F的温度下的第一熔融盐浴中,低于伽马提取溶质温度,然后在第二次熔融 盐浴保持在低于镍基超级合金的老化温度的温度下,然后在老化温度下对镍基超级合金进行沉淀热处理,以沉淀在镍基基质中具有γ'相的老化微结构。

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