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公开(公告)号:US08323569B2
公开(公告)日:2012-12-04
申请号:US13160883
申请日:2011-06-15
申请人: David T. Gillespie , Colin Lipishan , Lonnie G. Hazlitt , Alexander W. Degroot , Peter B. Arnoudse , Charles A. Williams
发明人: David T. Gillespie , Colin Lipishan , Lonnie G. Hazlitt , Alexander W. Degroot , Peter B. Arnoudse , Charles A. Williams
CPC分类号: G01N30/468 , G01N25/147 , G01N30/463 , G01N30/54 , G01N33/442 , G01N2030/008 , G01N2030/3007
摘要: Apparatus for GPC/TREF and TREF/GPC characterization of a polymer sample. The apparatus provides for the automated and integrated use of multiple TREF columns and a GPC system employing a multiple flow through detectors. In addition, a method for TREF/GPC characterization of a polymer sample by GPC analysis of TREF fractions at increasing TREF elution temperatures from multiple TREF columns operated in a coordinated and synchronized temperature cycle for increased sample throughput. Also, a method for GPC/TREF characterization of a polymer sample by GPC fractionation followed by TREF fractionation of the GPC fractionations.
摘要翻译: 用于GPC / TREF和TREF / GPC表征聚合物样品的装置。 该装置提供了多个TREF柱的自动化和集成使用以及采用多个流过检测器的GPC系统。 此外,通过在增加TREF洗脱温度的TREF洗脱温度下,通过GPC分析TREF级分,通过在协同和同步的温度循环中操作以提高样品通量的多个TREF柱来对聚合物样品进行TREF / GPC表征的方法。 此外,通过GPC分级随后进行GPC分馏的TREF分馏,GPC / TREF表征聚合物样品的方法。
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公开(公告)号:US07985593B2
公开(公告)日:2011-07-26
申请号:US11794417
申请日:2006-01-19
申请人: David T. Gillespie , Colin Li Pi Shan , Lonnie G. Hazlitt , Alexander W. DeGroot , Peter B. Arnoudse , Charles Allen Williams
发明人: David T. Gillespie , Colin Li Pi Shan , Lonnie G. Hazlitt , Alexander W. DeGroot , Peter B. Arnoudse , Charles Allen Williams
CPC分类号: G01N30/468 , G01N25/147 , G01N30/463 , G01N30/54 , G01N33/442 , G01N2030/008 , G01N2030/3007
摘要: Apparatus for GPC/TREF and TREF/GPC characterization of a polymer sample. The apparatus provides for the automated and integrated use of multiple TREF columns and a GPC system employing a multiple flow through detectors. In addition, a method for TREF/GPC characterization of a polymer sample by GPC analysis of TREF fractions at increasing TREF elution temperatures from multiple TREF columns operated in a coordinated and synchronized temperature cycle for increased sample throughput. Also, a method for GPC/TREF characterization of a polymer sample by GPC fractionation followed by TREF fractionation of the GPC fractionations.
摘要翻译: 用于GPC / TREF和TREF / GPC表征聚合物样品的装置。 该装置提供了多个TREF柱的自动化和集成使用以及采用多个流过检测器的GPC系统。 此外,通过在增加TREF洗脱温度的TREF洗脱温度下,通过GPC分析TREF级分,通过在协同和同步的温度循环中操作以提高样品通量的多个TREF柱来对聚合物样品进行TREF / GPC表征的方法。 此外,通过GPC分级随后进行GPC分馏的TREF分馏,GPC / TREF表征聚合物样品的方法。
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公开(公告)号:US20080166817A1
公开(公告)日:2008-07-10
申请号:US11794417
申请日:2006-01-19
申请人: David T. Gillespie , Colin Li Pi Shan , Lonnie G. Hazlitt , Alexander W. Degroot , Peter B. Arnoudse , Charles Allen Williams
发明人: David T. Gillespie , Colin Li Pi Shan , Lonnie G. Hazlitt , Alexander W. Degroot , Peter B. Arnoudse , Charles Allen Williams
CPC分类号: G01N30/468 , G01N25/147 , G01N30/463 , G01N30/54 , G01N33/442 , G01N2030/008 , G01N2030/3007
摘要: Apparatus for GPC/TREF and TREF/GPC characterization of a polymer sample. The apparatus provides for the automated and integrated use of multiple TREF columns and a GPC system employing a multiple flow through detectors. In addition, a method for TREF/GPC characterization of a polymer sample by GPC analysis of TREF fractions at increasing TREF elution temperatures from multiple TREF columns operated in a coordinated and synchronized temperature cycle for increased sample throughput. Also, a method for GPC/TREF characterization of a polymer sample by GPC fractionation followed by TREF fractionation of the GPC fractionations.
摘要翻译: 用于GPC / TREF和TREF / GPC表征聚合物样品的装置。 该装置提供了多个TREF柱的自动化和集成使用以及采用多个流过检测器的GPC系统。 此外,通过在增加TREF洗脱温度的TREF洗脱温度下,通过GPC分析TREF级分,通过在协同和同步的温度循环中操作以提高样品通量的多个TREF柱来对聚合物样品进行TREF / GPC表征的方法。 此外,通过GPC分级随后进行GPC分馏的TREF分馏,GPC / TREF表征聚合物样品的方法。
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公开(公告)号:US20110239746A1
公开(公告)日:2011-10-06
申请号:US13160883
申请日:2011-06-15
申请人: David T. Gillespie , Colin Li Pi Shan , Lonnie G. Hazlitt , Alexander W. Degroot , Peter B. Arnoudse , Charles Allen Williams
发明人: David T. Gillespie , Colin Li Pi Shan , Lonnie G. Hazlitt , Alexander W. Degroot , Peter B. Arnoudse , Charles Allen Williams
IPC分类号: G01N30/02
CPC分类号: G01N30/468 , G01N25/147 , G01N30/463 , G01N30/54 , G01N33/442 , G01N2030/008 , G01N2030/3007
摘要: Apparatus for GPC/TREF and TREF/GPC characterization of a polymer sample. The apparatus provides for the automated and integrated use of multiple TREF columns and a GPC system employing a multiple flow through detectors. In addition, a method for TREF/GPC characterization of a polymer sample by GPC analysis of TREF fractions at increasing TREF elution temperatures from multiple TREF columns operated in a coordinated and synchronized temperature cycle for increased sample throughput. Also, a method for GPC/TREF characterization of a polymer sample by GPC fractionation followed by TREF fractionation of the GPC fractionations.
摘要翻译: 用于GPC / TREF和TREF / GPC表征聚合物样品的装置。 该装置提供了多个TREF柱的自动化和集成使用以及采用多个流过检测器的GPC系统。 此外,通过在增加TREF洗脱温度的TREF洗脱温度下,通过GPC分析TREF级分,通过在协同和同步的温度循环中操作以提高样品通量的多个TREF柱来对聚合物样品进行TREF / GPC表征的方法。 此外,通过GPC分级随后进行GPC分馏的TREF分馏,GPC / TREF表征聚合物样品的方法。
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