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    Quaternized condensation products of trialkanolamines
    3.
    发明授权
    Quaternized condensation products of trialkanolamines 失效
    三烷醇胺的季铵化缩合产物

    公开(公告)号：US5015754A

    公开(公告)日：1991-05-14

    申请号：US396128

    申请日：1989-08-21

    申请人： Johannes P. Dix ,  Rolf Fikentscher ,  Ingrid Steenken-Richter

    发明人： Johannes P. Dix ,  Rolf Fikentscher ,  Ingrid Steenken-Richter

    IPC分类号： C08G18/48 ,  C08G18/83 ,  C08G59/14 ,  C08G63/685 ,  C08G64/12 ,  C08G65/28 ,  C08G65/32 ,  C08G69/48 ,  C08G71/00 ,  D06P1/52 ,  D06P3/52 ,  D06P3/66 ,  D06P5/08

    CPC分类号： D06P1/52 ,  C08G63/685 ,  C08G64/12 ,  C08G71/00 ,  D06P3/52 ,  D06P3/66 ,  D06P5/08

    摘要： Quaternized condensation products useful as aftertreating agents for fixing reactive dyeings and prints on textile materials which contain cellulose fibers are formed fromA) a precondensate of one or more trialkanolamines I ##STR1## (R.sup.1 -R.sup.3 =C.sub.2 -C.sub.4 -1,2-alkylene), B) a) a carboxylic acid or a derivative thereof IIa ##STR2## [n=0, 1; R.sup.4, R.sup.5 =OH (except if n=0), C.sub.1 -C.sub.8 -alkoxy (possibly joined together to form a 5- or 6-membered ring if n=0), Cl, Br; R.sup.6 =C.sub.1 -C.sub.50 -alkylene (possibly interrupted by one or more nonadjacent oxygen atoms)],b) a carboxamide IIb ##STR3## [m, n, r=0, 1; R.sup.7 =H, C.sub.1 -C.sub.4 -alkyl; R.sup.8 =H, C.sub.1 -C.sub.25 -alkyl, C.sub.2 -C.sub.25 -alkenyl, Ph (possibly substituted by C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, F, Cl, Br)],c) an epihalohydrin IIc, ##STR4## d) a monofunctional compound IIdR.sup.9 --Y IId [R.sup.9 =C.sub.1 -C.sub.25 -alkyl, C.sub.2 -C.sub.25 -alkenyl, Ph (possibly substituted by C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, F, Cl, Br); Y=isocyanate, OCONHR.sup.8, glycidyloxy],e) a bifunctional compound IIeZ.sup.1 --R.sup.10 --Z.sup.2 IIe [R.sup.10 =C.sub.a -C.sub.50 -alkylene (possibly interrupted by one or more nonadjacent oxygen atoms, possibly containing one or more mutually nonvicinal hydroxyl groups); Z.sup.1, Z.sup.2 =Cl, Br, isocyanate, NH--COOR.sup.9, glycidyloxy, OR.sup.9 ], andC) a benzyl halide III ##STR5## (p=0-2; R.sup.11 =C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, F, Cl, Br).

    摘要翻译： 季铵化缩合产物可用作用于固定活性染料和印刷品的纤维素纤维的纺织材料上的后处理剂，由A）一种或多种三烷醇胺的预缩合物形成I（R1-R3 = C2-C4-1,2- 亚烷基），B）a）羧酸或其衍生物IIa IIa [n = 0,1; R4，R5 = OH（n = 0时除外），C1-C8-烷氧基（如果n = 0，则可能连接在一起形成5-或6-元环），Cl，Br; R 6 = C 1 -C 50 - 亚烷基（可能被一个或多个不相邻的氧原子中断）]，b）甲酰胺IIb [m，n，r = 0,1; R7 = H，C1-C4-烷基; R 8 = H，C 1 -C 25 - 烷基，C 2 -C 25 - 烯基，Ph（可被C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，F，Cl，Br取代）]，c）表卤代醇IIc， IIc d）单官能化合物IId R9-YIId [R 9 = C 1 -C 25 - 烷基，C 2 -C 25 - 烯基，Ph（可能被C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，F，Cl，Br）取代; Y =异氰酸酯，OCONHR8，缩水甘油氧基]，e）双官能化合物IIe Z1-R10-Z2IIe [R10 = Ca-C50-亚烷基（可能被一个或多个不相邻的氧原子间隔，可能含有一个或多个相互非羟基的羟基） Z1，Z2 = Cl，Br，异氰酸酯，NH-COOR9，缩水甘油氧基，OR9]和C）苄基卤III III（p = 0-2; R11 = C1-C4-烷基，C1-C4-烷氧基 ，F，Cl，Br）。

    Preparation of condensates of arenesulfonic acids and formaldehyde and use thereof
    4.
    发明授权
    Preparation of condensates of arenesulfonic acids and formaldehyde and use thereof 失效
    芳烃磺酸和甲醛的缩合物的制备及其用途

    公开(公告)号：US5534166A

    公开(公告)日：1996-07-09

    申请号：US37392

    申请日：1993-03-26

    申请人： Ralf Brueckmann ,  Johannes P. Dix ,  Rolf Fikentscher ,  Manfred Herrmann ,  Norbert Zimmermann

    发明人： Ralf Brueckmann ,  Johannes P. Dix ,  Rolf Fikentscher ,  Manfred Herrmann ,  Norbert Zimmermann

    IPC分类号： C09B67/42 ,  B01F17/52 ,  C07G99/00 ,  C08G16/00 ,  C08G16/02

    CPC分类号： C07G17/002 ,  C08G16/0237

    摘要： Condensates of arenesulfonic acids and formaldehyde are prepared by sulfonating arenes obtainable by thermal cracking of a naphthenic residue oil and fractional distillation of the cracked products of the fraction obtained at 100-120.degree. C. under atmospheric pressure, sulfonating this aromatics fraction with oleum at 120.degree.-160.degree. C. using an amount of from 0.7 to 1.2 parts by weight of oleum having an SO.sub.3 content of 24% by weight per part by weight of aromatics fraction, and subsequently condensing the arenesulfonic acids with formaldehyde in a conventional manner, and are used as dispersants, in particular for preparing dye formulations.

    摘要翻译： 芳族磺酸和甲醛的冷凝物是通过磺化芳烃来制备的，该芳烃可通过环烷烃残余油的热裂解得到，并在100-120℃下在大气压下分馏得到的馏分的裂化产物，用发烟硫酸将该芳烃馏分磺化120 DEG -160℃，使用0.7至1.2重量份的SO 3含量为每重量份芳烃馏分24重量％的发烟硫酸，然后以常规方式将芳族磺酸与甲醛缩合，以及 用作分散剂，特别是用于制备染料配方。

    Methods of demulsifying employing condensates as demulsifiers for oil-in water emulsions
    6.
    发明授权
    Methods of demulsifying employing condensates as demulsifiers for oil-in water emulsions 失效
    使用冷凝剂作为水分乳化剂的分解剂的方法

    公开(公告)号：US5234626A

    公开(公告)日：1993-08-10

    申请号：US827170

    申请日：1991-02-11

    申请人： Rolf Fikentscher ,  Knut Oppenlaender ,  Johannes P. Dix ,  Wilfried Sager ,  Hans-Henning Vogel ,  Guenther Elfers

    发明人： Rolf Fikentscher ,  Knut Oppenlaender ,  Johannes P. Dix ,  Wilfried Sager ,  Hans-Henning Vogel ,  Guenther Elfers

    IPC分类号： B01D17/05 ,  B01F17/00 ,  C08G65/48 ,  C08G71/00

    CPC分类号： C08G71/00 ,  B01F17/005

    摘要： The present invention relates to methods of demulsifying employing condensates as demulsifiers for oil-in-water emulsions and prepared fromA) a precondensate from one or more trialkanolamines of the general formula I ##STR1## in which R.sup.1 to R.sup.3 denote the same or different 1,2-alkylene groups of from 2 to 4 carbon atoms, andB) from 0.1 to 30% w/w, based on said precondensate, of one or more of the following compounds II:a) urea or a urea derivative of the general formula IIa ##STR2## b) a urea derivative of the general formula IIb ##STR3## c) a urethane of the general formula IIc ##STR4## and/or d) a urethane of the general formula IId ##STR5## in which R.sup.1 is hydrogen, C.sub.1 -C.sub.20 -alkyl or C.sub.2 -C.sub.20 -alkenyl,R.sup.2 and R.sup.3 are the same or different and denote hydrogen or C.sub.1 -C.sub.4 -alkyl,R.sup.4 is C.sub.1 -C.sub.4 -alkyl andR.sup.5 is C.sub.1 -C.sub.12 -alkylene.

    摘要翻译： 本发明涉及使用缩合物作为水包油乳液的破乳剂进行破乳的方法，由A）来自一种或多种通式Ⅰ（I）的三链烷醇胺的预缩合物制备，其中R 1至R 3表示相同的 或不同的2至4个碳原子的1,2-亚烷基，以及B）0.1至30％w / w（基于所述预缩合物）一种或多种下列化合物II：a）脲或脲衍生物 通式IIa（IIa）的脲衍生物b）通式IIb的脲衍生物（IIb）c）通式IIc（IIc）的氨基甲酸酯和/或d）氨基甲酸酯 其中R 1是氢，C 1 -C 20 - 烷基或C 2 -C 20 - 链烯基，R 2和R 3相同或不同，表示氢或C 1 -C 4烷基，R 4是C 1 -C 4烷基， C4-烷基，R5是C1-C12-亚烷基。

    Preparation of concentrated solutions of cationic dyes as mono-carboxylates in glycol ether
    10.
    发明授权
    Preparation of concentrated solutions of cationic dyes as mono-carboxylates in glycol ether 失效
    在乙二醇醚中制备阳离子染料作为单羧酸盐的浓缩溶液

    公开(公告)号：US4976744A

    公开(公告)日：1990-12-11

    申请号：US406244

    申请日：1989-09-12

    申请人： Johannes P. Dix ,  Guenter Hansen ,  Hellmut Kast

    发明人： Johannes P. Dix ,  Guenter Hansen ,  Hellmut Kast

    IPC分类号： C09B67/32

    CPC分类号： C09B67/0075 ,  Y10S8/927

    摘要： Concentrated solutions of cationic dyes are prepared by treating the cationic dyes, which contain as the counterions the anions customarily present during their preparation, with alkali metal salts of monocarboxylic acids and with or without complexing agents in an aqueous glycol ether medium, and separating off the organic phase, which contains the dyes in the form of their monocarboxylic acid salts.

    摘要翻译： 阳离子染料的浓缩溶液通过在阳离子染料中处理阳离子染料，所述阳离子染料在其制备过程中通常含有阴离子与阴离子一起含有一元羧酸的碱金属盐，并且在含水二醇醚介质中含有或不与络合剂反应， 有机相，其含有其一元羧酸盐形式的染料。