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公开(公告)号：US20160002095A1
公开(公告)日：2016-01-07
申请号：US14858391
申请日：2015-09-18
发明人： Tomoyuki TSUJIMURA , Manabu NISHIZAWA , Akio KOIKE
摘要： The present invention relates to an alkali-free glass having a strain point of 725° C. or higher, an average thermal expansion coefficient at from 50 to 300° C. of from 30×10−7 to 40×107/° C., a temperature T2 at which a glass viscosity is 102 dPa·s of 1,710° C. or lower, and a temperature T4 at which a glass viscosity is 104 dPa·s of 1,320° C. or lower, the alkali-free glass including, in terms of mol % on the basis of oxides, SiO2: 66 to 70, Al2O3: 12 to 15, B2O3: 0 to 1.5, MgO: more than 9.5 and 13 or less, CaO: 4 to 9, SrO: 0.5 to 4.5, BaO: 0 to 1, and ZrO2: 0 to 2, in which MgO+CaO+SrO+BaO is from 17 to 21, MgO/(MgO+CaO+SrO+BaO) is 0.4 or more, MgO/(MgO+CaO) is 0.4 or more, MgO/(MgO+SrO) is 0.6 or more, and the alkali-free glass does not substantially contain an alkali metal oxide.
摘要翻译： 本发明涉及应变点为725℃以上，50〜300℃的平均热膨胀系数为30×10-7〜40×107 /℃的无碱玻璃。 玻璃粘度为102dPa·s的温度T2为1710℃以下，玻璃粘度为104dPa·s的温度T4为1320℃以下，所述无碱玻璃包括 以氧化物为基准的摩尔％，SiO2：66〜70，Al2O3：12〜15，B2O3：0〜1.5，MgO：9.5以上13以下，CaO：4〜9，SrO：0.5〜 MgO，CaO + SrO + BaO为17〜21，MgO /（MgO + CaO + SrO + BaO）为0.4以上，MgO /（MgO + CaO）为0.4以上，MgO /（MgO + SrO）为0.6以上，无碱玻璃基本不含有碱金属氧化物。
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公开(公告)号：US20150045203A1
公开(公告)日：2015-02-12
申请号：US14524880
申请日：2014-10-27
摘要： The present invention relates to a non-alkali glass having a strain point of from 710° C. to lower than 725° C., an average thermal expansion coefficient at from 50 to 300° C. of from 30×107 to 43×10−7/° C., a temperature T2 at which glass viscosity reaches 102dPa.s of 1710° C. or lower, a temperature T4 at which the glass viscosity reaches 104 dPd.s of 1320° C. or lower, and containing, indicated by mol % on the basis of oxides, SiO2 66 to 70, Al2O3 12 to 14, B2O3 exceeding 0 to 1.5, MgO exceeding 9.5 to 13 (or 5 to 9.5), CaO 4 to 9 (or 4 to 11), SrO 0.5 to 4.5, BaO 0 to 0.5 and ZrO 0 to 2.
摘要翻译： 本发明涉及应变点为710℃以上且低于725℃，50〜300℃的平均热膨胀系数为30×107〜43×10的非碱玻璃 -7℃，玻璃粘度达到102dPa.s为1710℃以下的温度T2，玻璃粘度达到104dPd.s的温度T4为1320℃以下， 基于氧化物的摩尔％表示，SiO 2 66〜70，Al 2 O 3 12〜14，B 2 O 3超过0〜1.5，MgO超过9.5〜13（或5〜9.5），CaO 4〜9（或4〜11），SrO 0.5〜4.5，BaO 0〜0.5，ZrO 0〜2。
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公开(公告)号：US20130274086A1
公开(公告)日：2013-10-17
申请号：US13912642
申请日：2013-06-07
发明人： Tomoyuki TSUJIMURA , Manabu Nishizawa , Akio Koike
摘要： The present invention relates to an alkali-free glass having a strain point of 725° C. or higher, an average thermal expansion coefficient at from 50 to 300° C. of from 30×10−7 to 40×10−7/° C., a temperature T2 at which a glass viscosity is 102 dPa·s of 1,710° C. or lower, and a temperature T4 at which a glass viscosity is 104 dPa·s of 1,320° C. or lower, the alkali-free glass including, in terms of mol % on the basis of oxides, SiO2: 66 to 70, Al2O3: 12 to 15, B2O3: 0 to 1.5, MgO: more than 9.5 and 13 or less, CaO: 4 to 9, SrO: 0.5 to 4.5, BaO: 0 to 1, and ZrO2: 0 to 2, in which MgO+CaO+SrO+BaO is from 17 to 21, MgO/(MgO+CaO+SrO+BaO) is 0.4 or more, MgO/(MgO+CaO) is 0.4 or more, MgO/(MgO+SrO) is 0.6 or more, and the alkali-free glass does not substantially contain an alkali metal oxide.
摘要翻译： 本发明涉及应变点为725℃以上，50〜300℃的平均热膨胀系数为30×10 -7〜40×10 -7 /°的无碱玻璃 玻璃粘度为102dPa·s的温度T2为1710℃以下，玻璃粘度为104dPa·s的温度T4为1320℃以下，无碱 玻璃，以氧化物为基准的摩尔％，SiO2：66〜70，Al2O3：12〜15，B2O3：0〜1.5，MgO：9.5以上13以下，CaO：4〜9，SrO： 0.5〜4.5，BaO：0〜1，ZrO 2：0〜2，MgO + CaO + SrO + BaO为17〜21，MgO /（MgO + CaO + SrO + BaO）为0.4以上，MgO / （MgO + CaO）为0.4以上时，MgO /（MgO + SrO）为0.6以上，无碱玻璃基本不含有碱金属氧化物。
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公开(公告)号：US20150162642A1
公开(公告)日：2015-06-11
申请号：US14626248
申请日：2015-02-19
IPC分类号： H01M10/0562 , C03C21/00 , H01M10/0525 , C03C10/00
CPC分类号： H01M10/0562 , C03B19/102 , C03B32/02 , C03C1/00 , C03C3/062 , C03C4/18 , C03C8/08 , C03C10/0009 , C03C12/00 , C03C21/002 , C03C2204/00 , H01M10/052 , H01M10/0525 , H01M2300/0071
摘要： A method of manufacturing a lithium ion conductive glass ceramic, includes a step of forming granules using a material including an SiO2 source, a ZrO2 source, a P2O5 source and an Na2O source; a step of obtaining a powder including a glass ceramic by passing the granules under a heated gas phase atmosphere to melt the granules and solidifying the melted granules; a step of obtaining a target object including a glass ceramic by performing a heat treatment on the powder to precipitate crystals; and a step of obtaining a lithium ion conductive glass ceramic by performing an ion-exchange process on the target object in molten salt including lithium ions.
摘要翻译： 制造锂离子传导性玻璃陶瓷的方法包括使用包括SiO 2源，ZrO 2源，P 2 O 5源和Na 2 O源的材料形成颗粒的步骤; 通过使所述颗粒在加热的气相气氛下通过以使所述颗粒熔融并固化所述熔融颗粒来获得包括玻璃陶瓷的粉末的步骤; 通过对粉末进行热处理以获得包含玻璃陶瓷的目标物体以沉淀晶体的步骤; 以及通过对包含锂离子的熔融盐中的目标物体进行离子交换处理来获得锂离子传导性玻璃陶瓷的工序。
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公开(公告)号：US20160068427A1
公开(公告)日：2016-03-10
申请号：US14943459
申请日：2015-11-17
摘要： The present invention relates to a non-alkali glass having a strain point of from 710° C. to lower than 725° C., an average thermal expansion coefficient at from 50 to 300° C. of from 30×10−7 to 43×10−7/° C., a temperature T2 at which glass viscosity reaches 102 dPa·s of 1710° C. or lower, a temperature T4 at which the glass viscosity reaches 104 dPa·s of 1320° C. or lower, and containing, indicated by mol % on the basis of oxides, SiO2 66 to 70, Al2O3 12 to 14, B2O3 exceeding 0 to 1.5, MgO exceeding 9.5 to 13 (or 5 to 9.5), CaO 4 to 9 (or 4 to 11), SrO 0.5 to 4.5, BaO 0 to 0.5 and ZrO 0 to 2.
摘要翻译： 本发明涉及应变点为710℃以上且低于725℃的无碱玻璃，50〜300℃的平均热膨胀系数为30×10 -7〜43 ×10-7 /℃，玻璃粘度达到102dPa·s的温度T2为1710℃以下，玻璃粘度达到104dPa·s的温度T4为1320℃以下， 以氧化物为基准的摩尔％表示，SiO 2 66〜70，Al 2 O 3 12〜14，B 2 O 3超过0〜1.5，MgO超过9.5〜13（或5〜9.5），CaO 4〜9（或4〜11） ），SrO 0.5〜4.5，BaO 0〜0.5，ZrO 0〜2。
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6.发明申请ALKALI-FREE GLASS SUBSTRATE AND METHOD FOR REDUCING THICKNESS OF ALKALI-FREE GLASS SUBSTRATE 审中-公开无碱玻璃基材和减少无碱玻璃基材厚度的方法公开(公告)号：US20150072130A1
公开(公告)日：2015-03-12
申请号：US14541484
申请日：2014-11-14
摘要： The present invention relates to an alkali-free glass substrate with a thickness of 0.4 mm or less, which has been reduced in thickness by 5 μm or more by a hydrofluoric acid (HF) etching treatment, in which the alkali-free glass substrate contains an alkali-free glass described below, and the alkali-free glass substrate after reduced in thickness has a specific modulus of 32 MNm/kg or more and a photoelastic constant of 31 nm/MPa/cm or less, the alkali-free glass having a strain point of 710° C. or higher, an average thermal expansion coefficient at 50 to 350° C. of from 30×10−7to 43×10−7/° C., a temperature T2 at which a glass viscosity reaches 102 dPa·s of 1710° C. or lower, a temperature T4 at which the glass viscosity reaches 104 dPa·s of 1320° C. or lower.
摘要翻译： 本发明涉及厚度为0.4mm以下的无碱玻璃基板，其通过氢氟酸（HF）蚀刻处理将厚度减小了5μm以上，其中无碱玻璃基板含有 下述的无碱玻璃，厚度减薄后的无碱玻璃基板的比模量为32MNm / kg以上，光弹性常数为31nm / MPa / cm以下，无碱玻璃具有 应变点为710℃以上，50〜350℃的平均热膨胀系数为30×10 -7〜43×10 -7 /℃，玻璃粘度达到102的温度T2 dPa·s为1710℃以下，玻璃粘度达到104dPa·s的温度T4为1320℃以下。
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7.发明申请NON-ALKALI GLASS FOR SUBSTRATES AND PROCESS FOR MANUFACTURING NON-ALKALI GLASS FOR SUBSTRATES 审中-公开用于基板的非碱性玻璃和用于制造用于基板的非碱性玻璃的方法公开(公告)号：US20140038807A1
公开(公告)日：2014-02-06
申请号：US14048382
申请日：2013-10-08
摘要： According to the present invention, an alkali-free glass for a substrate, having a thickness of 0.1 mm to 0.3 mm and a compaction of 9 ppm or lower can be obtained without performing heat treatment as a post-treatment for the alkali-free glass for a substrate after production (after forming, annealing and cutting).
摘要翻译： 根据本发明，作为无碱玻璃的后处理而不进行热处理，可以得到厚度为0.1mm〜0.3mm，压实度为9ppm以下的基材用无碱玻璃 用于生产后（成型，退火和切割）后的基材。
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公开(公告)号：US20130288877A1
公开(公告)日：2013-10-31
申请号：US13928617
申请日：2013-06-27
发明人： Tomoyuki TSUJIMURA , Manabu Nishizawa , Akio Koike
摘要： The present invention relates to an alkali-free glass having a strain point of 735° C. or higher, an average thermal expansion coefficient at from 50 to 350° C. of from 30×10−7 to 40×10−7/° C., a temperature T2 at which a glass viscosity is 102 dPa·s of 1,710° C. or lower, a temperature T4 at which a glass viscosity is 104 dPa·s of 1,340° C. or lower, and a devitrification temperature of 1,330° C. or lower, the alkali-free glass including, in terms of mol % on the basis of oxides: SiO2 66 to 69, Al2O3 12 to 15, B2O3 0 to 1.5, MgO 6 to 9.5, CaO 7 to 9, SrO 0.5 to 3, BaO 0 to 1, and ZrO2 0 to 2, in which MgO+CaO+SrO+BaO is from 16 to 18.2, MgO/(MgO+CaO+SrO+BaO) is 0.35 or more, MgO/(MgO+CaO) is 0.40 or more and less than 0.52, and MgO/(MgO+SrO) is 0.45 or more.
摘要翻译： 本发明涉及应变点为735℃以上，50〜350℃的平均热膨胀系数为30×10 -7〜40×10 -7 /°的无碱玻璃 玻璃粘度为102dPa·s的温度T2为1710℃以下，玻璃粘度为104dPa·s的温度T4为1340℃以下，脱玻温度为 1330℃以下，所述无碱玻璃以氧化物为基准的摩尔％为SiO 2 66〜69，Al 2 O 3为12〜15，B 2 O 0〜1.5，MgO 6〜9.5，CaO 7〜9， SrO 0.5〜3，BaO 0〜1，ZrO 2 0〜2，MgO + CaO + SrO + BaO为16〜18.2，MgO /（MgO + CaO + SrO + BaO）为0.35以上，MgO /（ MgO + CaO）为0.40以上且小于0.52，MgO /（MgO + SrO）为0.45以上。
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9.发明申请METHOD OF MANUFACTURING LITHIUM ION CONDUCTIVE SOLID ELECTROLYTE AND LITHIUM-ION SECONDARY BATTERY 有权锂离子导电固体电解质和锂离子二次电池的制造方法公开(公告)号：US20140170505A1
公开(公告)日：2014-06-19
申请号：US14189094
申请日：2014-02-25
发明人： Tomoyuki TSUJIMURA , Akio KOIKE , Syusaku AKIBA
IPC分类号： H01M10/0562
CPC分类号： H01M10/0562 , C03C3/062 , C03C3/112 , C03C10/00 , C03C10/0027 , C03C10/0045 , C03C10/16 , C03C21/002 , H01M10/052
摘要： A method of manufacturing a lithium ion conductive solid electrolyte includes (a) a step of preparing an object to be processed including a crystalline material, that includes alkali metal other than lithium and whose ionic conductivity at room temperature is greater than or equal to 1×10−13 S/cm; and (b) a step of performing an ion-exchange process on the object to be processed in molten salt including lithium ions.
摘要翻译： 锂离子传导性固体电解质的制造方法包括：（a）包含结晶性物质的被处理物的制造工序，其包含除锂以外的碱金属，室温下的离子导电率为1× 10-13 S / cm; 和（b）在包含锂离子的熔盐中对被处理物进行离子交换处理的工序。
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