公开(公告)号：US07125502B2

公开(公告)日：2006-10-24

申请号：US10189129

申请日：2002-07-02

申请人： Richard E. Smalley ,  Rajesh Kumar Saini ,  Ramesh Sivarajan ,  Robert H. Hauge ,  Virginia Angelica Davis ,  Matteo Pasquali ,  Lars Martin Ericson

发明人： Richard E. Smalley ,  Rajesh Kumar Saini ,  Ramesh Sivarajan ,  Robert H. Hauge ,  Virginia Angelica Davis ,  Matteo Pasquali ,  Lars Martin Ericson

IPC分类号： D01F9/12

CPC分类号： B82Y15/00 ,  D01F11/12 ,  Y10S977/842

摘要： The present invention involves fibers of highly aligned single-wall carbon nanotubes and a process for making the same. The present invention provides a method for effectively dispersing single-wall carbon nanotubes. The process for dispersing the single-wall carbon nanotubes comprises mixing single-wall carbon nanotubes with 100% sulfuric acid or a superacid, heating and stirring under an inert, oxygen-free environment. The single-wall carbon nanotube/acid mixture is wet spun into a coagulant to form the single-wall carbon nanotube fibers. The fibers are recovered, washed and dried. The single-wall carbon nanotubes were highly aligned in the fibers, as determined by Raman spectroscopy analysis.

公开(公告)号：US07288238B2

公开(公告)日：2007-10-30

申请号：US10187729

申请日：2002-07-02

申请人： Richard E. Smalley ,  Rajesh Kumar Saini ,  Ramesh Sivarajan ,  Robert H. Hauge ,  Virginia Angelica Davis ,  Matteo Pasquali ,  Lars Martin Ericson ,  Satish Kumar ,  Sreekumar Thaliyil Veedu

发明人： Richard E. Smalley ,  Rajesh Kumar Saini ,  Ramesh Sivarajan ,  Robert H. Hauge ,  Virginia Angelica Davis ,  Matteo Pasquali ,  Lars Martin Ericson ,  Satish Kumar ,  Sreekumar Thaliyil Veedu

IPC分类号： D01F9/12

CPC分类号： B82Y30/00 ,  B82Y15/00 ,  B82Y40/00 ,  C01B32/168 ,  C01B32/17 ,  C01B2202/02 ,  D01F11/12 ,  Y10S977/847

摘要： The present invention involves alewives of highly aligned single-wall carbon nanotubes (SWNT), process for making the same and compositions thereof. The present invention provides a method for effectively making carbon alewives, which are discrete, acicular-shaped aggregates of aligned single-wall carbon nanotubes and resemble the Atlantic fish of the same name. Single-wall carbon nanotube alewives can be conveniently dispersed in materials such as polymers, ceramics, metals, metal oxides and liquids. The process for preparing the alewives comprises mixing single-wall carbon nanotubes with 100% sulfuric acid or a superacid, heating and stirring, and slowly introducing water into the single-wall carbon nanotube/acid mixture to form the alewives. The alewives can be recovered, washed and dried. The properties of the single-wall carbon nanotubes are retained in the alewives.

摘要翻译： 本发明涉及高度排列的单壁碳纳米管（SWNT）的制备方法，其制备方法及其组合物。 本发明提供了一种有效制备碳酸蛭石的方法，它是排列的单壁碳纳米管的离散的针状聚集体，并且类似于同名的大西洋鱼。 单壁碳纳米管麻醉剂可以方便地分散在诸如聚合物，陶瓷，金属，金属氧化物和液体的材料中。 制备麻醉剂的方法包括将单壁碳纳米管与100％硫酸或超强酸混合，加热搅拌，并将水缓慢地引入单壁碳纳米管/酸混合物中以形成啤酒。 麻醉剂可以回收，洗涤和干燥。 单壁碳纳米管的性质保留在香水中。