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1.发明申请公开(公告)号：US20050080151A1
公开(公告)日：2005-04-14
申请号：US10954212
申请日：2004-10-01
CPC分类号： C08J9/32 , B01J13/14 , C08J2203/14 , C08J2203/22
摘要： The present invention provides thermo-expansive microspheres comprising thermoplastic resinous shell and a blowing agent being encapsulated in the shell, the blowing agent which is a fluorine-containing C2-10 compound having ether linkage, being free of chlorine and bromine atoms and gasifying at a temperature not higher than the softening point of the thermoplastic resin; and also provides the production and application processes thereof. The thermo-expansive microspheres have preferably an average particle size ranging from 1 to 100 μm and a CV, or coefficient of variation, of particle size distribution being 30% or less, and a retaining ratio of blowing agent encapsulated being 90% or more. The thermo-expansive microspheres have low environmental loading and superior flame-retardant or flame-resistant performance, and have particle sizes distributing in narrow ranges. Those thermo-expansive microspheres and foamed hollow microspheres are suitable for applying to fire-proof paints, flame-retardant or flame-resistant thermo-insulating materials, flame-retardant or flame-resistant lightweight fillers, and flame-retardant or flame-resistant lightweight molded products, in addition to the conventional application field.
摘要翻译： 本发明提供包含热塑性树脂壳和封装在壳中的发泡剂的热膨胀性微球，发泡剂是具有醚键的含氟C2-10化合物，不含氯和溴原子，并在 温度不高于热塑性树脂的软化点; 并提供其生产和应用程序。 热膨胀性微球体的平均粒径优选为1〜100μm，粒径分布的CV或变异系数为30％以下，发泡剂的保持率为90％以上。 热膨胀微球具有低环境负荷和优异的阻燃或阻燃性能，并且粒度分布范围窄。 这些热膨胀微球和发泡中空微球适用于防火涂料，阻燃或阻燃绝热材料，阻燃或阻燃轻质填料，以及阻燃或阻燃轻质 模制产品，除了常规应用领域。
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2.发明授权公开(公告)号：US07994229B2
公开(公告)日：2011-08-09
申请号：US12068430
申请日：2008-02-06
IPC分类号： C08J9/32
CPC分类号： C08J9/32 , B01J13/14 , C08J2203/14 , C08J2203/22
摘要： The present invention provides a process for producing thermo-expansive microspheres comprising a thermoplastic resinous shell and a blowing agent being encapsulated in the shell, the blowing agent which is a fluorine-containing C2-10 compound having ether linkage, being free of chlorine and bromine atoms and gasifying at a temperature not higher than the softening point of the thermoplastic resin. The thermo-expansive microspheres have preferably an average particle size ranging from 1 to 100 μm and a CV, or coefficient of variation, of particle size distribution being 30% or less, and a retaining ratio of blowing agent encapsulated being 90% or more.
摘要翻译： 本发明提供一种包含热塑性树脂壳和包封在壳中的发泡剂的热膨胀性微球的方法，发泡剂是具有醚键的含氟C2-10化合物，不含氯和溴 原子并在不高于热塑性树脂的软化点的温度下气化。 热膨胀性微球的平均粒径优选为1〜100μm，粒径分布的CV或变异系数为30％以下，发泡剂的保持率为90％以上。
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3.发明申请公开(公告)号：US20070154711A1
公开(公告)日：2007-07-05
申请号：US10595910
申请日：2004-11-15
CPC分类号： C08J9/22 , B01J13/04 , B01J13/14 , C08J9/32 , C08J2203/142 , Y10T428/2985 , Y10T428/2987 , Y10T428/2991
摘要： A production process for heat-expanded microspheres comprising the step of providing a gaseous fluid containing heat-expandable microspheres, which comprise shell of thermoplastic resin and a blowing agent encapsulated therein having a boiling point not higher than the softening point of the thermoplastic resin and have an average particle size from 1 to 100 μm, feeding the gaseous fluid through a gas-introducing tube having a dispersion nozzle on its outlet and being fixed inside a hot gas flow, and emitting a jet of the gaseous fluid through the dispersion nozzle; a step wherein the gaseous fluid is collided on a collision plate fixed under the dispersion nozzle so as to disperse the heat-expandable microspheres in the hot gas flow; and a step wherein the dispersed heat-expandable microspheres are heated in the hot gas flow at a temperature not lower than their expansion initiating temperature and thus expanded. The production process results in minimum difference in the variation coefficient of particle size distribution between the microspheres before and after heat-expansion, slight ratio of raw microspheres and slightly expanded microspheres contained in resultant heat-expanded microspheres, and suppressed formation of aggregated microspheres.
摘要翻译： 一种热膨胀微球的制造方法，包括以下步骤：提供包含热膨胀性微球的气态流体，其包含热塑性树脂壳和封装在其中的发泡剂，沸点不高于热塑性树脂的软化点，并具有 平均粒度为1〜100μm，通过具有分散喷嘴的气体导入管在其出口处供给气体流体并固定在热气流内，并通过分散喷嘴喷射气态流体; 其中气态流体碰撞在固定在分散喷嘴下方的碰撞板上，以将热膨胀性微球分散在热气流中; 以及在热气流中以不低于其膨胀开始温度的温度加热分散的热膨胀性微球从而膨胀的步骤。 生产过程导致热膨胀前后的微球之间的粒度分布的变异系数的差异最小，所得热膨胀微球中所含的微生物微球和微球的微小比例，抑制聚集的微球的形成。
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4.发明授权公开(公告)号：US07807729B2
公开(公告)日：2010-10-05
申请号：US10595910
申请日：2004-11-15
CPC分类号： C08J9/22 , B01J13/04 , B01J13/14 , C08J9/32 , C08J2203/142 , Y10T428/2985 , Y10T428/2987 , Y10T428/2991
摘要： A production process for heat-expanded microspheres includes the step of providing a gaseous fluid containing heat-expandable microspheres, which includes a shell of thermoplastic resin and a blowing agent encapsulated therein having a boiling point not higher than the softening point of the thermoplastic resin and have an average particle size from 1 to 100 μm. The gaseous fluid is fed through a gas-introducing tube having a dispersion nozzle on its outlet that is fixed inside a conduit having a hot gas flow flowing therethrough. A jet of the gaseous fluid is emitted through the dispersion nozzle. Further, the gaseous fluid is collided on a collision plate fixed under the dispersion nozzle so as to disperse the heat-expandable microspheres in the hot gas flow. The dispersed heat-expandable microspheres are heated in the hot gas flow at a temperature not lower than their expansion initiating temperature and thus expanded.
摘要翻译： 热膨胀微球的制造方法包括提供含有热膨胀性微球的气态流体的步骤，其包括热塑性树脂的壳和封装在其中的沸点不高于热塑性树脂的软化点的发泡剂， 平均粒径为1〜100μm。 气体流体通过其出口上具有分散喷嘴的气体导入管被供给，该出口固定在具有流过其中的热气流的管道内。 气体流体的射流通过分散喷嘴发射。 此外，气体流体在固定在分散喷嘴下方的碰撞板上碰撞，以将热膨胀性微球分散在热气流中。 分散的热膨胀性微球体在热气流中以不低于其膨胀开始温度的温度加热，从而膨胀。
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5.发明授权Inner plug and cap for liquid injection containers, and jig used to fix cap to inner plug 有权用于液体注射容器的内部塞子和盖子，以及用于将盖子固定到内部塞子上的夹具公开(公告)号：US06247605B1
公开(公告)日：2001-06-19
申请号：US09463060
申请日：2000-01-19
申请人： Takashi Fujie , Masaru Tamura , Takao Kishi
发明人： Takashi Fujie , Masaru Tamura , Takao Kishi
IPC分类号： B65D4134
CPC分类号： B65D47/103 , B65D47/123 , B65D2101/00 , B65D2565/385 , Y10T29/53961 , Y10T29/53978
摘要： The present invention provides an inner plug easily removable from a neck of a container, and a cap for covering the inner plug. The inner plug comprises an engaging portion to be fitted to a neck of the container, a threaded cylinder and a lip cylinder connected to said threaded cylinder. The engaging portion comprises an inner cylinder, an outer cylinder and a shoulder wall. The threaded cylinder is arranged on the inner cylinder. The cap has a side cylinder to be engaged with said threaded cylinder of said inner plug, and a cover cylinder covering said shoulder wall and said outer cylinder. The cover cylinder has a diameter larger than a diameter of said side cylinder. The outer cylinder is provided with a cut portion. The shoulder wall is provided with a cut portion connecting to said cut portion of the outer cylinder. The shoulder wall is provided on a lower surface thereof with a tear off groove along the outer cylinder. The groove is connected to said cut portion of the shoulder wall. Also, a jig for holding an inner plug unrotatably is provided.
摘要翻译： 本发明提供一种容易从容器颈部移除的内塞和用于覆盖内塞的盖。 所述内塞包括与所述容器的颈部配合的接合部分，螺纹圆筒和连接到所述螺纹圆筒的唇形圆筒。 接合部分包括内筒，外筒和肩壁。 螺纹圆筒布置在内筒上。 盖具有与所述内塞的所述螺纹圆筒接合的侧圆筒，以及覆盖所述肩部壁和所述外筒的盖圆筒。 盖筒的直径大于所述侧筒的直径。 外筒设有切口部。 肩部壁设置有连接到外筒的切割部分的切口部分。 肩壁在其下表面上设置有沿着外筒的撕开槽。 凹槽连接到肩壁的所述切割部分。 另外，提供了用于不能旋转地保持内塞的夹具。
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公开(公告)号：US5531339A
公开(公告)日：1996-07-02
申请号：US335883
申请日：1994-11-15
申请人： Nobuo Yamanaka , Takashi Fujie , Hiroshi Hidaka , Yoshio Akiyama
发明人： Nobuo Yamanaka , Takashi Fujie , Hiroshi Hidaka , Yoshio Akiyama
CPC分类号： B65D1/0207 , B05B11/0037 , B29B17/02 , B29B2017/0203 , B29K2023/06 , B29K2023/12 , B29K2025/00 , B29K2077/00 , B29L2031/7158 , B65D2501/0054 , Y02W30/622 , Y10S215/90
摘要： The present invention relates to a bottle made of synthetic resin, for containing various liquids, that can be easily fractured for easier handling during disposal or recycling. The bottle comprises a plurality of fracturing walls, each formed in a longitudinal band shape extending substantially in a direction of a central axis of the bottle, and main walls each disposed between the fracturing walls. The fracturing walls are made of a first material and a second material, the first material being a synthetic resin that is the same as a synthetic resin forming the main walls and/or has good compatibility with the synthetic resin of the main walls, the second material being a synthetic resin that has poor compatibility with the synthetic resin of the main walls. The bonding strength between the fracturing walls and the main walls is controlled so as to make the bottle easily fractured. If necessary, an inner covering member can be assembled within the bottle.
摘要翻译： PCT No.PCT / JP94 / 00413 Sec。 371日期：1994年11月15日 102（e）日期1994年11月15日PCT 1994年3月15日PCT公布。 公开号WO94 / 21521 日本公报1994年9月29日。本发明涉及一种由合成树脂制成的瓶子，用于容纳各种液体，在处理或再循环过程中易于破碎以便于处理。 瓶子包括多个压裂壁，每个压裂壁形成为沿着瓶的中心轴线方向延伸的纵向带状，以及分别设置在压裂壁之间的主壁。 压裂壁由第一材料和第二材料制成，第一材料是与形成主壁的合成树脂相同和/或与主壁的合成树脂具有良好相容性的合成树脂，第二材料 材料是与主壁的合成树脂具有差的相容性的合成树脂。 控制压裂壁与主壁之间的粘结强度，使瓶易于断裂。 如果需要，可以在瓶内装配内覆盖构件。
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7.发明申请公开(公告)号：US20080293838A1
公开(公告)日：2008-11-27
申请号：US12068430
申请日：2008-02-06
CPC分类号： C08J9/32 , B01J13/14 , C08J2203/14 , C08J2203/22
摘要： The present invention provides a process for producing thermo-expansive microspheres comprising a thermoplastic resinous shell and a blowing agent being encapsulated in the shell, the blowing agent which is a fluorine-containing C2-10 compound having ether linkage, being free of chlorine and bromine atoms and gasifying at a temperature not higher than the softening point of the thermoplastic resin. The thermo-expansive microspheres have preferably an average particle size ranging from 1 to 100 μm and a CV, or coefficient of variation, of particle size distribution being 30% or less, and a retaining ratio of blowing agent encapsulated being 90% or more.
摘要翻译： 本发明提供一种包含热塑性树脂壳和包封在壳中的发泡剂的热膨胀性微球的方法，发泡剂是具有醚键的含氟C2-10化合物，不含氯和溴 原子并在不高于热塑性树脂的软化点的温度下气化。 热膨胀性微球体的平均粒径优选为1〜100μm，粒径分布的CV或变异系数为30％以下，发泡剂的保持率为90％以上。
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8.发明授权Inner plug and cap for liquid injection containers, and jig used to fix cap to inner plug 有权用于液体注射容器的内部塞子和盖子，以及用于将盖子固定到内部塞子上的夹具公开(公告)号：US06574848B2
公开(公告)日：2003-06-10
申请号：US09819700
申请日：2001-03-29
申请人： Takashi Fujie , Masaru Tamura , Takao Kishi
发明人： Takashi Fujie , Masaru Tamura , Takao Kishi
IPC分类号： B25B2714
CPC分类号： B65D47/103 , B65D47/123 , B65D2101/00 , B65D2565/385 , Y10T29/53961 , Y10T29/53978
摘要： The present invention provides an inner plug easily removable from a neck of a container, and a cap for covering the inner plug. The inner plug comprises an engaging portion to be fitted to a neck of the container, a threaded cylinder, and a lip cylinder connected to the threaded cylinder. The engaging portion comprises an inner cylinder, an outer cylinder, and a shoulder wall. The threaded cylinder is arranged on the inner cylinder. The cap has a side cylinder to be engaged with the threaded cylinder of the inner plug, and a cover cylinder covering the shoulder wall and the outer cylinder. The cover cylinder has a diameter larger than a diameter of the side cylinder. The outer cylinder is provided with a cut portion. The shoulder wall is provided with a cut portion connecting to the cut portion of the outer cylinder. The shoulder wall is provided on a lower surface thereof with a tear off groove along the outer cylinder. The groove is connected to the cut portion of the shoulder wall. Also, a jig for holding an inner plug unrotatably is provided.
摘要翻译： 本发明提供一种容易从容器颈部移除的内塞和用于覆盖内塞的盖。 内塞包括一个与容器的颈部相配合的接合部分，一个带螺纹的圆柱体和一个连接到螺纹圆筒的唇形圆筒。 接合部分包括内筒，外筒和肩壁。 螺纹圆筒布置在内筒上。 盖具有与内塞的螺纹圆筒接合的侧圆筒和覆盖肩部壁和外筒的盖筒。 盖筒的直径大于侧筒的直径。 外筒设有切口部。 肩部壁设置有连接到外筒的切口部分的切口部分。 肩壁在其下表面上设置有沿着外筒的撕开槽。 凹槽连接到肩壁的切割部分。 另外，提供了用于不能旋转地保持内塞的夹具。
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9.发明授权公开(公告)号：US07351752B2
公开(公告)日：2008-04-01
申请号：US10954212
申请日：2004-10-01
IPC分类号： C08J9/00
CPC分类号： C08J9/32 , B01J13/14 , C08J2203/14 , C08J2203/22
摘要： The present invention provides thermo-expansive microspheres comprising thermoplastic resinous shell and a blowing agent being encapsulated in the shell, the blowing agent which is a fluorine-containing C2-10 compound having ether linkage, being free of chlorine and bromine atoms and gasifying at a temperature not higher than the softening point of the thermoplastic resin; and also provides the production and application processes thereof. The thermo-expansive microspheres have preferably an average particle size ranging from 1 to 100 μm and a CV, or coefficient of variation, of particle size distribution being 30% or less, and a retaining ratio of blowing agent encapsulated being 90% or more.The thermo-expansive microspheres have low environmental loading and superior flame-retardant or flame-resistant performance, and have particle sizes distributing in narrow ranges. Those thermo-expansive microspheres and foamed hollow microspheres are suitable for applying to fire-proof paints, flame-retardant or flame-resistant thermo-insulating materials, flame-retardant or flame-resistant lightweight fillers, and flame-retardant or flame-resistant lightweight molded products, in addition to the conventional application field.
摘要翻译： 本发明提供了包含热塑性树脂壳和封装在壳中的发泡剂的热膨胀性微球，发泡剂是具有醚键的含氟C 2-10 - 化合物，不含 氯和溴原子，并且在不高于热塑性树脂的软化点的温度下气化; 并提供其生产和应用程序。 热膨胀性微球体的平均粒径优选为1〜100μm，粒径分布的CV或变异系数为30％以下，发泡剂的保持率为90％以上。 热膨胀微球具有低环境负荷和优异的阻燃或阻燃性能，并且粒度分布范围窄。 这些热膨胀微球和发泡中空微球适用于防火涂料，阻燃或阻燃绝热材料，阻燃或阻燃轻质填料，以及阻燃或阻燃轻质 模制产品，除了常规应用领域。
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