公开(公告)号：US07780835B2

公开(公告)日：2010-08-24

申请号：US12427838

申请日：2009-04-22

申请人： John Tony Kinard ,  Brian John Melody ,  David Alexander Wheeler ,  Duane Earl Stenzinger ,  Albert Kennedy Harrington

发明人： John Tony Kinard ,  Brian John Melody ,  David Alexander Wheeler ,  Duane Earl Stenzinger ,  Albert Kennedy Harrington

IPC分类号： C25D11/06

CPC分类号： H01G9/0032 ,  C25D5/18 ,  C25D11/06 ,  C25D11/16 ,  H01G9/045 ,  H01G9/055 ,  Y10S428/935

摘要： A capacitor comprising an aluminum anode and a dielectric layer comprising phosphate doped aluminum oxide and process for making the capacitor. The capacitor has a CV Product of at least 9 μF−V/cm2 at 250 volts. Furthermore, the capacitor is formed by the process of: forming an aluminum plate; contacting the plate with an anodizing solution comprising glycerine, 0.1 to 1.0%, by weight, water and 0.01 to 0.5%, by weight, orthophosphate; applying a voltage to the aluminum plate and determining an initial current; maintaining the first voltage until a first measured current is no more than 50% of the initial current; increasing the voltage and redetermining the initial current; maintaining the increased voltage until a second measured current is no more than 50% of the redetermined initial current, and continuing the increasing of the voltage and maintaining the increased voltage until a final voltage is achieved.

摘要翻译： 包括铝阳极和包含磷酸盐掺杂的氧化铝的介电层的电容器和用于制造电容器的工艺。 该电容器具有在250伏特下至少9μF-V / cm 2的CV产品。 此外，电容器通过以下工序形成：形成铝板; 使板与阳极氧化溶液接触，所述阳极氧化溶液包含0.1-1.0％（重量）的水和0.01至0.5％重量的正磷酸的甘油; 向铝板施加电压并确定初始电流; 保持第一电压，直到第一测量电流不超过初始电流的50％; 增加电压并重新确定初始电流; 维持增加的电压，直到第二测量电流不超过重新确定的初始电流的50％，并且继续增加电压并保持升高的电压直到达到最终电压。

公开(公告)号：US20090205970A1

公开(公告)日：2009-08-20

申请号：US12427838

申请日：2009-04-22

申请人： John Tony Kinard ,  Brian John Melody ,  David Alexander Wheeler ,  Duane Earl Stenzinger ,  Albert Kennedy Harrington

发明人： John Tony Kinard ,  Brian John Melody ,  David Alexander Wheeler ,  Duane Earl Stenzinger ,  Albert Kennedy Harrington

IPC分类号： C25D11/10

CPC分类号： H01G9/0032 ,  C25D5/18 ,  C25D11/06 ,  C25D11/16 ,  H01G9/045 ,  H01G9/055 ,  Y10S428/935

摘要： A capacitor comprising an aluminum anode and a dielectric layer comprising phosphate doped aluminum oxide and process for making the capacitor. The capacitor has a CV Product of at least 9 μF−V/cm2 at 250 volts. Furthermore, the capacitor is formed by the process of: forming an aluminum plate; contacting the plate with an anodizing solution comprising glycerine, 0.1 to 1.0%, by weight, water and 0.01 to 0.5%, by weight, orthophosphate; applying a voltage to the aluminum plate and determining an initial current; maintaining the first voltage until a first measured current is no more than 50% of the initial current; increasing the voltage and redetermining the initial current; maintaining the increased voltage until a second measured current is no more than 50% of the redetermined initial current, and continuing the increasing of the voltage and maintaining the increased voltage until a final voltage is achieved.

摘要翻译： 包括铝阳极和包含磷酸盐掺杂的氧化铝的介电层的电容器和用于制造电容器的工艺。 该电容器具有在250伏特下至少9μF-V / cm 2的CV产品。 此外，电容器通过以下工序形成：形成铝板; 使板与阳极氧化溶液接触，所述阳极氧化溶液包含0.1-1.0％（重量）的水和0.01至0.5％重量的正磷酸的甘油; 向铝板施加电压并确定初始电流; 保持第一电压，直到第一测量电流不超过初始电流的50％; 增加电压并重新确定初始电流; 维持增加的电压，直到第二测量电流不超过重新确定的初始电流的50％，并且继续增加电压并保持升高的电压直到达到最终电压。

公开(公告)号：US07342773B2

公开(公告)日：2008-03-11

申请号：US11352050

申请日：2006-02-10

申请人： Albert Kennedy Harrington ,  John Tony Kinard ,  Brian John Melody ,  David Alexander Wheeler ,  Duane Earl Stenzinger

发明人： Albert Kennedy Harrington ,  John Tony Kinard ,  Brian John Melody ,  David Alexander Wheeler ,  Duane Earl Stenzinger

IPC分类号： H01G9/02

CPC分类号： H01G9/0032 ,  C25D5/18 ,  C25D11/06 ,  C25D11/16 ,  H01G9/045 ,  H01G9/055 ,  Y10S428/935

摘要： A capacitor comprising an aluminum anode and a dielectric layer comprising phosphate doped aluminum oxide and process for making the capacitor. Furthermore, the capacitor is formed by the process of: forming an aluminum plate; pre-hydrating the aluminum; contacting the plate with an anodizing solution comprising glycerine, 0.1 to 1.0%, by weight, water and 0.01 to 0.5%, by weight, orthophosphate; applying a voltage to the aluminum plate and determining an initial current; maintaining the first voltage until a first measured current is no more than 50% of the initial current; increasing the voltage and redetermining the initial current; maintaining the increased voltage until a second measured current is no more than 50% of the redetermined initial current, and continuing the increasing of the voltage and maintaining the increased voltage until a final voltage is achieved.

摘要翻译： 包括铝阳极和包含磷酸盐掺杂的氧化铝的介电层的电容器和用于制造电容器的工艺。 此外，电容器通过以下工序形成：形成铝板; 预水化铝; 使板与阳极氧化溶液接触，所述阳极氧化溶液包含0.1-1.0％（重量）的水和0.01至0.5％重量的正磷酸的甘油; 向铝板施加电压并确定初始电流; 保持第一电压，直到第一测量电流不超过初始电流的50％; 增加电压并重新确定初始电流; 维持增加的电压，直到第二测量电流不超过重新确定的初始电流的50％，并且继续增加电压并保持升高的电压直到达到最终电压。

公开(公告)号：US06591515B2

公开(公告)日：2003-07-15

申请号：US09948716

申请日：2001-09-10

申请人： John Tony Kinard ,  Michael John Maich ,  Brian John Melody ,  Duane Earl Stenzinger ,  David Alexander Wheeler ,  Keith Lee Moore

发明人： John Tony Kinard ,  Michael John Maich ,  Brian John Melody ,  Duane Earl Stenzinger ,  David Alexander Wheeler ,  Keith Lee Moore

IPC分类号： F26B1330

CPC分类号： F26B5/04 ,  F26B11/02

摘要： An apparatus is disclosed for drying materials wet with one or more solvents, particularly hygroscopic materials and materials wet with a high boiling point (low vapor pressure) solvent that are sensitive to heat. Wet material is loaded into a chamber, which is then sealed and caused to oscillate back and forth. Vacuum is enlisted to provide rapid evaporation of solvent at a lower temperature than possible at standard atmospheric pressure. The material is oscillated until a sudden decrease in the residual pressure of the chamber, which indicates completion of the drying cycle. Because vacuum is applied to an oscillating chamber, a rotary vacuum seal is not required to accomplish drying in accordance with the practice of the instant invention.

摘要翻译： 公开了一种用一种或多种溶剂干燥材料的装置，特别是吸湿材料和用热沸点敏感的高沸点（低蒸气压）溶剂湿润的材料。 将湿料装入室中，然后将其密封并使其振荡。 吸入真空以在标准大气压下在比较低的温度下提供溶剂的快速蒸发。 材料振荡直到室的残余压力突然下降，这表明干燥循环的完成。 由于真空被施加到振荡室，所以根据本发明的实践，不需要旋转真空密封来完成干燥。

公开(公告)号：US07090762B2

公开(公告)日：2006-08-15

申请号：US10634423

申请日：2003-08-05

申请人： Terrance B. Tripp ,  Brian John Melody ,  John Tony Kinard ,  David Alexander Wheeler ,  Duane Earl Stenzinger

发明人： Terrance B. Tripp ,  Brian John Melody ,  John Tony Kinard ,  David Alexander Wheeler ,  Duane Earl Stenzinger

IPC分类号： C25D11/02 ,  C25D9/02

CPC分类号： C25D9/02 ,  C25D5/54 ,  C25D11/26 ,  H01G9/028 ,  H01G9/042

摘要： The metal oxide surface coating of an anodized valve metal may be made conductive under certain conditions so that conductive coatings can be electrolytically deposited on the surface of the oxide. When a dry polar aprotic electrolyte solution is used at a reduced temperature and a relatively high field is applied, the oxide ceases to be insulative. The process is reversible, meaning that there is no permanent change in the oxide.

摘要翻译： 阳极氧化阀金属的金属氧化物表面涂层可以在某些条件下导电，使得导电涂层可以电解沉积在氧化物的表面上。 当干燥的极性非质子电解质溶液在降低的温度下使用并且施加相对较高的场时，氧化物不再是绝缘的。 该过程是可逆的，意味着氧化物没有永久的变化。

公开(公告)号：US06485676B1

公开(公告)日：2002-11-26

申请号：US09659555

申请日：2000-09-11

申请人： David Alexander Wheeler ,  Brian J. Melody ,  John Tony Kinard ,  Keith Lee Moore ,  Duane Earl Stenzinger

发明人： David Alexander Wheeler ,  Brian J. Melody ,  John Tony Kinard ,  Keith Lee Moore ,  Duane Earl Stenzinger

IPC分类号： B22F312

CPC分类号： C04B35/638 ,  B22F1/0059 ,  B22F3/1025 ,  B22F2999/00 ,  C04B35/58007 ,  C04B35/632 ,  C04B2235/6581 ,  C04B2235/721 ,  C04B2235/723 ,  B22F2201/02 ,  B22F2201/10

摘要： A method of thermally removing binder from porous compacts pressed from metallic or ceramic materials using atmospheric pressure and binder-free compacts produced therefrom.

摘要翻译： 使用大气压从金属或陶瓷材料压制的多孔压块和由其制成的无粘结剂压块热粘合剂的方法。