公开(公告)号：US20230183407A1

公开(公告)日：2023-06-15

申请号：US17938110

申请日：2022-10-05

Applicant: Dalian University of Technology

Inventor： Shufen ZHANG ,  Changtong ZHOU ,  Wenbin NIU ,  Wei MA ,  Bingtao TANG ,  Suli WU

IPC: C08F222/10

CPC classification number: C08F222/1063

Abstract: A double-inverse opal photonic crystal resin film is formed by embedding nanospheres in pores of polyacrylate inverse opal framework material and then filling the pores of the double-inverse opal photonic crystal resin film with an ethanol solution with hydrophilic acrylamide dissolved therein followed by photopolymerization to form a polyacrylamide network, so as to obtain the double-inverse opal photonic crystal resin film using water as ink. A mass fraction of hydrophilic acrylamide in the ethanol solution is 2 to 8 wt.%. The resin film can induce water to penetrate into the pores of the double-inverse opal photonic crystal resin film, making the nanospheres in the pores of the inverse opal framework distribute from random to order under the action of buoyancy force, thereby eliminating scattering interference and producing brilliant structural colors by regulating refractive index contrast.

公开(公告)号：US20240191080A1

公开(公告)日：2024-06-13

申请号：US18546986

申请日：2021-09-02

Applicant: DALIAN UNIVERSITY OF TECHNOLOGY

Inventor： Shufen ZHANG ,  Lei LI ,  Bingtao TANG ,  Rongwen LV ,  Wei MA ,  Suli WU ,  Wenbin NIU ,  Benzhi JU

IPC: C09B29/00 ,  B01J19/00 ,  B01J19/18

CPC classification number: C09B29/00 ,  B01J19/0066 ,  B01J19/1812 ,  B01J2219/00195

Abstract: A method for producing water-soluble azo dyes by utilizes continuous diazotization reaction and continuous coupling reaction in a pipeline reactor. The diazo component, hydrochloric acid and sodium nitrite are simultaneously fed at the bottom of the pipeline reactor at room temperature, to perform a diazotization reaction in the pipeline and leave the diazotization reaction site in time, followed by performing the coupling reaction with the introduced coupled component. Under stirring of micro stirring blades, the materials at each flow layer are uniformly mixed and reacted, and the reaction materials flow upward under the action of a feed driving force and are discharged from the top of the continuous reactor to produce a water-soluble azo dye.

公开(公告)号：US20230003993A1

公开(公告)日：2023-01-05

申请号：US17756714

申请日：2020-09-08

Applicant: DALIAN UNIVERSITY OF TECHNOLOGY

Inventor： Shufen ZHANG ,  Yong QI ,  Wenbin NIU ,  Suli WU ,  Wei MA ,  Bingtao TANG

IPC: G02B26/00 ,  C08F222/10 ,  C08J5/18 ,  G02B1/00

Abstract: A bilayer photonic crystal photoswitch thin-film device having the optical characteristics of both 2D and 3D photonic crystals, and a preparation method thereof are provided. When the bilayer photonic crystal photoswitch thin-film device is rotated periodically, different colors can be observed at a fixed rotation angle, that is, the device has the attribute of changing colors by means of rotation, and can thus realize the opening and closing of an optical path. The bilayer photonic crystal photoswitch thin-film new device has broad application prospects in the fields of photoswitches, optical waveguides, optical prisms, warming signs, anti-counterfeiting and information coding, etc.