Process for the recovery of vaporized sublimates from gas streams
    4.
    发明授权
    Process for the recovery of vaporized sublimates from gas streams 失效
    从气流中回收蒸发的升华物的方法

    公开(公告)号:US4391617A

    公开(公告)日:1983-07-05

    申请号:US216934

    申请日:1980-12-16

    申请人: Peter F. Way

    发明人: Peter F. Way

    CPC分类号: C07C51/573 B01D7/02 C07C51/43

    摘要: Sublimate vapors are recovered from gases in a heat-pipe exchanger system, operating alternately in a condensing mode and a melting mode, for condensing on the exchanger tube surfaces such sublimable vapors as phthalic anhydride, maleic anhydride, naphthalene and fatty acids from gases containing said vapors thereof during the condensing mode, and for melting out the accumulated sublimate solids during the melting mode. Multiple, such as two or more units may be used to provide continuous processing of the sublimate vapor-laden gas stream, at least one operating in the condensing mode while simultaneously at least one may operate in the alternate mode. The cooling of opposite heat-pipe exchanger ends to recover sublimate solids is economical and efficient with ambient air, either alone or with some warm recycle exchanger air to adjust the cooling temperature; and the heating to melt out the accumulated solids is effective with heated air or hot waste gases, such as combustion gases, preferably by incineration of residual sublimate tail gas from which the sublimate was condensed, or other hot combustion gases, but other sources of heating the air or gases may be optionally substituted. Important advantage is present in superior heat exchange efficiency using the heat-pipe exchanger for this service, in the ease of switching from heating to cooling of such exchangers for alternate operation in both condensing and melting modes, in the elimination of intermediary heat transfer media and the separate auxiliary equipment required for the heating and cooling cycles, in the utilization of waste heat from combustion gases, and in the great economy for sublimate storage tank vent condensers through elimination of both cooling water and steam requirements.

    摘要翻译: 升华蒸气从热交换器系统中的气体中回收,其以冷凝模式和熔融模式交替运行,用于在交换器管表面上冷凝,如来自含有所述蒸气的气体的邻苯二甲酸酐,马来酸酐,萘和脂肪酸的可升华蒸气 在冷凝模式期间其蒸气,并且在熔化模式期间熔化累积的升华固体。 可以使用多个,例如两个或更多个单元来提供升华的含气气流的连续处理,至少一个以冷凝模式工作,同时至少一个可以在交替模式下操作。 相对的热管交换器末端的冷却以恢复升华的固体,对于环境空气来说是经济和有效的,单独使用或与一些温暖的循环交换器空气调节冷却温度; 并且通过加热的空气或热的废气(例如燃烧气体),优选地通过焚烧升华物被冷凝的残余的升华尾气,或其它热的燃烧气体,但是其它的加热源 空气或气体可以任选地被取代。 在使用热交换器进行这种使用的优点的热交换效率方面存在重要的优点,即在冷凝和熔融模式中交替操作的这种交换器的加热到冷却的切换容易,消除中间传热介质和 加热和冷却循环所需的单独的辅助设备,利用来自燃烧气体的废热,以及通过消除冷却水和蒸汽要求,在经济上用于升华式储罐排气冷凝器。

    Removal of polychlorinated biphenyls by solvent extraction
    5.
    发明授权
    Removal of polychlorinated biphenyls by solvent extraction 失效
    通过溶剂萃取去除多氯联苯

    公开(公告)号:US4764256A

    公开(公告)日:1988-08-16

    申请号:US133263

    申请日:1987-12-16

    申请人: Peter F. Way

    发明人: Peter F. Way

    IPC分类号: C10G21/00 C10G21/28 C10G21/12

    摘要: A method is provided for continuous removal of polychlorinated biphenyl compounds (PCB) from oil contaminated therewith, comprising the steps of continuously extracting PCB compounds from contaminated oil with a PCB-selective solvent in the stripping section of a multistage extraction zone, partially distilling the extract from the extraction zone in a distillation zone, cooling and separating the bottom residue into a solvent phase and an oil/PCB phase, continuously recycling a major portion of the oil/PCB phase as extract reflux to the enriching section of the extraction zone where PCB compounds are extracted from the recycled portion by the solvent phase produced in the stripping section of the extraction zone to increase the PCB content of the extract, and withdrawing a minor portion of the oil/PCB phase from the separation step as a disposable PCB residue.

    摘要翻译: 提供一种用于从被污染的油中连续除去多氯联苯化合物(PCB)的方法,包括以下步骤:在多级萃取区的汽提段中用PCB选择性溶剂从被污染的油中连续提取PCB化合物,部分蒸馏提取物 从蒸馏区的萃取区中将底部残留物冷却并分离成溶剂相和油/ PCB相,连续循环将油/ PCB相的主要部分作为提取物回流至萃取区的富集区,其中PCB 通过在提取区的汽提部分中产生的溶剂相从再循环部分中提取化合物,以提高提取物的PCB含量,并将一部分油/ PCB相从分离步骤中作为一次性PCB残渣取出。

    Apparatus for the recovery of vaporized phthalic anhydride from gas
streams
    6.
    发明授权
    Apparatus for the recovery of vaporized phthalic anhydride from gas streams 失效
    用于从气流中回收蒸发的邻苯二甲酸酐的装置

    公开(公告)号:US4252772A

    公开(公告)日:1981-02-24

    申请号:US942616

    申请日:1978-09-15

    申请人: Peter F. Way

    发明人: Peter F. Way

    CPC分类号: C07C51/43 B01D7/02 C07C51/573

    摘要: Phthalic anhydride is recovered from gases in a multiple heat-pipe exchanger system, one or more for condensing phthalic anhydride from gases containing vapors thereof and one or more simultaneously melting out the condensed phthalic anhydride solids, the exchangers being switched in alternate cycles to melt out from the surfaces of the exchanger tube ends on which the phthalic anhydride solids were first accumulated, and to condense phthalic anhydride solids in the exchanger or exchangers from which the phthalic anhydride was cleared by melting out. The cooling of opposite heat-pipe exchanger ends to recover phthalic anhydride is economical and efficient with ambient air, either alone or with some warm recycle exchanger air to adjust the cooling temperature; and the heating to melt out accumulated phthalic anhydride is effected with hot gases, such as combustion gases, preferably by incineration of residual phthalic anhydride tail gas from which the phthalic anhydride was condensed, or other hot combustion gases, but other sources of heating the air or gases may be optionally substituted. Important advantage is present in superior heat exchange efficiency using the heat-pipe exchanger for this service, in the ready switching from heating to cooling of such exchangers for alternate operation in both condensing and melting out modes, in the elimination of intermediary heat transfer media and the separate auxiliary equipment required for the heating and cooling cycles, in the utilization of waste heat from combustion gases, and in the great economy for phthalic anhydride storage tank vent condensers through elimination of both cooling water and steam requirements.

    摘要翻译: 邻苯二甲酸酐在多重热交换器系统中从气体中回收,一种或多种用于将邻苯二甲酸酐从包含其蒸汽的气体中冷凝,并且一种或多种同时熔解冷凝的邻苯二甲酸酐固体,交换器交替循环以熔化 从其中首先积聚邻苯二甲酸酐固体的交换管端部的表面,并且在交换器中冷凝邻苯二甲酸酐固体,或通过熔融将邻苯二甲酸酐清除的交换器中。 相对的热交换器端部的冷却回收邻苯二甲酸酐是环境空气,单独或与一些温暖的循环交换器空气调节冷却温度是经济和有效的; 并且用热气体如燃烧气体,优选通过焚烧残留的邻苯二甲酸酐缩合的邻苯二甲酸酐尾气或其它热的燃烧气体来进行加热以熔化聚集的邻苯二甲酸酐,但其它加热空气的来源 或气体可以任选地被取代。 存在以下优点:使用热管换热器在这种使用中的热交换效率优异,在冷凝和融化模式中交替操作的这种交换器的加热到冷却的准备切换中,消除中间传热介质和 加热和冷却循环所需的单独的辅助设备,利用来自燃烧气体的废热,以及通过消除冷却水和蒸汽需求,在邻苯二甲酸酐储罐出口冷凝器的巨大经济中。

    Swing arm feeder
    7.
    发明授权
    Swing arm feeder 失效
    摆臂送料器

    公开(公告)号:US5341962A

    公开(公告)日:1994-08-30

    申请号:US18894

    申请日:1993-02-17

    IPC分类号: F23G5/44 G01F11/24

    CPC分类号: F23G5/442

    摘要: A feeder for discharging a load of material includes a hopper, a swing arm pivoting between raised and lowered positions in the hopper, and a ram mounted on the free end of the swing arm. The ram is moved by the swing arm back and forth on a curved floor in a trapezoidally shaped trough underneath the hopper to push material in the trough out of the hopper through a discharge outlet. A shutoff valve at the discharge outlet prevents backflow of discharged material into the trough.

    摘要翻译: 用于卸载材料的进料器包括料斗,在料斗中在升高和降低位置之间枢转的摆臂以及安装在摆臂自由端上的冲头。 该冲头由摆臂在料斗下面的梯形槽中的弯曲地板上来回移动,以通过排出口将料斗从料斗中推出。 排出口处的截止阀可防止排出的材料回流到槽中。