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    Process for preparing hydroxyalkylaminosulfonic acids
    1.
    发明授权
    Process for preparing hydroxyalkylaminosulfonic acids 失效
    制备羟烷基氨基磺酸的方法

    公开(公告)号：US4582651A

    公开(公告)日：1986-04-15

    申请号：US599823

    申请日：1984-04-13

    申请人： Keizou Ishii ,  Ryuzo Mizuguchi ,  Shinichi Ishikura ,  Tamotsu Yoshioka

    发明人： Keizou Ishii ,  Ryuzo Mizuguchi ,  Shinichi Ishikura ,  Tamotsu Yoshioka

    IPC分类号： A61K31/38 ,  A61K31/40 ,  A61K31/415 ,  C07D207/16 ,  C07D231/06 ,  C07C143/02 ,  C07C101/30

    CPC分类号： C07D231/06 ,  A61K31/38 ,  A61K31/40 ,  A61K31/415 ,  C07D207/16 ,  Y10S516/05 ,  Y10S516/91

    摘要： A process for preparing hydroxyalkylaminosulfonic acids which comprises reacting a hydroxyalkylamine of the formula: ##STR1## wherein R.sub.1 is a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, and R.sub.2 is a hydrogen atom, a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, or a lower alkyl group, with an alkali metal salt of an .alpha.,.beta.-unsaturated sulfonic acid of the formula: ##STR2## wherein R.sub.3 is a hydrogen atom or a methyl group and M is an alkali metal, followed by elimination of the alkali metal to give a hydroxyalkylaminosulfonic acid of the formula: ##STR3## wherein R.sub.1 and R.sub.3 are each as defined above and R.sub.2 ' is a hydrogen atom, a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, a lower alkyl group or a group of the formula: ##STR4## wherein R.sub.3 is as defined above.

    摘要翻译： 一种制备羟烷基氨基磺酸的方法，其包括使下式的羟烷基胺反应：其中R1是在烷基链中任选含有-O-或-COO-的C1-C20羟基烷基，R2是氢原子 ，在烷基链或低级烷基中任选含有-O-或-COO-的C1-C20羟烷基，与下式的α，β-不饱和磺酸的碱金属盐反应：（III） ）其中R3是氢原子或甲基，M是碱金属，然后除去碱金属，得到下式的羟烷基氨基磺酸：其中R 1和R 3各自如上所定义，和 R2'是氢原子，在烷基链中任选地含有-O-或-COO-的C 1 -C 20羟基烷基，低级烷基或下式的基团：其中R 3如上所定义。

    Polymerizable amino acid compounds and their production
    2.
    发明授权
    Polymerizable amino acid compounds and their production 失效
    可聚合氨基酸化合物及其生产

    公开(公告)号：US4452746A

    公开(公告)日：1984-06-05

    申请号：US372729

    申请日：1982-04-28

    申请人： Shinichi Ishikura ,  Tamotsu Yoshioka ,  Ryuzo Mizuguchi

    发明人： Shinichi Ishikura ,  Tamotsu Yoshioka ,  Ryuzo Mizuguchi

    IPC分类号： C07D295/088 ,  C08F12/26 ,  C07C143/58

    CPC分类号： C07D295/088 ,  C08F12/26

    摘要： A polymerizable amino acid compound of the formula: ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 are each hydrogen or methyl, R.sub.4 is C.sub.1 -C.sub.20 alkyl optionally bearing at least one hydroxyl and optionally having --O-- or --COO-- in the alkyl chain, R.sub.5 is hydrogen or C.sub.1 -C.sub.20 alkyl optionally bearing at least one hydroxyl and optionally having --O-- or --COO-- in the alkyl chain, or when R.sub.4 and R.sub.5 are taken together with the nitrogen atom to which they are attached, they represent a nitrogen atom containing heterocyclic group, R.sub.6 is an alkylene group having not more than 6 carbon atoms and A is --COO-- or --SO.sub.3 --, provided that when R.sub.4 is C.sub.1 -C.sub.20 alkyl, R.sub.5 is not hydrogen, which is highly soluble in water or organic solvents without any acidic or basic substance and can be introduced into the molecule of high molecular compounds.

    摘要翻译： 下式的可聚合氨基酸化合物：其中R 1，R 2和R 3各自为氢或甲基，R 4为任选带有至少一个羟基且任选在烷基链中具有-O-或-COO-的C 1 -C 20烷基 R 5为氢或任选具有至少一个羟基且任选在烷基链中具有-O-或-COO-的C 1 -C 20烷基，或者当R 4和R 5与它们所连接的氮原子一起时，它们代表 含有氮原子的杂环基，R6是不大于6个碳原子的亚烷基，A是-COO-或-SO3-，条件是当R 4为C 1 -C 20烷基时，R 5不是氢，其高度可溶于 水或有机溶剂，无任何酸性或碱性物质，并可引入高分子化合物分子。

    Polymerizable amino acid compounds and their production
    3.
    发明授权
    Polymerizable amino acid compounds and their production 失效
    可聚合氨基酸化合物及其生产

    公开(公告)号：US4543216A

    公开(公告)日：1985-09-24

    申请号：US594826

    申请日：1984-03-29

    申请人： Shinichi Ishikura ,  Tamotsu Yoshioka ,  Ryuzo Mizuguchi

    发明人： Shinichi Ishikura ,  Tamotsu Yoshioka ,  Ryuzo Mizuguchi

    IPC分类号： C07D295/088 ,  C08F12/26 ,  C07C143/68

    CPC分类号： C07D295/088 ,  C08F12/26

    摘要： A polymerizable amino acid compound of the formula: ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 are each hydrogen or methyl, R.sub.4 is C.sub.1 -C.sub.20 alkyl optionally bearing at least one hydroxyl and optionally having --O-- or --COO-- in the alkyl chain, R.sub.5 is hydrogen or C.sub.1 -C.sub.20 alkyl optionally bearing at least one hydroxyl and optionally having --O-- or --COO-- in the alkyl chain, or when R.sub.4 and R.sub.5 are taken together with the nitrogen atom to which they are attached, they represent a nitrogen atom containing heterocyclic group, R.sub.6 is an alkylene group having not more than 6 carbon atoms and A is --COO-- or --SO.sub.3 --, provided that when R.sub.4 is C.sub.1 -C.sub.20 alkyl, R.sub.5 is not hydrogen, which is highly soluble in water or organic solvents without any acidic or basic substance and can be introduced into the molecule of high molecular compounds.

    摘要翻译： 下式的可聚合氨基酸化合物：其中R 1，R 2和R 3各自为氢或甲基，R 4为任选带有至少一个羟基且任选在烷基链中具有-O-或-COO-的C 1 -C 20烷基 R 5为氢或任选具有至少一个羟基且任选在烷基链中具有-O-或-COO-的C 1 -C 20烷基，或者当R 4和R 5与它们所连接的氮原子一起时，它们代表 含有氮原子的杂环基，R6是不大于6个碳原子的亚烷基，A是-COO-或-SO3-，条件是当R 4为C 1 -C 20烷基时，R 5不是氢，其高度可溶于 水或有机溶剂，无任何酸性或碱性物质，并可引入高分子化合物分子。

    Process for preparing hydroxyalkylaminosulfonic acids
    5.
    发明授权
    Process for preparing hydroxyalkylaminosulfonic acids 失效
    制备羟烷基氨基磺酸的方法

    公开(公告)号：US4481150A

    公开(公告)日：1984-11-06

    申请号：US412977

    申请日：1982-08-27

    申请人： Keizou Ishii ,  Ryuzo Mizuguchi ,  Shinichi Ishikura ,  Tamotsu Yoshioka

    发明人： Keizou Ishii ,  Ryuzo Mizuguchi ,  Shinichi Ishikura ,  Tamotsu Yoshioka

    IPC分类号： C07C309/14 ,  C07C143/02

    CPC分类号： C07C309/14

    摘要： A process for preparing hydroxyalkylaminosulfonic acids which comprises reacting a hydroxyalkylamine of the formula: ##STR1## wherein R.sub.1 is a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, and R.sub.2 is a hydrogen atom, a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, or a lower alkyl group, with an alkali metal salt of an .alpha.,.beta.-unsaturated sulfonic acid of the formula: ##STR2## wherein R.sub.3 is a hydrogen atom or a methyl group and M is an alkali metal, followed by elimination of the alkali metal to give a hydroxyalkylaminosulfonic acid of the formula: ##STR3## wherein R.sub.1 and R.sub.3 are each as defined above and R.sub.2 ' is a hydrogen atom, a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, a lower alkyl group or a group of the formula: ##STR4## wherein R.sub.3 is as defined above.

    摘要翻译： 一种制备羟烷基氨基磺酸的方法，其包括使下式的羟烷基胺反应：其中R1是在烷基链中任选含有-O-或-COO-的C1-C20羟基烷基，R2是氢原子 ，在烷基链或低级烷基中任选含有-O-或-COO-的C1-C20羟烷基，与下式的α，β-不饱和磺酸的碱金属盐反应：（III） ）其中R3是氢原子或甲基，M是碱金属，然后除去碱金属，得到下式的羟烷基氨基磺酸：其中R 1和R 3各自如上所定义，和 R2'是氢原子，在烷基链中任选地含有-O-或-COO-的C 1 -C 20羟基烷基，低级烷基或下式的基团：其中R 3如上所定义。