公开(公告)号：US4252669A

公开(公告)日：1981-02-24

申请号：US76856

申请日：1979-09-19

申请人： Hiroji Kawai ,  Tomohiko Abe ,  Shigeru Yokono ,  Teruhiko Hoshina

发明人： Hiroji Kawai ,  Tomohiko Abe ,  Shigeru Yokono ,  Teruhiko Hoshina

IPC分类号： C09K11/77 ,  C09K11/46

CPC分类号： C09K11/7717

摘要： A luminescent material is disclosed which has the general formula:Zn.sub.1-x Cd.sub.x S:Ce.sub.y, M.sub.zwherein M is at least one alkali metal selected from Li, Na, K, Rb, and Cs, x is from about 0 to about 0.3, y and z are densities (g-atom/mol Zn.sub.1-x Cd.sub.x S) of Ce and M relative to Zn.sub.1-x Cd.sub.x S, y is from about 7.times.10.sup.-6 to about 1.5.times.10.sup.-2, and z is from about 7.times.10.sup.-6 to about 1.5.times.10.sup.-2.A method for making a luminescent material having the general formula:(ZnCd)S:Ce,Mwherein M is at least one alkali metal selected from Li, Na, K, Rb and Cs is disclosed which comprises the steps of preparing a mixture of (ZnCD)S:Ce compound, and alkali metal compound, heating the mixture under non-oxidizing atmosphere at a temperature between about 900.degree. C. and about 1170.degree. C., and quenching said mixture from said temperature.

摘要翻译： 公开了具有以下通式的发光材料：Zn1-xCdxS：Cey，Mz其中M是选自Li，Na，K，Rb和Cs中的至少一种碱金属，x为约0至约0.3，y和 z是Ce和M相对于Zn1-xCdxS的密度（g-原子/摩尔Zn1-xCdxS），y为约7×10 -6至约1.5×10 -2，z为约7×10 -6至约1.5×10 -1。 2。 公开了一种制备具有以下通式的发光材料的方法：（ZnCd）S：Ce，M其中M是选自Li，Na，K，Rb和Cs中的至少一种碱金属，其包括以下步骤： （ZnCD）S：Ce化合物和碱金属化合物，在非氧化性气氛下在约900℃至约1170℃的温度下加热混合物，并从所述温度淬灭所述混合物。

公开(公告)号：US4469619A

公开(公告)日：1984-09-04

申请号：US430952

申请日：1982-09-30

申请人： Katsutoshi Ohno ,  Tomohiko Abe ,  Teruhiko Hoshina, deceased ,  by Ikuko Hoshina, heir ,  by Aya Hoshina, heir ,  by Ken-Nosuke Hoshina, heir

发明人： Katsutoshi Ohno ,  Tomohiko Abe ,  Teruhiko Hoshina, deceased ,  by Ikuko Hoshina, heir ,  by Aya Hoshina, heir ,  by Ken-Nosuke Hoshina, heir

IPC分类号： C09K11/00 ,  C09K11/08 ,  C09K11/77 ,  C09K11/80 ,  C09K11/475

CPC分类号： C09K11/7774

摘要： A method for manufacturing a luminescent material having the formula:Y.sub.3 Al.sub.5 O.sub.12 : Tbin which the raw materials for the synthesis are combined in appropriate amounts together with a flux consisting of barium fluoride, barium chloride, or mixtures of the two and then heated in a sealed state to a temperature between about 1300.degree. C. and 1600.degree. C. The resultant product is then leached with an alkaline or acid solution to remove the residual flux from the product.

摘要翻译： 一种制造具有下式的发光材料的方法：其中将合成原料与由氟化钡，氯化钡或二者的混合物组成的助熔剂合并，然后在密封 状态至约1300℃至1600℃之间的温度。然后将所得产物用碱性或酸性溶液浸出以从产物中除去剩余的通量。