-
公开(公告)号:US4054499A
公开(公告)日:1977-10-18
申请号:US663890
申请日:1976-03-04
申请人: Masao Kawamura , Tadaaki Nishi , Hiro Tsuchiya , Syuzi Takagi
发明人: Masao Kawamura , Tadaaki Nishi , Hiro Tsuchiya , Syuzi Takagi
IPC分类号: B01J19/12 , C07D213/61 , B01J1/10
CPC分类号: B01J19/123 , C07D213/61
摘要: Pyridine is reacted with chlorine at a molar ratio of pyridine to chlorine of 0.5-10 : 1 in a gaseous phase in the presence of at least 0.2 moles, preferably 1 to 20 moles of steam per mole of pyridine under irradiation of ultraviolet rays of 2000-5000 A, thereby producing 2-chloropyridine.
摘要翻译: 吡啶与氯反应,吡啶与氯的摩尔比为0.5-10:1,气相中,在2000次紫外线照射下,每摩尔吡啶存在至少0.2摩尔,优选1〜20摩尔蒸气 -5000A,从而产生2-氯吡啶。
-
公开(公告)号:US5513675A
公开(公告)日:1996-05-07
申请号:US199935
申请日:1994-02-22
摘要: A pressurized fluid supply hose which conducts pressurized fluid discharged from a pump to a fluidically operated device is disclosed. A spiral tube formed by two spirally wound band members is fixed by caulking in one end of a steel pipe. The outer shape of the one end of the steel pipe includes a taper portion formed to slope gradually between a thin portion and an outer diameter portion. By effecting a caulking process with a caulking tool having a pressing portion extending in parallel to an outer surface of the steel pipe, the outer taper portion of the steel pipe is contracted to formed an inner taper portion at an internal surface thereof, and one end of the spiral tube is fixed to the inner taper portion. Because the spiral tube is gradually deformed along the inner taper portion of the steel pipe, it can avoided that a large clearance is formed between the two band members of the spiral tube.
摘要翻译: 公开了将从泵排出的加压流体传导到流体操作装置的加压流体供应软管。 由两个螺旋缠绕带部件形成的螺旋管通过在钢管的一端中的铆接而固定。 钢管的一端的外形包括形成为在薄部分和外径部分之间逐渐倾斜的锥形部分。 通过利用具有与钢管的外表面平行延伸的按压部的铆接工具进行铆接处理,钢管的外锥形部收缩,在其内表面形成内锥形部, 的螺旋管固定在内锥形部分上。 因为螺旋管沿着钢管的内锥部逐渐变形,所以能够避免在螺旋管的两个带状部件之间产生大的间隙。
-
公开(公告)号:US3969205A
公开(公告)日:1976-07-13
申请号:US530563
申请日:1974-12-06
申请人: Masao Kawamura , Tadaaki Nishi , Syuzi Takagi
发明人: Masao Kawamura , Tadaaki Nishi , Syuzi Takagi
IPC分类号: B01J19/12 , C07D213/61 , B01J1/10
CPC分类号: C07D213/61
摘要: Pyridine is reacted with chlorine in the presence of water by photolytic reaction under irradiation of photolytic light, using halogenated hydrocarbon such as carbon tetrachloride as a diluent. When the amount of water added exceeds at least 0.01 moles per one mole of pyridine, an effect of water addition appears, but usually addition of 0.2 to 10 moles, preferably 0.5 to 5 moles of water per one mole of pyridine makes the reaction proceed smoothly without any trouble, and ensures increase in yield and selectivity of 2-chloropyridine. The present process can be carried out in either gaseous or liquid phase.
摘要翻译: 吡啶在水的存在下通过光解反应在光解光照射下使用卤代烃如四氯化碳作为稀释剂与氯反应。 当加入的水量超过每摩尔吡啶至少0.01摩尔时,出现加水的作用,但通常每1摩尔吡啶加入0.2至10摩尔,优选0.5至5摩尔的水使反应顺利进行 没有任何麻烦,并确保提高2-氯吡啶的产率和选择性。 本方法可以在气相或液相中进行。
-
-