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    Process for the dealkylation of tert.-alkyl substituted phenols
    1.
    发明授权
    Process for the dealkylation of tert.-alkyl substituted phenols 失效
    叔烷基取代酚的脱烷基化方法

    公开(公告)号：US4150243A

    公开(公告)日：1979-04-17

    申请号：US744211

    申请日：1976-11-22

    申请人： Dieter W. Bruck ,  Helmut Fiege ,  Johann Renner ,  Feliks Bitners ,  Josef Haydn ,  Karlfried Wedemeyer

    发明人： Dieter W. Bruck ,  Helmut Fiege ,  Johann Renner ,  Feliks Bitners ,  Josef Haydn ,  Karlfried Wedemeyer

    IPC分类号： C07C27/00 ,  C07C37/50 ,  C07C39/07 ,  C07C67/00 ,  C07C39/04

    CPC分类号： C07C37/50

    摘要： A process for the tertiary dealkylation of a tertiary alkyl containing m- and/or p-cresol wherein a tertiary alkyl containing m- and/or p-cresol is continously introduced into a reaction vessel with a small amount of sulfuric acid or an quivalent amount of a sulfonic acid and the reaction vessel contains a high concentration of m- and/or p-cresol or a high boiling phenol which under the prevailing reaction conditions is not substantially vaporized from the reaction mixture. The reaction mixture is maintained at a temperature of no greater than 230.degree. C. The reaction products are withdrawn continuously from the reactor (and separated into its components) and at the same time a small amount of the reaction mixture being withdrawn intermittently or continously from the reactor.

    摘要翻译： 含有m-和/或对甲酚的叔烷基叔烷基化的方法，其中将含有间 - 和/或对 - 甲酚的叔烷基连续地引入具有少量硫酸或一定量的硫酸的反应容器中 的磺酸，并且反应容器含有高浓度的m-和/或对甲酚或高沸点苯酚，其在主要反应条件下基本上不从反应混合物中汽化。 将反应混合物保持在不高于230℃的温度。将反应产物从反应器中连续取出（并分离成其组分），同时将少量的反应混合物间歇地或连续地从 反应堆。

    Process for the production of cyanogen chloride from hydrocyanic acid and chlorine
    2.
    发明授权
    Process for the production of cyanogen chloride from hydrocyanic acid and chlorine 失效
    从氰氰酸和氯生产氯化氰的方法

    公开(公告)号：US4444739A

    公开(公告)日：1984-04-24

    申请号：US367538

    申请日：1982-04-12

    申请人： Heinrich Konigshofen ,  Dieter W. Bruck ,  Alfred Nierth ,  Marko Zlokarnik ,  Hans-Jorg Uhlmann

    发明人： Heinrich Konigshofen ,  Dieter W. Bruck ,  Alfred Nierth ,  Marko Zlokarnik ,  Hans-Jorg Uhlmann

    IPC分类号： C01C3/00 ,  C01B21/18

    CPC分类号： C01C3/004

    摘要： An improved process for the production of cyanogen chloride is disclosed according to which liquid hydrocyanic acid and gaseous chlorine are reacted in an aqueous medium. The liquid hydrocyanic acid and chlorine are introduced into a column-shaped reactor via at least one two-component nozzle. The reaction mixture is removed at the head of the column-shaped reactor. Preferably, the hydrocyanic acid is in liquid form and the chlorine is in gaseous form. By the process disclosed, quantitative yields of cyanogen chloride are obtained separately from aqueous solutions of hydrochloric acid of a strength suitable for commercial use.

    摘要翻译： 公开了一种用于生产氯化氰的改进方法，其中液体氢氰酸和气态氯在水性介质中反应。 液体氢氰酸和氯通过至少一个双组分喷嘴引入柱状反应器。 在柱状反应器的头部除去反应混合物。 优选氢氰酸为液体形式，氯为气态。 通过所公开的方法，氰化氯的定量产率是从适用于商业用途的强度的盐酸水溶液分开获得的。