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1.发明授权Glass fiber strand mats, thermosetting composites reinforced with the same and methods for making the same 失效玻璃纤维丝网，热固性复合材料与其相同的加固方法和制造方法
公开(公告)号：US5908689A
公开(公告)日：1999-06-01
申请号：US787735
申请日：1997-01-24
CPC分类号： B32B5/28 , B29C70/081 , D04H1/498 , D04H3/004 , D04H3/105 , D04H5/02 , D04H5/12 , Y10T442/604 , Y10T442/667 , Y10T442/67 , Y10T442/682
摘要： The present invention provides a mat adapted to reinforce a thermosetting matrix material to form a composite, composites formed therefrom, and methods related thereto. The mat includes a primary, supporting layer having a plurality of randomly oriented essentially continuous glass fiber strands. The primary layer has about 1 to about 10 weight percent of the mat on a total solids basis. The mat also includes a secondary layer positioned upon and supported by a surface of the primary layer, the secondary layer including a plurality of glass fiber strands. The mean average length of the glass fiber strands of the secondary layer ranges from about 20 to about 125 millimeters. The strands of the primary layer are entangled with the strands of the secondary layer by needling the primary layer and the secondary layer together.
摘要翻译： 本发明提供了一种适于加强热固性基质材料以形成复合材料，由其形成的复合材料的垫及其相关方法。 垫包括具有多个随机取向的基本上连续的玻璃纤维束的主要支撑层。 主层在总固体的基础上具有约1至约10重量％的垫。 垫还包括位于主层的表面上并由其支撑的第二层，第二层包括多个玻璃纤维束。 次级层的玻璃纤维束的平均长度范围为约20至约125毫米。 主层的股线通过将主层和次级层一起进行针刺而与次级层的股线缠结。
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2.发明授权
公开(公告)号：US4808478A
公开(公告)日：1989-02-28
申请号：US904728
申请日：1986-09-05
CPC分类号： C08J5/08 , C03C25/26 , C08K9/08 , Y10T428/2933 , Y10T428/2938 , Y10T428/2962 , Y10T428/2964
摘要： Chemically treated glass fiber reinforcement for thermosetting polymers having a moisture reduced residue of an aqueous chemical treating composition consisting essentially of a vinyl acetate-organosilane copolymer, a vinyl silane coupling agent, an amino-organo silane coupling agent, at least one cationic lubricant, polyoxyethylene, an antistatic agent, an aqueous dispersible or emulsifiable wax with a surfactant and water.
摘要翻译： 用于热塑性聚合物的化学处理玻璃纤维增强剂，其具有基本上由乙酸乙烯酯 - 有机硅烷共聚物，乙烯基硅烷偶联剂，氨基有机硅烷偶联剂，至少一种阳离子润滑剂，聚氧乙烯 抗静电剂，具有表面活性剂和水的水分散性或可乳化蜡。
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公开(公告)号：US4927869A
公开(公告)日：1990-05-22
申请号：US245099
申请日：1988-09-15
申请人： David E. Dana , Steven J. Morris
发明人： David E. Dana , Steven J. Morris
摘要： Chemically treated glass fibers of the present invention provide good processing properties in reinforcing thermosetting polymers while resulting in fiber reinforced thermosetting materials having good strength properties. The chemically treated glass fibers have a dried residue of an aqueous chemical treating composition having: two film forming polymers, at least an acryloxy alkyl trialkoxysilane, a fiber lubricant and polyester curing agent and water. One film forming polymer is a polyvinylacetate copolymer having a low solubility in acetone and the other film forming polymer is unsaturated, curable, essentially linear polyester polymer. The fiber lubricant is a nonionic polyethylene-containing polymer or a cationic lubricant like polyalkylene polyamine polyamino amide, and partially amidated polyalkylenimines and mixtures thereof present in an effective lubricating amount. The nonionic lubricant may be used and the cationic lubricant is used in conjunction with a fuzz reducing agent such as silylated polyazamide. Additional components which may be present include: an amino organofunctional silane coupling agent, and a polyoxyethylene polymer having a molecular weight in the range of 100,000 to 5 million. The dried residue is present on the fibers in the strand in an amount in the range of around 1.5 to 3 percent LOI. Also, the dried strands have a post treatment with an antistatic agent before the strands are utilized as reinforcement for thermosetting materials.
摘要翻译： 本发明的化学处理玻璃纤维在增强热固性聚合物中提供良好的加工性能，同时产生具有良好强度性能的纤维增强热固性材料。 化学处理的玻璃纤维具有水性化学处理组合物的干燥残余物，其具有两种成膜聚合物，至少丙烯酰氧基烷基三烷氧基硅烷，纤维润滑剂和聚酯固化剂和水。 一种成膜聚合物是在丙酮中溶解度低的聚乙酸乙烯酯共聚物，另一种成膜聚合物是不饱和的，可固化的，基本上为线性的聚酯聚合物。 纤维润滑剂是含有非离子聚乙烯的聚合物或阳离子润滑剂，如聚亚烷基多胺聚氨基酰胺，部分酰胺化的聚亚烷基亚胺及其混合物以有效的润滑量存在。 可以使用非离子润滑剂，并且阳离子润滑剂与绒毛还原剂如甲硅烷基化的叠氮烷一起使用。 可能存在的其它组分包括：氨基有机官能硅烷偶联剂和分子量在100,000至500万范围内的聚氧乙烯聚合物。 干燥的残余物在链中的纤维上以约1.5-3％LOI的量存在。 此外，干燥的股线在用作热固性材料的增强剂之前，使用抗静电剂进行后处理。
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