公开(公告)号：US4329327A

公开(公告)日：1982-05-11

申请号：US210480

申请日：1980-11-26

Applicant: James E. Neely, Jr. ,  Annette Moff ,  Chia-Cheng Lin ,  Charlene A. Falleroni

Inventor： James E. Neely, Jr. ,  Annette Moff ,  Chia-Cheng Lin ,  Charlene A. Falleroni

IPC: C01B25/44 ,  C01B25/36

CPC classification number: C01B25/44

Abstract: A method for preparing aluminum trimetaphosphate predominately in the B-form by heating a mixture of aluminum hydroxide and ammonium phosphate compound is disclosed.

Abstract translation: 公开了通过加热氢氧化铝和磷酸铵化合物的混合物来主要制备B-形式的三偏磷酸铝的方法。

公开(公告)号：US4824712A

公开(公告)日：1989-04-25

申请号：US785431

申请日：1985-10-08

Applicant: Charlene A. Falleroni ,  Chia-Cheng Lin

Inventor： Charlene A. Falleroni ,  Chia-Cheng Lin

IPC: C03B8/02 ,  C03B27/012 ,  C03C17/02 ,  C03B23/02 ,  C03B23/26

CPC classification number: C03B27/012 ,  C03C17/02 ,  Y02P40/57 ,  Y10T428/24322 ,  Y10T428/24347 ,  Y10T428/31 ,  Y10T428/315

Abstract: A method and composition for coating scored regions or holes in glass articles prior to heat treatment in order to maintain residual compressive stresses and reduce venting are disclosed. The method and composition of the present invention utilize silica-containing sols which gel and density and ultimately form glassy films during the heat treatment of the coated glass articles.

Abstract translation: 公开了一种用于在热处理之前涂覆玻璃制品中的刻痕区域或孔的方法和组合物，以便保持残余的压缩应力并减少排气。 本发明的方法和组合物在涂覆的玻璃制品的热处理中使用凝胶密度最终形成玻璃膜的含硅胶体。

公开(公告)号：US4731264A

公开(公告)日：1988-03-15

申请号：US915344

申请日：1986-10-03

Applicant: Chia-Cheng Lin ,  Charlene A. Falleroni

Inventor： Chia-Cheng Lin ,  Charlene A. Falleroni

IPC: C09D183/04 ,  C09D183/14 ,  B05D3/02 ,  C08G77/06

CPC classification number: C09D183/14 ,  C09D183/04

Abstract: An organoalkoxysilane/alumina sol-gel composition and method for its production are disclosed whereby an aluminum alkoxide is hydrolyzed in water to form a sol, to which is added a hydrolyzable organoalkoxysilane of the general formulaR.sub.x Si(OR').sub.4-xwherein R is an organic radical, R' is a low molecular weight alkyl radical, and x is at least 1 and less than 4. The composition is dried and cured to form an organosiloxane/alumina monolith or coating on a substrate.

Abstract translation: 公开了一种有机烷氧基硅烷/氧化铝溶胶 - 凝胶组合物及其制备方法，其中在水中水解铝醇盐以形成溶胶，向其中加入通式为RxSi（OR'）4-x的可水解的有机烷氧基硅烷，其中R为 有机基团R'是低分子量烷基，x至少为1且小于4.将组合物干燥并固化以在基材上形成有机硅氧烷/氧化铝整料或涂层。

公开(公告)号：US4333914A

公开(公告)日：1982-06-08

申请号：US210509

申请日：1980-11-26

Applicant: James E. Neely, Jr. ,  Chia-Cheng Lin ,  Charlene A. Falleroni ,  Annette Moff

Inventor： James E. Neely, Jr. ,  Chia-Cheng Lin ,  Charlene A. Falleroni ,  Annette Moff

IPC: C01B25/44 ,  C01B25/36

CPC classification number: C01B25/44

Abstract: A method for preparing aluminum trimetaphosphate comprising various chain form polyphosphate species by heating a mixture of aluminum hydroxide and ammonium phosphate is disclosed.

Abstract translation: 公开了一种通过加热氢氧化铝和磷酸铵的混合物制备三聚磷酸铝的方法，其包括各种链形聚磷酸酯物质。

公开(公告)号：US4312844A

公开(公告)日：1982-01-26

申请号：US210508

申请日：1980-11-26

Applicant: James E. Neely, Jr. ,  Charlene A. Falleroni ,  Annette Moff ,  Chia-Cheng Lin

Inventor： James E. Neely, Jr. ,  Charlene A. Falleroni ,  Annette Moff ,  Chia-Cheng Lin

IPC: C01B25/44

CPC classification number: C01B25/44

Abstract: A method for preparing a trimetaphosphate of a trivalent species by heating a mixture of ammonium phosphate and an oxygen-containing compound of the trivalent species is disclosed.

Abstract translation: 公开了通过加热磷酸铵和三价物质的含氧化合物的混合物来制备三价三价三磷酸的方法。

公开(公告)号：US6094942A

公开(公告)日：2000-08-01

申请号：US874529

申请日：1997-06-13

Applicant: Charlene A. Falleroni ,  Donald L. DeSantis ,  Kevin G. Hill

Inventor： Charlene A. Falleroni ,  Donald L. DeSantis ,  Kevin G. Hill

IPC: C03B18/18 ,  C03B18/20 ,  C03B13/00 ,  C03B5/16 ,  C03B15/00 ,  C03B17/00

CPC classification number: C03B18/18 ,  Y02P40/57

Abstract: The present invention provides a method of reducing tin defects in flat glass made by the float process. In the float process, molten glass is delivered onto a pool of molten tin within an enclosed chamber and formed into a glass ribbon. Oxygen gas dissolved in the molten tin combines with the tin to form tin oxide which vaporizes and collects within the chamber, resulting in defects in the glass. In the present invention, hydrogen gas is introduced directly into the molten tin to react with the oxygen gas and tin oxide within the molten tin to form water and elemental tin, resulting in a reduction in the amount of tin oxide within the molten tin. In one particular embodiment of the invention, the hydrogen gas is introduced into the molten tin through an elongated, porous graphite member submerged in the molten tin within the forming chamber such that it extends along and is located outboard of selected portions of the edge of the glass ribbon.

Abstract translation: 本发明提供一种减少由浮法制成的平板玻璃中的锡缺陷的方法。 在浮法工艺中，将熔融玻璃输送到封闭室内的熔融锡池中并形成玻璃带。 溶解在熔融锡中的氧气与锡组合形成氧化锡，其在室内蒸发并收集，导致玻璃中的缺陷。 在本发明中，将氢气直接引入熔融锡中，与熔融锡内的氧气和氧化锡反应形成水和元素锡，导致锡内氧化锡的量减少。 在本发明的一个具体实施方案中，氢气通过浸没在成形室内的熔融锡中的细长的多孔石墨构件引入熔融锡中，使得其沿着并位于外部的边缘的选定部分外侧延伸 玻璃丝带。